Simultaneous Analysis
Mostrando 1-12 de 1029 artigos, teses e dissertações.
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1. AN ADAPTED UNMANNED AERIAL VEHICLE FOR ENVIRONMENTAL WATER SAMPLING
In this work an unmanned aerial vehicle (UAV) was adapted to be used as an environmental tool to collect water samples of sea, estuary, and mangrove for further analysis by gas chromatography with a mass detector (GC-MS). The sampling automated system was based on a microcontroller, a solenoid valve, and a peristaltic mini-pump that was coupled to a quadcopt
Química Nova. Publicado em: 2022
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2. Idiopathic musculoskeletal pain, musculoskeletal pain syndromes, and use of electronic devices in adolescents with asthma
Abstract Objective: To evaluate idiopathic musculoskeletal pain, musculoskeletal pain syndromes, and use of electronic devices in adolescents with asthma and healthy controls. Methods: Cross-sectional study was conducted on 150 asthmatic adolescents and 300 controls. Adolescents completed a self-administered questionnaire regarding painful symptoms, use of
Jornal de Pediatria. Publicado em: 2022
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3. Biphasic 0.8BaTiO3/0.2Ni(1-x)CoxFe2O4 nanopowders by in situ sol-gel synthesis
Abstract Nanopowders of the 0.8BaTiO3/0.2Ni(1-x)CoxFe2O4 (x=0, 0.25, 0.5, 0.75, and 1) were synthesized by the in situ sol-gel method using poly(acrylic acid) (PAA1800) as a chelating agent. The synthesis developed using PAA1800 ensured the simultaneous crystallization of two phases. The results provided a reliable method for producing biphasic nanopowders i
Cerâmica. Publicado em: 2022
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4. Simultaneous GC-NCI-MS Determination of Persistent Organic Pollutants and Current-Use Pesticides in Breast Milk Samples
To preserve human health, persistent organic pollutants (POPs) and current-use pesticides (CUPs) should be monitored in fatty tissues, including breast milk. Therefore, this study aimed to optimize sample preparation conditions using a 32 factorial design for the determination of POPs and CUPs by gas chromatography coupled to mass spectrometry with negative
Journal of the Brazilian Chemical Society. Publicado em: 2022
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5. Development of a Simple and Fast Procedure Based on Acid Dilution for Determination of Macro and Microelements in Guarana-Based Beverages by ICP OES
A simple analytical procedure is proposed for the direct analysis of guarana-based beverages in order to determine nutrient elements by inductively coupled plasma optical emission spectrometry (ICP OES). A Box-Behnken design, combined with Derringer’s desirability function, was applied to the simultaneous optimization of the ICP OES radiofrequency (RF), sa
J. Braz. Chem. Soc.. Publicado em: 2021-07
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6. Development and Validation of a Gas Chromatographic Method for the Quantification of Minor Alkaloids in Cocaine
The quantification of minor alkaloids in seized cocaine can provide information for drug profiling and law enforcement initiatives. This work presents the development and validation of an analytical method to quantitate minor alkaloids in cocaine samples using gas chromatography with flame ionization detector, after derivatization. The method was validated i
J. Braz. Chem. Soc.. Publicado em: 2021-04
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7. The association of seminal oxidation reduction potential with sperm parameters in patients with unexplained and male factor ınfertility
ABSTRACT Purpose: Understanding the effects of high oxidation reduction potential (ORP) levels on sperm parameters will help to identify patients with unexplained and male factor infertility who may have seminal oxidative stress and determine if ORP testing is needed. This study aimed to evaluate the association between seminal ORP and conventional sperm pa
Int. braz j urol.. Publicado em: 2021-02
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8. Selection of best videos of the year for 2020
ABSTRACT Purpose: Understanding the effects of high oxidation reduction potential (ORP) levels on sperm parameters will help to identify patients with unexplained and male factor infertility who may have seminal oxidative stress and determine if ORP testing is needed. This study aimed to evaluate the association between seminal ORP and conventional sperm pa
Int. braz j urol.. Publicado em: 2021-02
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9. Editorial Comment: Endoclips as novel fiducial markers in trimodality bladder preserving therapy of muscle-invasive bladder carcinoma: feasibility and patient outcomes
ABSTRACT Purpose: Understanding the effects of high oxidation reduction potential (ORP) levels on sperm parameters will help to identify patients with unexplained and male factor infertility who may have seminal oxidative stress and determine if ORP testing is needed. This study aimed to evaluate the association between seminal ORP and conventional sperm pa
Int. braz j urol.. Publicado em: 2021-02
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10. Reordering of Depolymerized Silicates as Adsorbents for Large Nitrogen Compounds
The adsorption capacities of two synthesized zeolites (crystalline ZSM-5 and semi-crystalline faujasite Y) for a mixture of indole, quinoline and carbazole were studied. The different samples obtained show different crystalline degree, mesoporosity and Si/Al ratios. The synthesis procedure is based on the simultaneous depolymerization of a mixture of high su
J. Braz. Chem. Soc.. Publicado em: 2021-01
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11. Bilateral simultaneous percutaneous nephrolithotomy versus staged approach: a critical analysis of complications and renal function
RESUMO INTRODUÇÃO: Paciente com cálculos renais bilaterais e de grande volume são casos desafiadores para os endourologistas. A nefrolitotripsia percutânea bilateral simultânea (NLPbs) é um opção, entretanto esse procedimento pode ser acompanhado de morbidade importante. Uma alternativa é a NLP estagiada, operando um lado de cada vez. Aqui, nós c
Rev. Assoc. Med. Bras.. Publicado em: 2020-12
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12. Electroanalytical Method for Determination of Trace Metals in Struvite Using Electrochemically Treated Screen-Printed Gold Electrodes
We present an electroanalytical method using square-wave anodic stripping voltammetry on electrochemically-treated screen-printed gold electrodes to the simultaneous determination of lead(II), copper(II) and mercury(II) in struvite (natural fertilizer produced from urine). Electrochemical treatment via cyclic voltammetry of the working electrodes increased s
J. Braz. Chem. Soc.. Publicado em: 2020-09