Energy Dispersive Spectroscopy
Mostrando 13-24 de 330 artigos, teses e dissertações.
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13. Chemically-Activated Biochar from Ricinus communis L. Cake and Their Potential Applications for the Voltammetric Assessment of Some Relevant Environmental Pollutants
Biochar is a rich-carbon material highly functionalized, which allows the use as electrodes modifier for preconcentration and voltammetric determination of several species. This work describes a castor cake biochar production and chemical activation with different reaction conditions using HNO3 and/or H2O2. Biochar samples were characterized using scanning e
J. Braz. Chem. Soc.. Publicado em: 2020-05
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14. Biosorption Potential of the Aspergillus sp. and Insights into Secondary Metabolism in the Presence of Copper and Lead
The fungus Aspergillus sp. was isolated from copper mining rejects and cultured in a liquid culture medium (potato dextrose, PD) enriched with CuSO4.5H2O and Pb(NO3)2 in different concentrations. By flame atomic absorption spectrometry (FAAS) it was observed that fungus absorbed 86% of both copper and lead, with initial concentrations of 100, 500 and 1000 mg
J. Braz. Chem. Soc.. Publicado em: 2020-03
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15. PMMA-SiO2 Organic-Inorganic Hybrid Coating Application to Ti-6Al-4V Alloy Prepared through the Sol-Gel Method
Siloxane-poly(methyl methacrylate) (PMMA) hybrid was synthesized based on the sol-gel method and applied to Ti-6Al-4V through dip-coating. The structural feature of the hybrid was subjected to Fourier-transform infrared spectroscopy (FTIR) and thermogravimetric analysis (TG); its morphological properties were analyzed through scanning electron microscope (SE
J. Braz. Chem. Soc.. Publicado em: 2020-02
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16. Evaluation of a Graphite-Polyurethane Composite Electrode Modified with Copper Nanoparticles as an Amperometric Flow Detector in a Wall-Jet System for the Determination of Cysteine
A graphite-polyurethane composite electrode (GPUE) was modified by electrodeposition of copper nanoparticles (CuNP) followed by electrochemical treatment in NaOH (GPUE-CuNP), in order to prepare an amperometric sensor for the determination of cysteine (Cys). Cyclic votammograms of Cys solutions at GPUE-CuNP allowed the description of a sequence of electroche
J. Braz. Chem. Soc.. Publicado em: 2020-02
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17. Influence of treatment with water-soluble CCB preservative on the physical-mechanical properties of brazilian tropical timber
This aim of this work is to present an analysis of the influence of impregnation against biological demand, realized with saline solution of CCB (Chromated Copper Borate preservative) by vacuum-pressure process, on physical-mechanical properties of tropical wood species Simarouba sp., Cedrelinga catenaeformis and Erisma uncinatum Warm. In theory, such proces
Mat. Res.. Publicado em: 13/01/2020
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18. STUDY OF THE EFFECT OF FUNCTIONALIZATION OF CARBON NANOTUBES ON GAS SEPARATION
Abstract In order to improve the adsorption capacity and selectivity of CO2/CH4 and CO2/N2, we have functionalized multi-walled carbon nanotubes (MWCNT) with 3-aminopropyltriethoxysilane (APTES). The functionalized MWCNT was characterized by Fourier transform infrared (FT-IR), energy dispersive X-ray spectroscopy (EDX) and BET analysis. CO2, CH4 and N2 adsor
Braz. J. Chem. Eng.. Publicado em: 13/01/2020
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19. Effect of Etching Temperature on Surface Properties of Ti6Al4V Alloy for Use in Biomedical Applications
The objective of this study is to evaluate the surface physicochemical properties of Ti6Al4V alloy after etching with a piranha’s solution at temperatures of 25 °C, 40 °C, and 60 °C for 30 min. Scanning electron microscopy with energy-dispersive X-ray spectroscopy, optical profilometry, X-ray diffraction, and wettability analyses were used to characteri
Mat. Res.. Publicado em: 10/01/2020
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20. Chemical and structural composition of black pigmented supragingival biofilm of bovines with periodontitis
RESUMO: A periodontite bovina é uma infecção multifatorial associada primariamente à microbiota potencialmente patogênica presente no biofilme bucal. Biofilmes são estruturas organizadas, nas quais os constituintes convivem em simbiose, descritos em outras espécies como um fator predisponente à periodontite. O objetivo do presente estudo foi caracter
Pesq. Vet. Bras.. Publicado em: 10/01/2020
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21. Solvothermal Synthesis of Cerium-Doped Titania Nanostructured Materials Modified with Acetylacetone for Solar-Driven Photocatalysis
This study reports the preparation of nanostructured cerium-doped titanium dioxide photocatalysts containing different cerium concentrations by a modified sol-gel route involving the use of acetylacetone. The nanocrystalline powders had their structural, morphological, and optical properties characterized by X-ray diffraction, vibrational and Raman spectrosc
J. Braz. Chem. Soc.. Publicado em: 2020-01
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22. Strontium Oxide Decorated Iron Oxide Activated Carbon Nanocomposite: A New Adsorbent for Removal of Nitrate from Well Water
In the present study, activated carbon was magnetized by iron oxide and modified by strontium based nanoparticles (FeAC@Sr) to introduce it as an efficient favorable adsorbent for the removal of nitrate ions from underground water. The decorated adsorbent was characterized in terms of size, structure, morphology and composition using scanning electron micros
J. Braz. Chem. Soc.. Publicado em: 2020-01
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23. Cation Vacancies in NiFe2O4 During Heat Treatments at High Temperatures: Structural, Morphological and Magnetic Characterization
Nickel ferrite (NiFe2O4) was synthesized by mixing stoichiometric amounts of α-Fe2O3 and NiO using mechanical milling and heat treatments at high temperatures. The physical characterization of the samples was carried out using X-ray diffraction, infrared and Raman spectroscopies, Mössbauer spectrometry, magnetization measurements, scanning electron microsc
Mat. Res.. Publicado em: 20/12/2019
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24. Microstructural Evolution and Phase Transformation of a Ti-5Nb-5Al Alloy During Annealing Treatment
The microstructural evolution and phase transformation of a Ti-5Nb-5Al alloy during isothermal annealing treatment were studied in this paper. The microstructural evolution was analyzed by X-ray diffraction (XRD), scanning electron microscope (SEM) equipped with X-ray energy dispersive spectroscopy (EDS) and electron backscattering diffraction (EBSD). The fi
Mat. Res.. Publicado em: 05/12/2019