Energy Dispersive Spectroscopy
Mostrando 1-12 de 330 artigos, teses e dissertações.
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1. Study of rhombohedral tricalcium phosphate in hexagonal crystal structure family on the sample prepared by the sol-gel route and the effect of calcination temperature
Abstract The effect of the calcination temperature at 800 and 1000 °C on the stable formation of the tricalcium phosphate with rhombohedral structure in the system of the hexagonal crystal family was determined, while its precursor was made from limestone obtained from nature in the Lumajang district, Indonesia. The rhombohedral tricalcium phosphate samples
Cerâmica. Publicado em: 2023
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2. A química analítica aplicada aos estudos de pigmentos rupestres: uma revisão
Instrumental advances have been employed in the study of archeological remains such as prehistoric rupestrians paintings with the objective of chemically characterizing them in order to reconstruct the cultural technologies of a prehistoric human group and/or to support conservation science studies. The analytical techniques most commonly used in archaeometr
Química Nova. Publicado em: 2022
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3. Phase transformation of kaolinite to hexagonal kalsilite using K2CO3
Abstract Hydrothermal synthesis of kalsilite was facilitated by the inclusion of potassium carbonate (K2CO3) as the source of the potassium ion. After a 24 h reaction at 220 °C, kaolin clay treated with 1.25 M K2CO3 showed the most significant peaks at 2θ of 28.5° and 34.7° by X-ray diffraction corresponding to the hexagonal kalsilite. In addition, field
Cerâmica. Publicado em: 2022
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4. Morphology Behavior of Copper Films Deposited after Wet Surface Treatment on Polished Alumina
In this paper, a pre-treatment process for electroless copper (Cu) deposition on the polished alumina (Al2O3) 99.9% and the behavior of Cu plating by electroless process after Al2O3 surface treatment were explored. Our work was carried out by changing the roughness of Al2O3 through micro-etching (coarsening), nucleation its surface by a two-step method (sens
Journal of the Brazilian Chemical Society. Publicado em: 2022
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5. CLOROFILA EXTRAÍDA DE RESÍDUO INDUSTRIAL DA ERVA-MATE (Ilex paraguaiensis) UMA POSSIBILIDADE DE ECONOMIA CIRCULAR
Chlorophyll is the most abundant green pigment on the planet, it is unstable and decomposes naturally. Mate-herb is a traditional native plant in the southern region of South America, and its tea is part of the local culture and extractive agriculture. The mate-herb industry generates as a by-product a resinous material rich in chlorophyll whose use is propo
Química Nova. Publicado em: 2022
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6. Production of nanostructured crystalline composite using residual ashes from flocculated sludge burning process in a poultry slaughterhouse wastewater treatment system
Abstract Nanostructured crystalline composite (activated carbon) was synthesized from residual ashes of the burning process of the sludge generated in the flotation step of a poultry slaughterhouse and was used for Allura red dye adsorption. The ashes were chemically activated using two types of reagents, H2O2 and H3PO4, and the structure, morphology, and su
Cerâmica. Publicado em: 2022
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7. EFFECT OF REACTION CONDITIONS ON PARTICLE SIZE OF ZNO NANOPARTICLES VIA CONTROLLED PRECIPITATION METHOD AND IN-VITRO ANTIBACTERIAL CAPACITY
High-yield ZnO spheroidal nanoparticles with an average diameter around 23 nm (≈ 25% frequency) and 30 nm (≈ 28% frequency) were obtained by controlled semicontinuous precipitation at low temperatures. This synthesis was obtained from hydrozincite (Zn5(CO3)2(OH)6) as primary nanoparticles. The Zn5(CO3)2(OH)6 nanoparticles were synthesized by hydrolysis o
Química Nova. Publicado em: 2022
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8. Tópicos Emergentes em Insuficiência Cardíaca: Terapias Intervencionistas na Insuficiência Cardíaca
In this paper a novel supramolecular strategy to improve the efficiency of a voltammetric sensor to determine two biologically relevant molecules (epinephrine (EP) and uric acid (UA)) is presented. The strategy is based on the use of a glassy carbon electrode modified with a copper(II) complex ([Cu(H2dimpy)Cl]PF6) adsorbed on multi-walled carbon nanotubes (M
Arq. Bras. Cardiol.. Publicado em: 2020-11
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9. Preparation of Fluorescent Carbon-Based Dots from Waste Tire Pyrolysis
The pyrolysis of waste tire has been proposed as an alternative route to its recycling producing residual oils that can be used as fuels. In this work, a physicochemical process to obtain carbon-based dots (CBD) from carbon black (CBL) derivatives of tires is described. For this, the CBL was treated with different acids to produce CBL1 and CBL2 particles sus
J. Braz. Chem. Soc.. Publicado em: 2020-11
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10. Synergistic Supramolecular Effect on the Electro-Oxidation of Biological Relevant Molecules: A Novel Sensor for Simultaneous Determination of Epinephrine and Uric Acid in Human Urine Using MWCNT and a Copper(II) Complex
In this paper a novel supramolecular strategy to improve the efficiency of a voltammetric sensor to determine two biologically relevant molecules (epinephrine (EP) and uric acid (UA)) is presented. The strategy is based on the use of a glassy carbon electrode modified with a copper(II) complex ([Cu(H2dimpy)Cl]PF6) adsorbed on multi-walled carbon nanotubes (M
J. Braz. Chem. Soc.. Publicado em: 2020-11
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11. Dielectric and Magnetic Properties of Epoxy with Dispersed Iron Phosphate Glass Particles by Microwave Measurement
Abstract This paper investigates the dielectric properties and magnetic properties of epoxy composites with different amount of powdered iron phosphate glass (IPG) at 8.2 GHz to 12.4 GHz using microwave technique. IPG composed of 60P2O5-40Fe2O3 (mol%) was produced by conventional melt and quenching method and crushed into powder. The IPG powder was character
J. Microw. Optoelectron. Electromagn. Appl.. Publicado em: 2020-06
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12. Synthesis, Characterization, and Synergic Photocatalytic Activity of Amorphous TiO2/Chitosan Carbon Microspheres
In this work, we report the synthesis and characterization of new amorphous graphene-like TiO2/chitosan carbon microspheres and its performance as photocatalyst. Four different carbon chitosan microspheres materials were obtained based on the distinctive procedure to incorporate TiO2 and TiOSO4 to chitosan structure by pyrolysis at 600 °C. Detailed characte
J. Braz. Chem. Soc.. Publicado em: 2020-06