Water Ethanol
Mostrando 1-12 de 579 artigos, teses e dissertações.
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1. New Europium(III)-TTA Complex Containing 2-Pyrrolidone as Coligand to Application as Luminescent Sensor: PbII and Ethanol in Gasoline
This work describes the synthesis and application of an europium(III) complex, [Eu(TTA)3(2-pyr) (H2O)], containing 2-thenoyltrifuoroacetonate (TTA) and 2-pyrrolidone (2-pyr) as ligands, obtained as white solid and soluble in ethanol. In solution, the complex showed red emission, characteristic of the EuIII emission in the solid state (λexc = 375 nm and λem
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Determinação de etil-glicuronídeo e etil-sulfato em sangue por UPLC-MS/MS: aplicação clínica em vítimas de trauma
We developed a UPLC-MS/MS method for the quantification of the ethanol metabolites ethyl-glucuronide (EtG) and ethyl-sulfate (EtS) in blood samples. Sample preparation was a protein precipitation with acetonitrile 0.1% formic acid containing internal standards (IS) 0.5 µg mL-1 EtG-D5 and EtS-D5. Chromatographic separation was performed in a fluoro-phenyl co
Química Nova. Publicado em: 2022
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3. Optimization of ultrasound-assisted extraction of turkish propolis and characterization of phenolic profile, antioxidant and antimicrobial activity
Abstract This study aimed to determine optimum conditions of the ultrasound assited extraction (UAS) parameters for different solvent types by using response surface methodology (RSM) and Box- Behnken design. The model parameters namely, time, temperature and ultrasound power significantly affected TPC value of the propolis extract (P < 0.05). The optimum pr
Food Sci. Technol. Publicado em: 2021-09
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4. Fundamental bioflotation aspects of hematite using an extracted Rhodococcus opacus by-product
Abstract The aim of this study is to assess the floatability of hematite using a crude biosurfactant (BS) extracted from Rhodococcus opacus. Throughout high-pressure ethanol extraction, unrefined surfactant was extracted from the bacteria with a yield of 0.3 g/L. An FTIR analysis on this extract, shows the presence of alcohol (–OH) and ketone (C=O) groups,
REM, Int. Eng. J.. Publicado em: 2021-09
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5. Structural Study of Wheat Gliadin in Different Solvents by Spectroscopic Techniques
Physicochemical properties of gliadin in different solvents (dimethyl sulfoxide (DMSO), H2O, and aqueous ethanol) and pH (9.8, 6.8, and 1.2) were investigated using dynamic light scattering (DLS), zeta potential (ZP), and attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR). Gliadin-DMSO and gliadin-deionized water (H2O) (pH 9.8) s
J. Braz. Chem. Soc.. Publicado em: 2021-04
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6. Evaluation of Antibacterial Activity, Chromatographic Analysis for Rutin and Quercetin Quantification Using HPLC-UV-Vis from the Hydro-Alcoholic Extract Obtained from Bidens pilosa Linné
Novel and miniaturized technique, a dynamic sonication-assisted solvent extraction before the analysis by high performance liquid chromatography-ultraviolet visible (HPLC-UV-Vis) for isolation, identification and quantification of rutin and quercetin metabolites in alcoholic extracts from Bidens pilosa Linné, was developed. The results showed that the flowe
J. Braz. Chem. Soc.. Publicado em: 2021-03
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7. Improving composition and microbiological characteristics of milk kefir using colostrum
Abstract Kefir characteristics are influenced by raw materials. Fresh milk and colostrum have different characteristics. In this research, colostrum was used as additional material in kefir production which could affect the chemical, microbiological, and antimicrobial properties of final the product. This study was aimed to investigate the chemical and micro
Food Sci. Technol. Publicado em: 2020-12
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8. Synthesis and Antioxidant and Antimicrobial Properties of β-Hydroxy Sulfides, Sulfoxides, and Sulfones Derived from Cardanol and Glycerol Derivatives
Natural and synthetic sulfur-bearing organic compounds have many applications in medicinal chemistry. This article reports the preparation of amphiphilic β-hydroxy sulfides, sulfoxides, and sulfones derived from cardanol and glycerol. Thiolysis of cardanol epoxide 3 with various thiols (4a-4j) in ethanol or water yielded the corresponding β-hydroxy sulfide
J. Braz. Chem. Soc.. Publicado em: 2020-12
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9. Development of diet cereal bar sweetened with stevia leaves pre-treated with ethanol
Abstract The objective of this work was to perform the ethanolic pretreatment of stevia leaves from the plant Stevia UEM-13 line and to characterize its physical-chemical properties aiming its use as a sweetener in the development of a diet cereal bar. The same formulation of the cereal bar with stevia leaves without pretreatment was elaborated for comparati
Food Sci. Technol. Publicado em: 2020-12
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10. Self-Assembled Nanoparticles of Diruthenium(II,III)-Ibuprofen Anticancer Metallodrug
The diruthenium(II,III)-ibuprofen (RuIbp) metallodrug shows anticancer activity in vitro and in vivo. The encapsulation into lipid nanoparticles enhanced the efficacy in glioblastoma, breast and prostate cancer cells. Here we report data for RuIbp hydrophobicity, solubility in alcohol/water, and behavior in 1-5% ethanol/water and ethanol/cell culture medium.
J. Braz. Chem. Soc.. Publicado em: 2020-11
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11. HPLC METHOD IMPROVEMENT FOR 4-NONYLPHENOL DETERMINATION IN ANAEROBIC REACTORS: DECREASING SOLVENT CONSUMPTION AND WASTE GENERATION
The aim of this study was to develop a chromatographic method for 4-NP determination in anaerobic batch reactors using low amount of organic solvents and also evaluate 4-NP degradation in the presence of different co-substrates. Chromatographic parameters was improved for stationary phase (C-8 column), mobile phase (acetonitrile/water solution 90:10, v:v), c
Quím. Nova. Publicado em: 2020-09
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12. Determination of Methanol in Gasoline and Ethanol Fuels by High-Performance Liquid Chromatography
Gasoline and ethanol fuels have been adulterated with methanol in Brazil. Methanol is not permitted in concentrations greater than 0.5 vol% due its toxicity but its lower price stimulates the adulteration. A new approach for quantitative analysis of methanol in gasoline and ethanol fuels is reported employing high-performance liquid chromatography coupled wi
J. Braz. Chem. Soc.. Publicado em: 2020-05