Fractional Factorial Design
Mostrando 13-24 de 56 artigos, teses e dissertações.
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13. Turbo-extraction of glycosides from Stevia rebaudiana using a fractional factorial design
ABSTRACT Stevia rebaudiana (Bertoni) Bertoni, Asteraceae, leaf extract has recently called the attention of food industry as a proposal for natural sweetener. The sweet flavor is attributed to the glycosides, in especial stevioside and rebaudioside A, which are the plant main chemical markers. The aim of the work reported here was to optimize the turbo-extra
Rev. bras. farmacogn.. Publicado em: 2017-08
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14. Coencapsulation of trans-Dehydrocrotonin and trans-Dehydrocrotonin:hydroxypropyl-β-cyclodextrin into Microparticles
The aim of this study was to develop and characterize poly-ε-caprolactone (PCL) and poly(D,L-lactic-co-glycolic)-acid (PLGA) microparticles containing coencapsulated trans-dehydrocrotonin (t-DCTN) and t-DCTN:hydroxypropyl-β-cyclodextrin inclusion complex (t-DCTN:HP-β-CD), with t-DCTN loaded at concentrations ranging from 11.25 to 45.00 mg. A preformulatio
J. Braz. Chem. Soc.. Publicado em: 2017-08
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15. ADSORPTION PROCESS OF MOLECULARLY IMPRINTED SILICA FOR EXTRACTION OF LACTOSE FROM MILK
Abstract In Brazil, about 25-30% of the population has some degree of intolerance to lactose, a disorder associated with the inability of the body to digest lactose due to a disability or absence of the enzyme lactase. The goal of this study was to evaluate the performance of adsorption of lactose from fresh milk using a fixed bed column of molecularly impri
Braz. J. Chem. Eng.. Publicado em: 2016-06
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16. Dispersive Liquid-Liquid Microextraction with Liquid Chromatography-Tandem Mass Spectrometry for the Determination of Triazine, Neonicotinoid, Triazole and Imidazolinone Pesticides in Mineral Water Samples
Mineral water is known for its high purity. Because mineral water is produced by the infiltration of water through the soil, there is the possibility of contamination with pesticides. The aim of this study was to develop a simple, rapid and efficient method for the extraction and preconcentration of different classes of pesticides in mineral water samples by
J. Braz. Chem. Soc.. Publicado em: 2015-09
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17. Catalytic Ozonation Using Fe2+ in the Treatment of Dairy Effluent in a Semi-Batch Process with Recycle
This work describes the treatment of dairy industry effluent using catalytic ozonation with Fe2+ as its catalyst in a semi-batch process with recycle. A fractional factorial design 24-1 was used with a reduction percentage of total organic carbon (TOCred) as response. Optimal conditions were obtained by the reaction time of 30 min, o
J. Braz. Chem. Soc.. Publicado em: 2015-07
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18. Optimization of Auxiliary Solvent Demulsification Microextraction for Determination of Cyanide in Environmental Water and Biological Samples by Microvolume UV-Vis Spectrophotometry
A new, simple, rapid and efficient solvent terminated-auxiliary solvent-dispersive liquid-liquid microextraction (ST-AS-DLLME) technique for determination of cyanide ions by microvolume UV-Vis spectrophotometry was developed. Effective parameters on the extraction and absorbance of cyanide were optimized using two optimization methods: fractional factorial d
J. Braz. Chem. Soc.. Publicado em: 2015-06
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19. Optimization of the extraction process of polyphenols from cashew apple agro-industrial residues
The goal of this study was to determine the chemical composition of cashew apples agro-industrial residue and optimize the process of polyphenols extraction in this residue. The extraction process conditions were defined using a 24-1 fractional factorial experimental design using acetone and methanol as solvents. The independent variables were: time (30 to 9
Food Sci. Technol. Publicado em: 2015-04
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20. STATISTICAL OPTIMIZATION OF MINERAL SALT AND UREA CONCENTRATION FOR CELLULASE AND XYLANASE PRODUCTION BY Penicillium echinulatum IN SUBMERGED FERMENTATION
Abstract Penicillium echinulatum S1M29 is a mutant with cellulase and xylanase production comparable to the most studied microorganisms in the literature. However, its potential to produce these enzymes has not been fully investigated. This study aimed at optimizing salt and urea concentrations in the mineral solution, employing the response surface methodol
Braz. J. Chem. Eng.. Publicado em: 2015-03
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21. Growth Characteristics Modeling of Mixed Culture of Bifidobacterium bifidum and Lactobacillus acidophilus using Response Surface Methodology and Artificial Neural Network
Different culture conditions viz. additional carbon and nitrogen content, inoculum size and age, temperature and pH of the mixed culture of Bifidobacterium bifidum and Lactobacillus acidophilus were optimized using response surface methodology (RSM) and artificial neural network (ANN). Kinetic growth models were fitted for the cultivations using a Fractional
Braz. arch. biol. technol.. Publicado em: 2014-12
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22. Influence of reaction operation conditions on the final properties of high impact polystyrene (hips)
The main objective of the present work is to analyze the influence of some important operational reaction parameters (agitation speed, polybutadiene - PB - content and initiator concentration) on the final properties of High Impact Polystyrene (HIPS) produced in bulk. Variable effects are analyzed both qualitatively and quantitatively with the help of a frac
Braz. J. Chem. Eng.. Publicado em: 2013-09
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23. BTEX: DESENVOLVIMENTO DE BARRAS DE EXTRAÇÃO SORTIVA, DETERMINAÇÃO EM EFLUENTE HOSPITALAR E DEGRADAÇÃO POR MEIO DE FOTOCATÁLISE HETEROGÊNEA COM TiO2 SUPORTADO EM POLÍMEROS / BTEX: DEVELOPMENT OF BARS SORPTIVE EXTRACTION, DETERMINATION IN HOSPITAL EFFLUENT AND DEGRADATION BY HETEROGENEOUS PHOTOCATALYSIS WITH TIO2 SUPPORTED IN POLYMERS.
In this work were developed low cost bars of sorptive extraction, using commercial adhesive based on polydimethylsiloxane (PDMS) for the preconcentration and determination of benzene, toluene, ethylbenzene and xylene (BTEX) in effluent from the University Hospital of Santa Maria (HUSM). It was applied multivariate fractional factorial design (26-2) to invest
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 24/02/2012
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24. Estudos sobre as propriedades catalíticas da frutosiltransferase de Rhodotorula sp. livre e imobilizada em suporte inorgânico / Catalytic properties of fructosyltransferase from Rhodotorula sp., free and immobilized on inorganic support
A obtenção de fruto-oligossacarídeos (FOS), um açúcar prebiótico de vasta aplicação industrial, por enzimas imobilizadas abrange dois conceitos em grande expansão: aplicação industrial de enzimas imobilizadas e alimentos funcionais. A partir de flores da Mata Atlântica Brasileira uma cepa foi isolada e identificada como Rhodotorula sp. LEB-V10 e
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 13/02/2012