Sample Preparation
Mostrando 13-24 de 705 artigos, teses e dissertações.
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13. Multivariate Analysis: Use of Doehlert Design (DD) for Optimization of a Simple Sample Preparation Procedure for the Determination of Inorganic Constituents in Cocoa Beans Employing Microwave Acid Digestion and ICP OES
This study presents a microwave-assisted procedure for sample preparation of cocoa beans using diluted HNO3 with H2O2 for the determination of Ba, Ca, Cu, K, Mg, Mn, P, S, Sr and Zn by inductively coupled plasma optical emission spectrometry (ICP OES). Doehlert modified design was used for optimization of experimental condition, and the volume of H2O2 (0, 0.
J. Braz. Chem. Soc.. Publicado em: 2020-10
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14. The paths of Graves’ disease in the 21st century: precision medicine is closer
This study presents a microwave-assisted procedure for sample preparation of cocoa beans using diluted HNO3 with H2O2 for the determination of Ba, Ca, Cu, K, Mg, Mn, P, S, Sr and Zn by inductively coupled plasma optical emission spectrometry (ICP OES). Doehlert modified design was used for optimization of experimental condition, and the volume of H2O2 (0, 0.
Arch. Endocrinol. Metab.. Publicado em: 2020-10
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15. Systemic treatment and surgery versus systemic treatment alone for metastatic breast cancer
This study shows the development and application of an analytical method for the determination of bisphenol A (BPA) in aqueous samples such as tap, river and mineral water and plastic leachates, based on an extensive literature search to understand the gaps for the determination of BPA in aqueous samples. We found that most of the methods in the literature e
Rev. Assoc. Med. Bras.. Publicado em: 2020-08
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16. A Simple and Effective Liquid-Liquid-Liquid Microextraction Method with Ultraviolet Spectrophotometric Detection for the Determination of Bisphenol A in Aqueous Matrices and Plastic Leachates
This study shows the development and application of an analytical method for the determination of bisphenol A (BPA) in aqueous samples such as tap, river and mineral water and plastic leachates, based on an extensive literature search to understand the gaps for the determination of BPA in aqueous samples. We found that most of the methods in the literature e
J. Braz. Chem. Soc.. Publicado em: 2020-08
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17. Nursing Guidelines on Cardiac Surgery and Parents’ Anxiety: Randomized Clinical Trial
Abstract Objective: The preparation of parents of children who should undergo cardiac surgery requires special treatment such as the explanations about the event. This study aims to compare the effects of standardized nursing guidelines with routine institutional orientation on the anxiety of parents of children undergoing cardiac surgery. Methods: Randomi
Braz. J. Cardiovasc. Surg.. Publicado em: 2020-08
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18. Rapid Determination of Vitamins D2 and D3 in Dairy Products by High-Performance Liquid Chromatography after Solid Phase Extraction Based on Polystyrene/Polypyrrole Composite Nanofibers
The detection of vitamin D in complex samples is challenging because of the instability of vitamin D in sample preparation. To resolve this problem, packed-fiber solid-phase extraction (PFSPE) has been successfully developed for the pre-treatment of samples containing vitamin D2 (D2) and vitamin D3 (D3) in dairy products. Based on PFSPE, vitamin D could avoi
J. Braz. Chem. Soc.. Publicado em: 2020-06
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19. A Protocol for Fish Lipid Analysis Using Nuclear Magnetic Resonance Spectroscopy
This article reports on an easy-to-follow methodology for fish lipids analysis, including the biological sample collection, lipid extraction, sample preparation, nuclear magnetic resonance (NMR) spectroscopy analysis and statistical data analysis, with details on parameters used for the NMR analysis and the care needed in each step execution. As an example o
J. Braz. Chem. Soc.. Publicado em: 2020-04
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20. ELECTROCHEMICAL DETERMINATION OF 2-NAPHTHYLAMINE IN PERFUME SAMPLES USING BORONDOPED DIAMOND ELECTRODE
This work presents a simple electrochemical method for 2-naphthylamine (2NAP) determination in perfume by differential-pulse voltammetry (DPV) employing a boron-doped diamond (BDD) electrode cathodically treated. Simple dilution of sample in supporting electrolyte was performed before electrochemical analysis. A borate buffer solution of pH 10.0 containing 2
Quím. Nova. Publicado em: 2020-03
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21. Optimization of New Sample Preparation Technique for the Determination of Methadone and Codeine in Plasma Sample by GC-FID
A continuous sample drop flow microextraction (CSDF-ME) technique was modified for the pretreatment of plasma samples in the determination of methadone and codeine. The limit of detection and linear range for methadone were 15.0 µg L-1 and 0.1-10.0 mg L-1, respectively. The detection limit and linear range for codeine were 25.0 µg L-1 and 0.2-15.0 mg L-1,
J. Braz. Chem. Soc.. Publicado em: 2020-03
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22. METABOLÔMICA DE PLANTAS: MÉTODOS E DESAFIOS
Metabolomics has played a central role in various areas of plant sciences, offering new perspectives for the advancement of agriculture, drug discovery, chemical ecology and taxonomy. Plant metabolomics (identification and quantification) aims to understand the relationship between biological systems and genetic, pathological and or environmental stimuli in
Quím. Nova. Publicado em: 2020-03
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23. Sucrose-free milk chocolate manufacture using bulking agents and a non-caloric sweetener
Abstract Sucrose is important in the production of chocolates because it contributes to its texture and sensory acceptance. The aim was to evaluate the effect of adding bulking agents and a non-caloric sweetener in the preparation of a sucrose-free milk chocolate. One control sample (with sucrose) and 11 treatments were taken varying the ratio between bulkin
Food Sci. Technol. Publicado em: 2020-03
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24. Quantification of Glyphosate and AMPA by HPLC-ICP-MS/MS and HPLC-DAD: A Comparative Study
In this work, the direct determination methodology of glyphosate and aminomethylphosphonic acid (AMPA) by high performance liquid chromatography (HPLC) using inductively coupled plasma with triple quadrupole mass spectrometer (ICP-MS/MS) was compared with the conventional method using diode array detector (HPLC-DAD). Both methods were selective, but the chro
J. Braz. Chem. Soc.. Publicado em: 2020-02