Saxs Small Angle X Ray Scattering
Mostrando 13-24 de 57 artigos, teses e dissertações.
-
13. Solution properties of a hydrophobically associating polyacrylamide and its polyelectrolyte derivatives determined by light scattering, small angle x-ray scattering and viscometry
Uma poliacrilamida hidrofobicamente modificada e dois dos seus derivados parcialmente hidrolisados, contendo grupos hidrofóbicos e carboxila, foram preparados por polimerização micelar e pós-hidrólise. A massa molar, o segundo coeficiente do virial e o raio de giração foram determinados por espalhamento de luz estático (SLS). O espalhamento de luz di
Journal of the Brazilian Chemical Society. Publicado em: 2011-03
-
14. Caracterização de três fatores de transcrição pertencentes à família LysR de Xylella fastidiosa / Characterization of three LysR type transcriptional factor from Xylella fastidiosa
Após o sequenciamento do genoma da Xylella fastidiosa, linhagem 9a5c houve um grande aumento de informações relacionadas a este organismo. Porém grande parte das proteínas desta bactéria ainda não apresentam funções preditas. No presente estudo, objetivou-se a caracterização inicial de três proteínas deste micro-organismo, a saber: XfCysB (orf X
Publicado em: 2011
-
15. Porous biodegradable polyurethane nanocomposites: preparation, characterization, and biocompatibility tests
A porous biodegradable polyurethane nanocomposite based on poly(caprolactone) (PCL) and nanocomponents derived from montmorillonite (Cloisite®30B) was synthesized and tested to produce information regarding its potential use as a scaffold for tissue engineering. Structural and morphological characteristics of this nanocomposite were studied by infrared spec
Materials Research. Publicado em: 2010-06
-
16. Estudos de macromoleculas biologicas parcialmente desestruturadas usando espalhamento de raios-X / Study of partially unstructured macromolecules using X-ray scattering
As técnicas de caracterização estrutural de macromoléculas tradicionais se baseiam no fato de uma macromolécula possuir uma conformação compacta e estruturada. Partes flexíveis ou regiões desordenadas têm sido sempre consideradas como grandes obstáculos para técnicas como a cristalografia de raios-X e a ressonância magnética nuclear (RMN). A ne
Publicado em: 2010
-
17. Estudo sobre o hidróxido de potássio no processo de produção industrial de poliol poliéter
Metallic ions may interact with polyether polyols giving macromolecular complexes. From this approach, it was investigated the interaction of cationic potassium with polyether polyols by means of several techniques in order to proof complexation as well as its ocurrence. The industrial synthesis of polyether polyols does not result in a pure product but give
Publicado em: 2010
-
18. Síntese e caracterizção eletroquímica de membranas híbridas Nafion-SIO2 para a aplicação como eletrólito polimérico em células a combustível tipo PEM / Synthesis and electrochemical characterization of hybrid membrane nafion-SiO2 for application as polymer electrolyte in PEM fuel cell
In this work, the effect of sol-gel synthesis parameters on the preparation and polarization response of Nafion-SiO2 hybrids as electrolytes for proton exchange membrane fuel cells (PEMFC) operating at high temperatures (130 oC) was evaluated. The inorganic phase was incorporated in a Nafion matrix with the following purposes: to improve the Nafion water upt
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 23/11/2009
-
19. Repulsive and attractive ferroglasses: a SAXS and XPCS study
A dynamical freezing, which is the analogous of a glass transition, is observed at large concentrations in aqueous dispersions of maghemite nanoparticles. We study experimentally the structure and the dynamical properties of two dense ferroglass-formers in two very distinct states of interparticle interaction, either strongly repulsive or attractive. The sta
Brazilian Journal of Physics. Publicado em: 2009-04
-
20. Gravitational and magnetic separation in self-assembled clay-ferrofluid nanocomposites
We report on experimental observations of self-assemblies in colloidal dispersions of clay nanoplatelets and magnetic nanoparticles. Visual observations have been combined with small angle X-ray scattering (SAXS) in the study of several composites at a fixed clay concentration in the dilute regime, and varying ferrofluid concentrations. Our visual observatio
Brazilian Journal of Physics. Publicado em: 2009-04
-
21. Characterization and application of thin film of carboxymehtylcellulose acetate butyrate / Caracterização e aplicação de filmes finos de acetato butirato carboximetil celulose
The effect of ethyl acetate and acetone on the solution behavior of cellulose acetate butyrate (CAB) and carboxymehtylcellulose acetate butyrate (CMCAB) and on the characteristics of films obtained either by spin coating or adsorption was investigated. Viscosity and small angle X-ray scattering (SAXS) measurements showed that ethyl acetate is a better solven
Publicado em: 2009
-
22. Equilíbrio líquido-líquido de sistemas aquosos constituídos por copolímero tribloco e sal em diferentes temperaturas / Liquid-liquid equilibrium of aqueous systems consisting of triblock copolymer and salt at different temperatures
Phases diagrams of aqueous biphasic systems (ABS) formed by triblock copolymer+salt+H2O were construed at three temperatures: The ABS L64+Na2SO4+H2O and L64+Li2SO4+H2O at 5, 10 and 25 C and ABS L35+Na2CO3+H2O, F68+Na3C6H5O7+H2O, F68+Na2C4H4O6+H2O, F68+Na2CO3+H2O and F68+Na2C4H4O4+H2O at 10, 25 and 40 C. The effect of temperature on the position of the binoda
Publicado em: 2009
-
23. Protein decorated Nanoparticules : Small Unilamellar Lipid Vesicules and Block Copolymers Micelles. / Nanoparticules Décorées par des Protéines : Vésicules Lipidiques Unilamellaires et Micelies à Base de Copolymères à Blocs
The formation of protein Annexin-A5 decorated (bio-functionalized) nanoparticles is of particular interest in micelle-mediated target drug delivery, in vivo magnetic resonance imaging, or controlled fabrication of biochips. This work describes an easy access to the synthesis and manipulation of block copolymer nano-objects exhibiting binding ability for the
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 03/07/2008
-
24. Espalhamento de raios-X a baixo ângulo aplicado ao estudo estrutural de proteínas / Small Angle X ray Scattering applied to protein characterization studies
Small angle X-ray scattering has been proven to be a powerful tool in the structural analysis of proteins in solution. This technique permits the three-dimensional visualization of native proteins envelop at the level of nanometers. In this study we discuss the small angle X-ray scattering theory and we proposed a new methodology to determine the molecular w
Publicado em: 2008