X Ray Spectrometry
Mostrando 1-12 de 221 artigos, teses e dissertações.
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1. Catalysts Derived from Thermal Treatments of Hydrocalumite-Type Compounds: Synthesis and Application in Transesterification Reactions
Catalyst performance is a relevant factor in biodiesel production because it can affect the efficiency of the process. This work provides a study of the performance of heterogeneous catalysts for biodiesel production derived from thermal-treated hydrocalumite-type compounds. This work aimed to synthesize and characterize hydrocalumite-type compounds intercal
Journal of the Brazilian Chemical Society. Publicado em: 2023
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2. A química analítica aplicada aos estudos de pigmentos rupestres: uma revisão
Instrumental advances have been employed in the study of archeological remains such as prehistoric rupestrians paintings with the objective of chemically characterizing them in order to reconstruct the cultural technologies of a prehistoric human group and/or to support conservation science studies. The analytical techniques most commonly used in archaeometr
Química Nova. Publicado em: 2022
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3. Photo-Fenton-Based Degradation of Methylene Blue Dye Using Hydroxyapatite Nanoparticles Doped with Fe3O4/γ-Fe2O3
In this study, we evaluated the catalytic properties of hydroxyapatite (HA) nanoparticles (NPs) doped with Fe3O4/γ-Fe2O3 for the degradation of methylene blue (MB) dye using a photo-Fenton process at pH 2.5, 7.0, and 9.0. The HA NPs were characterized using X-ray diffraction, scanning electron microscopy, Fourier-transform infrared spectrometry, Raman spect
Journal of the Brazilian Chemical Society. Publicado em: 2022
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4. CLOROFILA EXTRAÍDA DE RESÍDUO INDUSTRIAL DA ERVA-MATE (Ilex paraguaiensis) UMA POSSIBILIDADE DE ECONOMIA CIRCULAR
Chlorophyll is the most abundant green pigment on the planet, it is unstable and decomposes naturally. Mate-herb is a traditional native plant in the southern region of South America, and its tea is part of the local culture and extractive agriculture. The mate-herb industry generates as a by-product a resinous material rich in chlorophyll whose use is propo
Química Nova. Publicado em: 2022
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5. Microstructure and diametral fracture strength of spark plasma sintered WC-6Co-0.2B and WC-6Co-0.5B ceramic composites from nanosized and metastable WC powders
Abstract The present work aimed at evaluating the microstructures and mechanical properties of spark plasma sintered WC-6 wt% Co ceramic composites doped with boron (0.2 and 0.5 wt%). W-50 at% C (W-6.13 wt% C) powders produced under different milling times (20, 60, 180, and 600 min) were used as starting materials and subsequently mixed with Co (6 wt%) and B
Cerâmica. Publicado em: 2022
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6. A Comparison of the Photolytic and Photocatalytic Degradation of Triclosan: Identification of Transformation Products and Ecotoxicity Evaluation
Triclosan (5-chloro-2-(2,4-dichlorophenoxy)phenol) is commonly used as an antibacterial agent in various industrial products and is often detected in wastewater effluent. Comparison was made for triclosan degradation by photolysis and TiO2 photocatalysis (under UV irradiation (125 W)) based on analysis of transformation products, together with ecotoxicity ev
J. Braz. Chem. Soc.. Publicado em: 2021-08
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7. What to Expect for the New Year?
In this work, an analytical method for determination of Ba, Cu, Ni, V, and Zn, in medicinal herbs, through direct solid sample analysis by energy dispersive X-ray fluorescence spectrometry (EDXRF), was applied. Accuracy and precision (intra and inter day) of the analytical method were confirmed through analysis of certified reference material, tomato leaves
J. Braz. Chem. Soc.. Publicado em: 2021-01
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8. Direct Solid Sample Analysis of Medicinal Herbs for Determination of Ba, Cu, Ni, V and Zn by EDXRF
In this work, an analytical method for determination of Ba, Cu, Ni, V, and Zn, in medicinal herbs, through direct solid sample analysis by energy dispersive X-ray fluorescence spectrometry (EDXRF), was applied. Accuracy and precision (intra and inter day) of the analytical method were confirmed through analysis of certified reference material, tomato leaves
J. Braz. Chem. Soc.. Publicado em: 2021-01
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9. Synthesis, Characterization and Exchange Reactions of Layered Double Hydroxides of Copper and Aluminum, Intercalated with Sulfate
Layered double hydroxides (LDHs) of Cu:Al in the molar ratio of 2:1, intercalated with sulfate, sulfate/(Li+, Na+, K+ or NH4+), NO3- and CO32-, were synthesized by co-precipitation with increasing pH. The materials were submitted to exchange reactions using B2SO4 (B = Li+, Na+, K+, NH4+) solutions in an attempt to replace previously intercalated cations or i
J. Braz. Chem. Soc.. Publicado em: 2021-01
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10. X-ray Scattering and Chemometrics as Tools to Assist in the Identification of Gunshot Residues by Wavelength Dispersive X-ray Fluorescence Spectrometry
Wavelength dispersion X-ray fluorescence spectrometry (WDXRF) is a non-destructive technique and therefore attractive for gunshot residues (GSR) analysis. It is well known for determination of inorganic constituents of samples. However, X-ray scattering region spectral data is not commonly used, although it may provide information about organic constituents
J. Braz. Chem. Soc.. Publicado em: 2020-12
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11. “Half-Sandwich”/RuII Anticancer Complexes Containing Triphenylphosphine and p-Substituted Benzoic Acids
Mononuclear and binuclear RuII/arene/triphenylphosphine complexes with p-substituted benzoic acid derivatives were prepared and characterized. These monocationic complexes of type [Ru(η6-p-cymene)(PPh3)L] (L = benzoic acid (1), p-hydroxybenzoic acid (2), p-nitrobenzoic acid (3) and terephthalic acid (4)) were characterized using various techniques, such as
J. Braz. Chem. Soc.. Publicado em: 2020-11
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12. Intercalation of Apocarotenoids from Annatto (Bixa orellana L.) into Layered Double Hydroxides
Synthetic conditions were evaluated to intercalate norbixin into layered double hydroxides (LDH). Norbixin was isolated from a hydrosoluble commercial annatto extract. LDH samples comprising M2+/Al3+ (M = Mg, Zn) were synthesized by coprecipitation and characterized by X-ray diffraction, thermal analysis coupled to mass spectrometry, vibrational spectroscopi
J. Braz. Chem. Soc.. Publicado em: 2020-11