Flow Injection Analysis
Mostrando 1-12 de 193 artigos, teses e dissertações.
-
1. SEQUENTIAL MULTI-ELEMENT DETERMINATION OF TRACE-METALS IN BIODIESEL SAMPLES USING HR-CS FAAS
In this work the feasibility of sequential multi-element determination of Zn, Fe, Mg, Cu, Na, K, Cr, Al and Ca in biodiesel samples by high-resolution continuum source flame atomic absorption spectrometry (HR-CS FAAS) was investigated. Biodiesel samples obtained from different sources and different chemical processes were analysed. The samples were diluted w
Quím. Nova. Publicado em: 2021-02
-
2. Synthesis, Characterization, Spectroelectrochemical, Photophysical and HSA-Binding Properties of Novel and Versatile meso-Tetra(4-pyridylvinylphenyl)porphyrins Coordinated to Ruthenium(II)-Polypyridyl Derivatives
The free-base meso-tetra(4-pyridylvinylphenyl)porphyrin (1a) and its zinc(II) complex were synthesized and then functionalized with [Ru(bpy)2Cl]+ units (2a and 2b) via conventional methods and evaluated in terms of photophysical, electrochemical and biological aspects. All porphyrins present moderate singlet oxygen production and fluorescence quantum yield,
J. Braz. Chem. Soc.. Publicado em: 2020-11
-
3. An augmented patient-specific approach to administration of contrast agent for CT renal angiography
ABSTRACT Purpose This hybrid retrospective and prospective study performed on 200 consecutive patients undergoing renal CTA, investigates the opacification of renal vasculature, radiation dose, and reader confidence. Materials and Methods 100 patients were assigned retrospectively to protocol A and the other 100 were allocated prospectively to protocol B
Int. braz j urol.. Publicado em: 07/11/2019
-
4. Estudo da substituição do nylon por compósito de polipropileno com fibra de vidro
RESUMO Peças fabricadas com polímeros de alto desempenho têm sido substituídas por materiais similares, sendo produzidas com uma composição de polipropileno (PP), que tem um custo mais baixo. Uma das composições mais comumente utilizadas é a junção do polipropileno com fibras, resultando na formação de um novo material, com características dife
Matéria (Rio J.). Publicado em: 16/09/2019
-
5. Characterization of venturi injector using dimensional analysis
RESUMO Injetores Venturi são comumente empregados para fins de fertirrigação na agricultura, extraindo fertilizante de um tanque para a linha de irrigação. O conhecimento da quantidade de líquido a ser injetado por este dispositivo é útil para assegurar operação e manejo adequados da fertirrigação. Os objetivos desta pesquisa foram: (1) conduzir
Rev. bras. eng. agríc. ambient.. Publicado em: 10/07/2019
-
6. Comportamento hidrodinâmico de sistemas alagados construídos de escoamento horizontal subsuperficial de diferentes proporções geométricas e tempos de operação
RESUMO No presente trabalho, teve-se por objetivo avaliar a influência da proporção geométrica e o tempo de operação na hidrodinâmica do sistema. Para isso, três sistemas alagados construídos de escoamento horizontal subsuperficial (SACs-EHSS) de diferentes razões comprimento:largura (L/B) foram caracterizados no que se refere ao comportamento hidr
Eng. Sanit. Ambient.. Publicado em: 25/04/2019
-
7. Investigation on Ruthenium(II) Bipyridine/AgIII Complexes Chemiluminescence System and Its Application for Sensitive Norfloxacin and Ofloxacin Detection
The reaction mechanism of AgIII complex ([Ag(HIO6)2]5–) with ruthenium(II) bipyridine (Ru(bpy)32+) in acid medium was investigated. A novel flow injection chemiluminescence (CL) analysis method was developed for the detection of norfloxacin (NFLX) and ofloxacin (OFLX) in commercial drug, milk and human urine samples based on AgIII-ruthenium(II) bipyridine
J. Braz. Chem. Soc.. Publicado em: 2019-04
-
8. Design and analysis of different models of microfluidic devices evaluated in Enhanced Oil Recovery (EOR) assays
ABSTRACT Microfluidic devices are a new platform for Enhanced Oil Recovery (EOR) assays. The application of Colloidad Dispersion Gels (CDG) injection method has been proposed in recent years. However, the mechanism of oil recovery enhancement has not been completely elucidated. Its purpose is to mobilize oil by decreasing the permeability of channeled zones.
Matéria (Rio J.). Publicado em: 19/07/2018
-
9. An Environmental Friendly Flow-Injection Procedure for On Line Extraction and Spectrophotometric Determination of Gossypol in Cottonseed Meal
A fast, simple and inexpensive procedure is described for the determination of gossypol in cottonseed meal. The procedure is based on a flow injection analysis system and a complexation reaction with spectrophotometric detection at 620 nm. A fluidized bed column was used to implement the on line that was coupled to the extraction flow system in order to anal
J. Braz. Chem. Soc.. Publicado em: 2017-11
-
10. DETERMINAÇÃO RÁPIDA E SIMPLES DE CITRATO DE SILDENAFILA (VIAGRA® E GENÉRICOS) EMPREGANDO ELETRODO IMPRESSO DE CARBONO EM SISTEMAS FIA E BIA COM DETECÇÃO AMPEROMÉTRICA
This work presents two amperometric methods for Sildenafil Citrate (SC) determination in erectile dysfunction drugs (Viagra® and Generics), using Batch Injection Analysis (BIA) and Flow Injection Analysis (FIA) systems with a cell for Screen Printed Electrodes (SPE). In Britton- Robinson buffer solution (pH 2), the SC presented an irreversible anodic peak a
Quím. Nova. Publicado em: 2017-08
-
11. Solid Phase Extraction to On-Line Preconcentrate Trace Cadmium Using Chemically Modified Nano-Carbon Black with 3-Mercaptopropyltrimethoxysilane
Carbon black (CB) grafted with 3-mercaptopropyltrimethoxysilane (3-MPTMS) was used as solid phase extractor for Cd2+ in a flow injection system coupled to flame atomic absorption spectrometry (FAAS). The influence of pH, buffer concentration, preconcentration flow rate and eluent concentration on preconcentration of Cd2+ were investigated by means of chemome
J. Braz. Chem. Soc.. Publicado em: 2016-10
-
12. Stability-indicating RP-LC method for quantification of fusidic acid in cream
ABSTRACT Fusidic acid is an antibiotic steroid indicated for the treatment of infections caused by the genus Staphylococcus, including methicillin resistant Staphylococcus aureus strains, and other Gram-positive bacteria. In the present study, a stability-indicating reversed-phase liquid chromatography (RP-LC) method was developed and validated for the deter
Braz. J. Pharm. Sci.. Publicado em: 2016-09