Icpms
Mostrando 13-24 de 238 artigos, teses e dissertações.
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13. Halogen Determination in Polymeric Waste of Electrical and Electronic Equipment: Overcoming Limitations in Sample Preparation
Sample preparation of polymers for halogen determination requires special attention because they are difficult to bring into solution and due to the risk of analyte losses when using acid digestion. A method using microwave-induced combustion (MIC) was optimized for accurate determination of halogens in polymeric parts obtained in waste of electrical and ele
J. Braz. Chem. Soc.. Publicado em: 24/10/2019
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14. AVALIAÇÃO DE COMPOSTOS BIOATIVOS E ATIVIDADE ANTIOXIDANTE DE EXTRATOS DE FOLHAS DE AMOREIRA PRETA (Morus nigra L.) UTILIZANDO PLANEJAMENTO EXPERIMENTAL
Extracts of black mulberry leaves present phytochemicals such as phenolic compounds and minerals. These substances have been studied because they show several health benefits. In this work we report the influence of drying temperature, infusion temperature and extraction time by means of factorial design monitoring the total phenolic content (CFT) of aqueous
Quím. Nova. Publicado em: 26/08/2019
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15. Structural and mineralochemical characterization of a pegmatite deposit in the Santa Rosa Pegmatite Field, Minas Gerais Brazil
Abstract The Santa Rosa Pegmatite Field (SRPF), in northeastern Minas Gerais State, is one of the most important gemstone sources in Brazil. The economy of several neighboring cities greatly relies on the trade of its gemstones. However, efforts to improve gemstone mining with practical, scientific methods are scarce, making it a yet inexpensive, marginally
REM, Int. Eng. J.. Publicado em: 19/06/2019
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16. Automatized Separation of Fractions from Petroleum Based on Spectrophotometric Signal Derivative Using Open-Source Hardware for the Determination of Ni and V Linked to Porphyrins
An automated method based on open-source hardware was created for the separation of porphyrins fractions from crude oil, an essential step for the quantification of V and Ni as metalloporphyrins. Preparative liquid chromatography was implemented with a reverse phase gradient from MeOH to toluene. The system allows three solvents and fractions changes by usin
J. Braz. Chem. Soc.. Publicado em: 23/05/2019
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17. Metal Contents and Pb Isotopes in the Surface Seawater of the Gulf of Prigi, Indonesia: Detection of Anthropogenic and Natural Sources
In order to investigate the anthropogenic and natural sources of metals in the Gulf of Prigi, Indonesia, it was analyzed their metal contents and Pb isotopes of surface seawater together with sediment, grouper fish, mosh, seaweed, soil, and sharp grass for protecting the environmental pollution of the study area. Samples were leached using a microwave digest
J. Braz. Chem. Soc.. Publicado em: 08/04/2019
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18. Biomonitoring of Toxic Elements in Plants Collected Near Leather Tanning Industry
The present work aimed the study of atmospheric deposition of toxic elements near to a tannery industry by collecting black material deposited on leaf surfaces of cinnamon trees (Cinnamomum zeylanicum). Elements such as As, Ba, Cr, Cu, Fe, Ni, Pb, Sb, V, and Zn were analyzed by inductively coupled plasma mass spectrometry (ICP-MS). For comparison purpose, bl
J. Braz. Chem. Soc.. Publicado em: 2019-02
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19. PRÉ-CONCENTRAÇÃO BASEADA NA COPRECIPITAÇÃO USANDO CROMATO DE PRATA COMO CARREADOR PARA DETERMINAÇÃO DE COBRE POR FAAS
In the present paper, a preconcentration procedure based in the coprecipitation of copper by silver dichromate (Ag2CrO4) and consecutive determination by flame atomic absorption spectrometry (FAAS) was proposed. The experimental factors were optimized from application of the Doehlert matrix and the conditions set: chromate concentration 5.8 × 10-4 mol L-1,
Quím. Nova. Publicado em: 2019-01
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20. Heavy Metal Bioaccumulation in Enteromorpha intestinalis, (L.) Nees, a Macrophytic Algae: The Example of Kadin Creek (Western Anatolia)
ABSTRACT This study aims to specify the amount of ten heavy metals (Al, Cr, Mn, Ni, Cu, Zn, As, Cd, Hg, Pb) in water, sediment and Enteromorpha intestinalis samples gathered from Kadin Creek in seasonal periods in 2011 and 2012 and to reveal bioaccumulation capability of this macrophytic algae. In this regard, heavy metal concentrations in the gathered sampl
Braz. arch. biol. technol.. Publicado em: 29/10/2018
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21. Elementos essenciais, teores de óleo e proteína de híbridos de girassol cultivados no Brasil
Resumo No presente trabalho, foram determinados os elementos minerais, os teores de óleo e proteína de 13 híbridos de girassol. Além disso, foi avaliada a possibilidade de se obterem, conjuntamente, produtos com alta produtividade e altos teores de óleo e proteína. A pesquisa mostrou alta produtividade de aquênios, excedendo a média nacional, princi
Braz. J. Food Technol.. Publicado em: 06/09/2018
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22. Evaluation of metals in tomato sauces stored in different types of packaging
Abstract There is a growing concern about health and food safety when it comes to processed food. In the present study, it has been hypothesized that tomato sauces contain high amounts of metals possibly leached from packaging. Concentrations of As, Cd, Pb, Cr, Ni, Sn and Sb were determined by ICP-MS in tomato sauces stored in metallic, plastic, cellulosic
Food Sci. Technol. Publicado em: 26/07/2018
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23. Fit-for-Purpose ICP-MS Procedure Supporting Brazilian Regulations on Inorganic Constituents in Fresh and Saline Waters
This work aimed the development of an analytical procedure using inductively coupled plasma mass spectrometry (ICP-MS) in four modes of operation for simple and fast determination of Al, Ag, As, B, Ba, Be, Ca, Cd, Co, Cr, Cu, Fe, Li, Mg, Mn, Na, Ni, Pb, Sb, Se, Tl, Hg, V, U, and Zn in fresh and sea water samples attending simultaneously four Brazilian regula
J. Braz. Chem. Soc.. Publicado em: 2018-07
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24. Discrimination of habitat use between two sympatric species of mullets, Mugil curema and Mugil liza (Mugiliformes: Mugilidae) in the rio Tramandaí Estuary, determined by otolith chemistry
RESUMO Duas espécies de tainha simpátricas, Mugil curema e M. liza, usam o estuário do Rio Tramandaí como zona de berçário. Quando espécies do mesmo gênero são simpátricas, vários mecanismos podem permitir sua coexistência, incluindo segregação espacial ou temporal que resultam no uso distinto dos recursos pelos quais elas competem. Para invest
Neotrop. ichthyol.. Publicado em: 11/06/2018