Activation Analysis
Mostrando 1-12 de 4907 artigos, teses e dissertações.
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1. Catalytic Effects of Ruthenocene Bimetallic Compounds Derived from Fused Aromatic Ring Ligands on the Main Oxidizing Agent for Solid Rocket Motor
We report the catalytic effect of three ruthenocene bimetallic compounds derived from fused aromatic rings of general formula [{Cp*Ru}2L], with Cp*: pentamethylcyclopentadiene and L = pentalene (1), 2,6-diethyl-4,8-dimethyl-s-indacene (2), and 2,7-diethyl-as-indacene (3), on the thermal decomposition of ammonium perchlorate (AP). The new compound 3 was chara
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Morphology Behavior of Copper Films Deposited after Wet Surface Treatment on Polished Alumina
In this paper, a pre-treatment process for electroless copper (Cu) deposition on the polished alumina (Al2O3) 99.9% and the behavior of Cu plating by electroless process after Al2O3 surface treatment were explored. Our work was carried out by changing the roughness of Al2O3 through micro-etching (coarsening), nucleation its surface by a two-step method (sens
Journal of the Brazilian Chemical Society. Publicado em: 2022
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3. Molecular signature of immunological mechanism behind impaired endometrial receptivity in polycystic ovarian syndrome
ABSTRACT Objective: Despite the treatment of anovulation, infertility is still one of the main complications in PCOS women during reproductive age, which appears to be mainly due to impaired uterine receptivity. This study investigated the transcriptome profiles of endometrium in PCOS patients and healthy fertile individuals as the control group. Material
Archives of Endocrinology and Metabolism. Publicado em: 2022
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4. Association of Anti-β1 and Anti-M2 Antibodies with Autonomic Nervous System Modulation in Patients with Chronic Chagas Cardiomyopathy
Abstract Background: Different immune mechanisms of myocardial damage involved in the pathophysiology of Chagas disease coexist with high titers of autoantibodies induced by T. cruzi . There are few studies in the literature about the adaptive role of anti-β1 and anti-M2 antibodies in chronic Chagas cardiomyopathy (CCC). Objectives: To evaluate the associ
International Journal of Cardiovascular Sciences. Publicado em: 2022
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5. Could serum total cortisol level at admission predict mortality due to coronavirus disease 2019 in the intensive care unit? A prospective study
ABSTRACT BACKGROUND: Critical diseases usually cause hypercortisolemia via activation of the hypothalamic-pituitary-adrenal axis. OBJECTIVES: To investigate the relationship between serum total cortisol level and mortality among coronavirus disease 2019 (COVID-19) patients in the intensive care unit (ICU), at the time of their admission. DESIGN AND SETTIN
Sao Paulo Med. J.. Publicado em: 2021-08
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6. Purification of raw palygorskite: a comparative study involving different processes and dispersing agents
Abstract Palygorskite (Pal) is a natural clay mineral with fibrous morphology and high surface area. Depending on the geological origin, it presents impurities, such as quartz and carbonates, which can harm some of its properties. Therefore, this work seeks to define a viable methodology for the purification of a Brazilian Pal. Two types of mixing processes
Cerâmica. Publicado em: 2021-06
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7. Compatibility by a Nonisothermal Kinetic Study of Azathioprine Associated with Usual Excipients in the Product Quality Review Process
Azathioprine is an immunosuppressive drug for several inflammatory disorders. Due to its clinical relevance, to explore the solid-state properties for excipient compatibility in the product quality review process is essential. Fourier transform infrared spectroscopy, powder X-ray diffraction and thermal analysis (thermogravimetry/derivative thermogravimetry
J. Braz. Chem. Soc.. Publicado em: 2021-03
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8. Influence of sintering parameters on the microstructure and mechanical properties of nanosized 3Y-TZP ceramics
Abstract The fracture toughness of 3Y-TZP ceramics obtained from a nanocrystalline powder with an optimized microstructure and highly transformable tetragonal grains was investigated. Samples of ZrO2-3 mol% Y2O3 were sintered at temperatures between 1250 and 1400 °C, with isothermal holding times of up to 16 h. Samples sintered at 1250 °C exhibited relativ
Cerâmica. Publicado em: 2021-03
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9. Aqueous Extract of Cumaru (Dipteryx odorata) Seeds as Corrosion Inhibitor for Mild Steel in Hydrochloric Acid Solution
The corrosion inhibition of mild steel by aqueous extract of cumaru (Dipteryx odorata) seeds and its high molecular weight fraction (HMWF) was investigated in 1 mol L-1 HCl solution. The study was carried out through gravimetric essays, open circuit potential measurements, anodic and cathodic polarization curves and electrochemical impedance analyses, as wel
J. Braz. Chem. Soc.. Publicado em: 2021-02
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10. Effect of Quiet and Noise on P300 Response in Individuals with Auditory Neuropathy Spectrum Disorder
Abstract Introduction Auditory neuropathy spectrum disorder (ANSD) is a clinical condition in which individuals have normal cochlear responses and abnormal neural responses. There is a lack of evidence in the literature regarding the neural discrimination skill in individuals with ANSD, especially when the signal is presented in the presence of noise. Obje
Int. Arch. Otorhinolaryngol.. Publicado em: 2020-12
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11. Sunlight-Driven Dehydrogenative Oxidation Photocatalysis by a Mononuclear Complex Acting as both Chromophore and Catalyst
Under simulated solar irradiation in the visible spectral region, the catalytically active RuIV-oxo species [Ru(O)(bpy)(tppz)]2+ (tppz = tetrapyridylpyrazine, a strongly π-accepting tridentate N, N, N-ligand) is produced directly from a single metal-to-ligand charge-transfer (MLCT) photoexcitation of the resting RuII-aquo complex [Ru(H2O)(bpy)(tppz)]2+ in a
J. Braz. Chem. Soc.. Publicado em: 2020-11
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12. Is it still worth Publishing Case Reports? They are Part of our Lives
Partially hydrogenated soybean oil and palm olein are oils that are widely used in the food industry. Continuous contact with air may cause changes of the triglycerides chemical structure, to eventually produce substances of lower molar masses that may be toxic to mammals. This study aimed to determine the kinetic parameters for the thermal oxidation of thes
Braz. J. Cardiovasc. Surg.. Publicado em: 2020-10