Fractional Factorial Design
Mostrando 1-12 de 56 artigos, teses e dissertações.
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1. Dispersive Solid-Phase Extraction Using 3-Mercaptopropyltrimethoxysilane Functionalized Magnetic MWCNT-Based Nanocomposite for Selective and Efficient Preconcentration of Pb2+ with FAAS Determination
A novel nanocomposite based on magnetic multiwalled carbon nanotubes coated with SiO2 and functionalized with 3-mercaptopropyltrimethoxysilane (3-MPTMS) was prepared for the efficient extraction and quantification of lead ions from water samples. The adsorption capacity of this adsorbent could reach 1.995 mg g-1 Pb2+ in an equilibrium time of 30 min. Under o
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Multivariate Optimization Applied to the Synthesis of Meglumine Antimoniate with Low Levels of Trivalent Antimony
Meglumine antimoniate (MA) is a pentavalent antimony (SbV) drug recommended for the treatment of leishmaniasis. It is known that the trivalent antimony (SbIII) present as a residue in MA contributes to the drug side effects. In this article, multivariate optimization was used in the synthesis of MA in order to obtain a drug with low levels of SbIII. Four var
J. Braz. Chem. Soc.. Publicado em: 2021-08
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3. Development of Analytical Method for Determination of Inorganic Constituents in Powder Refreshment Using Dilute Mineral Acids and Detection by ICP OES
An analytical method for multi-elementary determination in powder refreshment, based on sample digestion using dilute mineral acids and detection by inductively plasma coupled optical emission spectrometry (ICP OES) is proposed. Chemometric tools, such as fractional factorial design and principal component analysis (PCA) and hierarchical cluster analysis (HC
J. Braz. Chem. Soc.. Publicado em: 2021-07
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4. Development of a Methodology Based on Extraction Induced by Emulsion Breaking for Copper Determination in Gasohol by Graphite Furnace Atomic Absorption Spectrometry
The development of a method based on extraction induced by emulsion breaking (EIEB) aiming copper determination in gasohol using graphite furnace atomic absorption spectrometry (GF AAS) is reported. Emulsification of the gasohol samples was carried out using nitric acid solution, (1,1,3,3-tetramethylbutyl)phenyl-polyethylene glycol surfactant (Triton X-114),
J. Braz. Chem. Soc.. Publicado em: 2021-02
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5. Performance of Avocado Seed Activated Carbon as Adsorbent for Highly Sensitive Determination of Cd Using a Flow Injection System Online Coupled to TS-FF-AAS
A flow-injection preconcentration system using detection by the thermospray flame furnace atomic absorption spectrometry (FIA-TS-FF-AAS) is proposed. Cd2+ are adsorbed on avocado seed activated carbon (ASAC) packed into a cylindrical mini-column and eluted using HCl solutions for the detection system. A 25–1 fractional factorial and Doehlert matrix design
J. Braz. Chem. Soc.. Publicado em: 2020-01
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6. Lipase Production by Aspergillus niger C by Submerged Fermentation
Abstract This study aimed to evaluate the effects of variables on the process of lipases production by Aspergillus niger C by submerged fermentation (SmF). The production assays were performed in shake flasks for 72 hours at 150 rpm and 32°C. First, a fractional factorial design 25-1 (FFD) was carried out to evaluate the effect of the following process vari
Braz. arch. biol. technol.. Publicado em: 24/10/2019
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7. OPTIMIZATION OF HIGH-CONCENTRATION TRANS-ANETHOLE PRODUCTION THROUGH HYDRODISTILLATION OF STAR ANISE
Abstract Illicium verum Hook essential oil (EO) is composed mainly of trans-anethole (TA), which has therapeutic potential. The extraction is usually by hydrodistillation, taking long hours, leaving the process costly and product with lower quality. Thus, the present study sought to optimize dehydrated fruit fragmentation by Box-Wilson central composite desi
Braz. J. Chem. Eng.. Publicado em: 30/09/2019
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8. Factorial design to obtain magnetized poly(ethyl acrylate-co-divinylbenzene)
Abstract Magnetized polymers are produced by incorporating magnetic particles in a polymeric matrix. This article describes the use of the suspension polymerization technique using ethyl acrylate and divinylbenzene as monomers, in the presence of heptane and/or toluene as diluent, initiated by free radicals. To produce the polymer, we first performed fractio
Polímeros. Publicado em: 04/07/2019
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9. Uma análise conjunta para identificação dos atributos de um dispositivo para reconhecimento de características de produtos alimentícios customizados
Resumo A possibilidade de combinação de ingredientes alimentícios em cada refeição torna complexo o reconhecimento das características dos alimentos personalizados. A utilização de dispositivos com tecnologias da Internet of Things (IoT) consiste em uma alternativa para os clientes acessarem informações dos alimentos personalizados. Nesta pesquisa,
Braz. J. Food Technol.. Publicado em: 06/06/2019
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10. Optimization of Atmospheric Pressure Photoionization for the Crude Oil Analysis Using Ultra-High Resolution Mass Spectrometry
Design of experiments (DOE) applied to mass spectrometry (MS), mainly focusing on the optimization of ionization techniques, has been applied to optimize experiments in order to provide the highest amount of information with the lowest number of experiments. However, DOE has not been used in petroleomics. For the first time, we applied DOE to optimize the ma
J. Braz. Chem. Soc.. Publicado em: 2019-04
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11. Chicken nuggets packaging attributes impact on consumer purchase intention
Abstract The aim of this study was to evaluate the influence of chicken nuggets packaging attributes on Brazilian consumer purchase intention. Focus group technique was employed in order to identify the relevant packaging characteristics. Forty consumers were interviewed in six sessions where five different types of chicken nuggets packaging were evaluated.
Food Sci. Technol. Publicado em: 10/12/2018
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12. Dynamic maceration of Matricaria chamomilla inflorescences: optimal conditions for flavonoids and antioxidant activity
ABSTRACT The aim of this paper was to study and optimize the dynamic maceration process to obtain Matricaria chamomilla L., Asteraceae, inflorescences extracts with optimum flavonoid content and antioxidant activity using a multivariate approach. Hydroalcoholic extracts were obtained by dynamic maceration in lab scale and the influence of extraction temperat
Rev. bras. farmacogn.. Publicado em: 2018-01