Mesoporous Silica
Mostrando 1-12 de 75 artigos, teses e dissertações.
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1. Evaluation of the Structural Integrity of Layered Double Hydroxides and Mesoporous Silica During the Preparation of Heterostructures
Heterostructures constructed with mesoporous silica and layered double hydroxides are interesting for catalytic and drug delivery applications. Different arrangements between these phases are possible. In this study, we prepared heterostructures by embedding layered double hydroxides phases [M4Al2(OH)12](CO3) (M = Mg2+ or Zn2+) within the MCM41 mesoporous si
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. PREPARATION OF HYBRID POLYMERS AND USE AS CONTROLLED RELEASE DELIVERY VEHICLE FOR VOLATILE REPELLENT TO CONTROL Aedes aegypti
The Zika virus is a flavivirus spread by the Aedes aegypti mosquito, which also transmits dengue and chikungunya. Current forms of control include elimination of mosquito breeding sites, use of insecticides, repellents and other means. The present study developed new adsorbent materials based on silica and biomaterials capable of releasing an Aedes aegypti m
Quím. Nova. Publicado em: 2021-04
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3. Magnetic and Mesoporous Silica-Niobia Material as Modifier of Carbon Paste Electrode for p-Nitrophenol Electrochemical Determination
In the present work, the sol-gel synthesis method was employed as strategy to obtain a magnetic and mesoporous silica-niobia material. The planned synthesis was based on the hetero-condensation of niobium and silicon alkoxide precursors, in the presence of spherical magnetite particles. The resulting material presented interesting characteristics such as mag
J. Braz. Chem. Soc.. Publicado em: 2021-03
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4. Comparative Effect of Calcium Mesoporous Silica Versus Calcium and/or Fluoride Products Against Dental Erosion
Resumo O objetivo deste estudo foi comparar os efeitos de uma única aplicação de uma nova nanopartícula de sílica mesoporosa de cálcio (Ca2+ -MSN) versus outros produtos à base de cálcio e / ou fluoreto contra a erosão dentária. Blocos de esmalte foram parcialmente cobertos e distribuídos em seis grupos (n = 10): Ca2+ -MSNs; fosfopeptídeos de cas
Braz. Dent. J.. Publicado em: 2020-04
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5. Synthesis and characterization of mesoporous materials with SBA and MCM structure types
Resumo Materiais mesoporosos são estruturas promissoras para aplicação em catálise e adsorção devido à elevada área superficial e grande tamanho dos poros. Materiais mesoporosos foram sintetizados pelo método hidrotérmico com novos surfactantes, distintos daqueles observados na literatura, a fim de realizar um estudo de sua estrutura e obter materi
Cerâmica. Publicado em: 14/11/2019
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6. Silica/Titania Graphite Composite Modified with Chitosan and Tyrosinase Employed as a Sensitive Biosensor for Phenolic Compounds
A mesoporous, high surface area and conductive silica/titania graphite composite modified with chitosan and functionalized with tyrosinase was prepared. The composite was obtained by the sol-gel method and the surface of the resultant material was modified with chitosan solutions containing 5, 10 and 15% by mass. The textural characterization showed that eve
J. Braz. Chem. Soc.. Publicado em: 24/10/2019
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7. Development of Silica-Based Monoliths for the Capture of CO2
The synthesis of mesoporous materials in macroscopic scale, as for example, the monoliths, has been of great interest in view of the wide range of applications that this material holds. Thus, this work consists of the production of silica monoliths for the purpose of they being used in the carbon dioxide (CO2) adsorption process. The adsorbents were prepared
Mat. Res.. Publicado em: 30/09/2019
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8. Imidazo[1,2-a]pyridine A3-Coupling Catalyzed by a Cu/SiO2 Material
In this work, we report the preparation of a copper-silica material (Cu/SiO2) by a sol-gel methodology and its characterization concerning composition and textural properties. The Cu/SiO2 material was successfully applied as a Lewis acid heterogeneous catalyst for the A3-coupling from 2-aminopyridine, aldehydes and alkynes to imidazo[1,2-a]pyridines (45-82%)
J. Braz. Chem. Soc.. Publicado em: 16/09/2019
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9. Synthesis of Highly Ordered Mesoporous MCM-41: Selective External Functionalization by Time Control
Sol-gel synthesis is commonly used to modify the surface of mesoporous silica nanoparticles (MSN) with organic groups through the co-condensation method. The template removal, and the site-controlled addition of organic groups and their partial occlusion inside the framework walls are still a challenge in the one-pot synthesis. Here, we optimize the synthesi
J. Braz. Chem. Soc.. Publicado em: 12/08/2019
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10. Design and characterization of nanocarriers loaded with Levofloxacin for enhanced antimicrobial activity; physicochemical properties, in vitro release and oral acute toxicity
Inorganic and carbon based nanomaterials are widely used against several diseases, such as cancer, autoimmune diseases as well as fungi and bacteria colonization. In this work, Santa Barbara Amorphous mesoporous silica (SBA), Halloysite Nanotubes (HNTs) and Multiwalled Carbon Nanotubes (CNTs) were loaded with fluoroquinolone Levofloxacin (LVF) to be applied
Braz. J. Pharm. Sci.. Publicado em: 12/08/2019
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11. Influence of Crystallization and Ageing Time on the Reproducibility of Mesoporous Molecular Sieve SBA-15
ABSTRACT The study aimed to assess how the crystallization and ageing times in SBA-15 synthesis influence the reproducibility and particle size of mesoporous molecular sieves. X-ray diffraction showed that higher crystallization times provide greater reproducibility of mesoporous silica, due to the fact that there is no significant variation in the width and
Matéria (Rio J.). Publicado em: 10/06/2019
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12. Síntese e avaliação de nanopartículas de sílica mesoporosas na liberação controlada de feromônios repelentes de abelha
Resumo Neste estudo foi avaliado o armazenamento e liberação de feromônios repelentes de abelhas em uma nanoestrutura de sílica mesoporosa. O nanomaterial foi sintetizado via método sol-gel e caracterizado por microscopia eletrônica de transmissão, espectroscopia de infravermelho e método BET. As nanopartículas mesoporosas apresentaram-se com área
Cerâmica. Publicado em: 06/06/2019