Microscopy
Mostrando 25-36 de 15344 artigos, teses e dissertações.
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25. Analysis and evaluation of structural properties of Co3O4 microparticles obtained at low temperature
Abstract In the present research, the synthesis of cobalt oxide Co3O4 was carried out using the sol-gel technique with subsequent heat treatment at 225 and 235 °C. The final product obtained was characterized by X-ray diffraction (XRD), showing a pure crystalline phase of Co3O4, cell parameters a=b=c=8.071 Å, and a volume of 525.7 Å3. The particle size wa
Cerâmica. Publicado em: 2022
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26. Atomic Absorption Spectrometry as an Alternative to Determine the Presence of Gold Nanoparticles on or in Silica Matrix
Two different gold-silica-based nanomaterials were prepared: (i) silica-supported gold nanoparticles (AuNP/SiO2); and (ii) gold-silica core-shell nanoparticles (AuNP@SiO2). Three strategies for sample treatment (S), consisting in acid treatments, were employed: (S1) HNO3; (S2) HNO3 + HCl; and (S3) HF + HNO3 + HCl, applying microwave oven digestion for S2 and
Journal of the Brazilian Chemical Society. Publicado em: 2022
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27. Simple and fast process using hydrochloric acid for producing synthetic zinc-rich stevensite
Abstract In the last decades, clays have been used in sectors such as health and cosmetics. This requires products that are increasingly pure and present homogeneous properties, hardly found in natural clays. The use of synthetic clays can be a solution. For this, it is necessary to explore techniques for their production. The main focus of this study was to
Cerâmica. Publicado em: 2022
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28. The influence of separately and combined bentonite and kaolinite as binders for pelletization of NaA zeolite from coal fly ash
Abstract Pelletization of zeolitic materials is required to facilitate their practical industrial and commercial applications. Zeolite-NaA was synthesized from fly ash by the fusion method and shaped into spherical granules. Bentonite, kaolinite, and a combination of bentonite with kaolinite were tested as binders with different contents from 5 to 10 wt%. Th
Cerâmica. Publicado em: 2022
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29. Obtainment of a new metal matrix composite from the recycling of UNS S31803 duplex stainless steel by powder metallurgy
Abstract The purpose of circular economy is to maximize resources efficiency. With the increase in consumption of raw materials, energy and waste generation, recycling is necessary for environmental and industrial reasons. Thus, the powder metallurgy, together with mechanical milling, stands as a new method for scraps recycling. This study aimed to produce U
REM - International Engineering Journal. Publicado em: 2022
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30. An alternative route to extract nickel and cobalt from non-commercial laterite ore
Abstract Laterite ores, which represent around two-thirds of nickel reserves, became an important source of nickel and cobalt metals. The objective of the present study was to investigate the efficiency of a hybrid route to extract nickel and cobalt present in a laterite ore sample which was not commercially attractive to be processed through the current rou
REM - International Engineering Journal. Publicado em: 2022
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31. Designing and fabrication of a low-cost dip-coater for rapid production of uniform thin films
In this work, a self-made dip-coater equipment was developed for the fabrication of thin films. The assembly of the apparatus was carried out using simple mechanical and electronic pieces, recycle parts, and spending an inexpensive budget suitably. The production, software design, and features of the device were focused on the sol-gel dip-coating method, whi
Química Nova. Publicado em: 2022
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32. Preparation and performance of magnetic zirconium-iron oxide nanoparticles loaded on palygorskite in the adsorption of phosphate from water
Magnetic zirconium-iron oxide nanoparticles loaded on palygorskite as a low-cost adsorbent was produced by one-step co precipitation technique and its properties for phosphate adsorption were overall investigated. The Brunauer Emmett Teller (BET) specific surface area analysis, scanning electron microscopy (SEM), thermo gravimetric analysis (TGA), Fourier tr
Química Nova. Publicado em: 2022
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33. Expansion of cord blood stem cells in fibronectin-coated microfluidic bioreactor
ABSTRACT Background: Hematopoietic stem/progenitor cell transplantation is the main treatment option for hematological malignancies and disorders. One strategy to solve the problem of low stem cell doses used in transplantation is pre-transplant expansion. We hypothesized that using fibronectin-coated microfluidic channels would expand HSPCs and keep self-r
Hematology, Transfusion and Cell Therapy. Publicado em: 2022
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34. Enhancement of Visible Light-Responsive Photocatalytic Efficiency by Using a Laccaic Acid-Modified Titanium Dioxide Photocatalyst
In this study, a laccaic acid-modified TiO2 photocatalyst (Lac-TiO2) was prepared via an impregnation method with 0.50, 1.00, 2.50, and 5.00 wt.% laccaic acid. The products’ physical properties were examined through X-ray powder diffraction (XRD), field emission scanning electron microscopy (FE-SEM), X-ray photoemission spectroscopy (XPS), UV-Vis diffused
Journal of the Brazilian Chemical Society. Publicado em: 2022
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35. Subbasal corneal nerve damage in patients with bacterial keratitis: in vivo confocal microscopy study
RESUMO Objetivo: Relatar as alterações no plexo nervoso corneano subbasal em pacientes com ceratite infecciosa de origem bacteriana utilizando a microscopia confocal in vivo. Métodos: Treze olhos de 13 pacientes com ceratite bacteriana unilateral e 12 indivíduos saudáveis como grupo controle foram incluídos prospectivamente no estudo. A microscopia c
Arquivos Brasileiros de Oftalmologia. Publicado em: 2022
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36. Three-dimensional cell culture for the study of nasal polyps
Abstract Objectives: Three-dimensional (3D) cell cultures have many applications such as stem cell biology research, new drug discovery, cancer, and Chronic Rhinosinusitis with Nasal Polyps (CRSwNP). This disease is characterized by a significant impact on quality of life and productivity. The diversity of factors that act in the progression of CRSwNP point
Brazilian Journal of Otorhinolaryngology. Publicado em: 2022