Ms Exchange
Mostrando 1-12 de 149 artigos, teses e dissertações.
-
1. Structural Study of Phenolic Acids by Triple Quadrupole Mass Spectrometry with Electrospray Ionization in Negative Mode and H/D Isotopic Exchange
This work reports the theoretical and experimental study of fragmentation reactions in the gas phase of five phenolic acids using triple quadrupole mass spectrometry by electrospray ionization in negative ionic mode, as well as the isotope exchange experiments. MS/MS spectra were analyzed to suggest the fragmentation mechanisms, while theoretical calculation
J. Braz. Chem. Soc.. Publicado em: 2020-02
-
2. Development and Validation of a UPLC-ESI-MS Method for Quantitation of the Anti-Alzheimer Drug Galantamine and other Amaryllidaceae Alkaloids in Plants
Our study aimed at the development of a method based on ultra-performance liquid chromatography coupled to mass spectrometry (UPLC-ESI-MS) using selected ion monitoring for the simultaneous quantitation of the alkaloids galantamine, pseudolycorine, sanguinine and narciclasine in Amaryllidaceae species (Hippeastrum elegans, Habranthus cf. irwinianus, Hymenoca
J. Braz. Chem. Soc.. Publicado em: 2020-02
-
3. Não linearidade entre câmbio e preços no Brasil e implicações para uma estratégia de desenvolvimento econômico
RESUMO O objetivo deste artigo é realizar uma análise da política monetária no Brasil a partir de um modelo de Vetores Autorregressivos com Cadeias de Markov (MS-VAR), na busca de evidências da não linearidade da relação entre câmbio e preços no Brasil. A análise demonstrou que, em períodos de apreciação cambial, tanto pelo lado da demanda quan
Brazil. J. Polit. Econ.. Publicado em: 02/05/2019
-
4. Análise do fluxo de água virtual: uma abordagem a partir da balança comercial de Mato Grosso do Sul
Resumo: A alocação dos recursos hídricos tem despertado a atenção dos mais diversos segmentos da sociedade moderna. Geralmente, em regiões caracterizadas pela agropecuária, como é o caso do estado de Mato Grosso do Sul (MS), o uso da água no processo de produção se torna mais intensivo, de forma a refletir na utilização dos recursos naturais. A
Interações (Campo Grande). Publicado em: 08/04/2019
-
5. Structural, Morphological and Magnetic Properties of FeCo-(Fe,Co)3O4 Nanocomposite Synthesized by Proteic Sol-Gel Method Using a Rotary Oven
FeCo nanoparticles coated with (Fe,Co)3O4 (magnetite doped with cobalt) were synthesized by the proteic sol-gel chemical route. The synthesized materials were characterized by Thermogravimetry (TG), X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), vibrating-sample magnetometer (VSM) and Mössbauer spectrosc
Mat. Res.. Publicado em: 18/03/2019
-
6. Arsenic Speciation in Fish and Rice by HPLC-ICP-MS Using Salt Gradient Elution
This paper presents arsenic speciation studies by high-performance liquid chromatography with inductively coupled plasma-mass spectrometer (HPLC-ICP-MS) using a chromatography column containing a strong anion exchange stationary phase (Agilent Bio SAX G3154A/101) for determination of arsenobetaine (AsB), dimethylarsinic acid (DMA), AsIII, monomethylarsonic a
J. Braz. Chem. Soc.. Publicado em: 2018-08
-
7. Actiflagelin, a new sperm activator isolated from Walterinnesia aegyptia venom using phenotypic screening
Abstract Background Sperm contains a wealth of cell surface receptors and ion channels that are required for most of its basic functions such as motility and acrosome reaction. Conversely, animal venoms are enriched in bioactive compounds that primarily target those ion channels and cell surface receptors. We hypothesized, therefore, that animal venoms shou
J. Venom. Anim. Toxins incl. Trop. Dis. Publicado em: 22/02/2018
-
8. Polysaccharide rich fractions from barks of Ximenia americana inhibit peripheral inflammatory nociception in mice Antinociceptive effect of Ximenia americana polysaccharide rich fractions
Abstract Ximenia americana L., Olacaceae, barks are utilized in folk medicine as analgesic and anti-inflammatory. The objective was to evaluate the toxicity and antinociceptive effect of polysaccharides rich fractions from X. americana barks. The fractions were obtained by extraction with NaOH, followed by precipitation with ethanol and fractionation by ion
Rev. bras. farmacogn.. Publicado em: 2017-06
-
9. Ion Exchange Chromatography and Mass Bias Correction for Accurate and Precise Zn Isotope Ratio Measurements in Environmental Reference Materials by MC-ICP-MS
Precise and accurate d66/64Zn data for environmental reference materials (RMs) including rocks, sediments, soils and plants are presented in order to improve the metrological traceability and analytical control of Zn isotope ratio determinations in future environmental studies. Previously developed ion exchange chromatography protocols were adjusted to enabl
J. Braz. Chem. Soc.. Publicado em: 2017-02
-
10. Successive Cultivation of Soybean/Corn Intercropped with Urochloa brizantha topdressed with Nitrogen
ABSTRACT Corn intercropped with Urochloa brizantha (Syn, Brachiaria brizantha) has been indicated as a suitable alternative management practice for rational land use in crop-livestock production systems in the Cerrado region of Brazil. An experiment was carried out in Maracaju, MS, Brazil to evaluate the effect of sequences of soybean/second-crop corn system
Rev. Bras. Ciênc. Solo. Publicado em: 29/08/2016
-
11. Determination of Boron Isotope Ratios in Tooth Enamel by Inductively Coupled Plasma Mass Spectrometry (ICP-MS) After Matrix Separation by Ion Exchange Chromatography
Boron isotopes in teeth has been a new proxy for dietary reconstructions and its resistance to diagenetic alteration. In this study a method using inductively coupled plasma source mass spectrometry (ICP-MS) for the measurement of boron isotope ratio in human dental enamel has been developed. Human dental enamel were digested with HNO3-H2O2 in a microwave sy
J. Braz. Chem. Soc.. Publicado em: 2015-05
-
12. Valor nutricional do feno de Brachiaria decumbens em três idades
Brachiaria decumbens forage is one well adapted to climate and soil conditions in Brazil, but focuses much of its dry matter production at certain times of year. The making hay of this plant enables supplementation of livestock during seasonal scarcity of fodder. The objective was to evaluate the nutritive value of Brachiaria decumbens hay cut at ages 56, 84
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 16/12/2011