Nuclear Magnetic Ressonance Nmr
Mostrando 1-12 de 17 artigos, teses e dissertações.
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1. SYNTHESIS OF GLYCEROL-FLUORINATED TRIAZOLE DERIVATIVES AND EVALUATION OF THEIR FUNGICIDAL ACTIVITY
The control of fungal species in agriculture is mainly conducted with the use of contact or systemic fungicides. However, environmental and human health concerns and increased resistance of fungal species to existing fungicides have increased the pressure on researchers to find new active ingredients for fungal control which present low toxicity to non-targe
Química Nova. Publicado em: 2022
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2. Synthetic Niobium Oxyhydroxide as a Bifunctional Catalyst for Production of Ethers and Allyl Alcohol from Waste Glycerol
A synthetic niobia was modified by treatment with hydrogen peroxide to be used as a catalyst for converting glycerol into petrochemical compounds. The catalytic properties of niobium oxyhydroxide were obtained by generating acidic and oxygenated groups (peroxo groups) on the solid surface. Compounds like ethers and allyl alcohol were obtained. A very active
J. Braz. Chem. Soc.. Publicado em: 2017-11
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3. Solid-Phase Peptide Synthesis of Dipeptide (Histidine-β-Alanine) as a Chelating Agent by Using Trityl Chloride Resin, for Removal of Al3+, Cu2+, Hg2+ and Pb2+: Experimental and Theoretical Study
Solid-phase peptide synthesis of dipeptide (histidine-β-alanine) as a chelating agent examined by common N-9-fluorenylmethyloxycarbonyl-N-trityl-L-histidine and tert-butyloxycarbonyl-β-alanine-OH amino acid derivatives. Trityl chloride resin was used as a carrier resin. The molecular structure of the dipeptide was definite by using different methods such a
J. Braz. Chem. Soc.. Publicado em: 2016-10
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4. Synthesis and Characterization of Methylcellulose Produced from Bacterial Cellulose under Heterogeneous Condition
In this work, methylcellulose (MC) was produced from bacterial cellulose (BC), using dimethyl sulfate in a 3 h (MC3h) or 5 h (MC5h) reaction under heterogeneous conditions, with reagent substitution at each hour. MC3h showed a degree of substitution (DS) of 2.26 ± 0.13 and MC5h showed a DS of 2.33 ± 0.05. The two samples were characterized by Fourier trans
J. Braz. Chem. Soc.. Publicado em: 2015-09
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5. Desenvolvimento e caracterização de dispositivo de PLLA/Trietil-Citrato associado à derme suína acelular para reparação de lesões cutâneas / Development and characterization of PLLA/Triethyl citrate device associated to acellular dermal matrix to repair cutanous wounds
One of the challenges of the Tissue Engineering is to promote a better functioning of organs and tissues damaged by diseases or traumas. With target for developing a biphasic device for future regeneration and dermal application in Tissue Engineering and Regenerative Medicine, fibroblasts from VERO cell line were cultivated on a porcine acellular dermal matr
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 15/02/2012
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6. Certificação de beta-N-metil-amino-alanina: um modelo para produção de materiais de referência de substâncias orgânicas obtidas in-house / Certification of beta-N-methyl-amino-alanine: a model for in-house preparation of reference materials of organic substances
Materiais de Referência (MR) de substâncias químicas têm ampla aplicação, sobretudo na área analítica, servindo de referência para validação de métodos, calibração de instrumentos e controle de qualidade, estabelecendo a comparabilidade de resultados analíticos em escala global e permitindo a transferência da exatidão entre métodos, laborat
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 04/05/2011
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7. Use of steady state free precession (SSFP) to enhance signal to noise ratio in high resolution NMR / Desenvolvimento da técnica de precessão livre no estado estacionário para aumento da razão sinal ruído em espectros de RMN de alta resolução
It was performed a detailed analysis of the advantages and disadvantages of Steady State Free Precession (SSFP) sequence for a rapid acquisition of 13C Nuclear Magnetic Resonance (NMR) spectra. The SSFP regime is obtained by the application of a pulse train with the same phase, duration and intensity, separated by a time interval (Tp) shorter than the transv
Publicado em: 2009
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8. INFLUENCE OF SYNTHESIS PARAMETERS IN THE PROPERTIES OF MCM-22 ZEOLITE / INFLUÊNCIA DOS PARÂMETROS DE SÍNTESE NAS PROPRIEDADES DA ZEÓLITA MCM-22
MCM-22 zeolite was first synthesized by Mobil researchers in 1990. It is an aluminosilicate with molecular sieve characteristics and several applications in catalytic processes because of its two independent pore systems. In this work, the MCM-22 zeolite synthesis conditions were studied using both static as stirred hydrothermal treatment. Molar composition
Publicado em: 2008
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9. Ditiocarbamatos derivados do glicoluril, ácido úrico, ácido parabânico e hidantoína: compostos de coordenação e uso como inibidores de corrosão do bronze
This thesis work is about dithiocarbamates compounds, their synthesis, study and application as corrosion inhibitors. The dithiocarbamates herein studied were synthesized from four substances: glycoluril, uric acid, parabanic acid and hydantoin. The pro-ligands were synthesized through reaction with CS2 and NaOH, characterized via elemental analysis (CHN) an
Publicado em: 2008
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10. Preparação de resinas de poliuretana à base de óleo de mamona e dietanolamina
The aim of this work was the preparation of polyols from reactions between castor oil and dietanolamine to increase the hydroxyl content and the network degree in the products to application in electronic devices. The polyols and the mixtures obtained were characterized by nuclear magnetic ressonance. Castor oil (CO) is a natural triglyceride - based polyol
Publicado em: 2007
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11. SÃntese e caracterizaÃÃo de surfactantes glicosÃdicos a partir da amilose e alquil fenÃis extraÃdos do LCC. / Synthesis and characterization of glycosidic surfactantes from amylose and alkyl extracted phenols of the LCC.
Nonionic surfactants are synthesised from renewable raw materials such as fat acids and sugars. They are dermatological safe, biodegradable and provide excellent surface active properties, such as good wettability, good foaming production and good cleaning ability. The present work deals with the synthesis and characterization of alkyl polyglycosides where t
Publicado em: 2007
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12. Strutural characterization of hypothetical proteins complex - XACb0032/XACb0033 from Xanthomonas axonopodis pv. citri / Caracterização estrutural do complexo de proteinas hipoteticas - XACb0032/XACb0033 da bacteria Xanthomonas axonopodis pv. citri
Xanthomonas axonopodis pv. citri (Xac) is the causative agent of citrus canker, a disease of significant economic importance worldwide. The molecular bases of the virulence mechanism are still unknown, but is believed that transfer of bacterial virulence proteins directly into the host cell cytoplasm is mediated by protein secretion systems, mainly type III
Publicado em: 2007