X Ray Emission
Mostrando 13-24 de 239 artigos, teses e dissertações.
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13. Blue-Emitting MWO4:Tm3+ (M: Sr, Ba) Phosphors Prepared by Coprecipitation Method at Room Temperature
MWO4 host matrices (M: Sr, Ba) doped with different Tm3+ concentrations (0.02, 0.04, 0.06, 0.08 and 0.10 mol%) have been successfully prepared by the coprecipitation method at room temperature. The as-prepared nanophosphors were characterized by infrared spectroscopy showing intense absorption bands in the range of 700-1000 cm-1 attributed to the symmetrical
J. Braz. Chem. Soc.. Publicado em: 2020-11
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14. Elemental Composition of Particulate Matter in the Southeastern Brazilian Ceramic Pole by Synchrotron Radiation X-ray Fluorescence Technique (SR-XRF)
In the present study, the elemental content of the particulate matter PM2.5 (particulate matter with diameters lower than 2.5 µm) and PM10 (particulate matter with diameters lower than 10 µm) of the Brazilian city of Rio Claro (SP) were analyzed by synchrotron radiation X-ray fluorescence (SR-XRF) in the Brazilian Synchrotron Light Laboratory (LNLS). A fra
J. Braz. Chem. Soc.. Publicado em: 2020-06
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15. BACTERIAL NANOCELLULOSE BIOMEMBRANE AS A SUPPORT FOR HUMAN INSULIN AIMING AT TRANSDERMAL PERMEATION
Production of bacterial nanocellulose was pursued as a matrix system for the stabilization of human insulin. The biomembranes produced by Gluconacetobacter hansenii were washed with 2% aqueous sodium dodecylsulfate solution, rinsed with ultrapure water and immersed in 1 mol L-1 NaOH aqueous solution at 60 °C for 90 min until neutralization. For the insulin
Quím. Nova. Publicado em: 2020-05
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16. Synthesis, Characterization and Photocatalytic Activity of Au/SiO2@TiO2 Core-Shell Microspheres
By using HAuCl4 as the gold precursor, spherical Au@SiO2/TiO2 core-shell nanostructures were prepared with the sol-gel method and ethanol reflux. The preparation process was convenient and fast. The obtained samples were characterized by UV-Vis, X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TE
J. Braz. Chem. Soc.. Publicado em: 2020-03
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17. Characterization of Nanocellulose Obtained from Cereus Forbesii (a South American cactus)
Crystalline cellulose nanofibers are obtained from the bark of Cereus Forbesii, a cactus native to the arid areas of South America. The obtaining of cellulose nanofibers was carried out in several steps: pretreatment of the raw material, elimination of hemicellulose and lignin to obtain cellulose, and an acid hydrolysis of cellulose to obtain crystalline cel
Mat. Res.. Publicado em: 20/01/2020
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18. Biologically Synthesized Silver Nanoparticles for Enhancing Tetracycline Activity Against Staphylococcus aureus and Klebsiella pneumoniae
Abstract Phytochemical content of plant extracts can be used effectively to reduce the metal ions to nanoparticles in one-step green synthesis process. In this study, six plant extracts were used for the synthesis of silver nanoparticles (AgNPs). Biologically synthesized AgNPs was characterized using UV-Vis Spectrophotometer, Field Emission Scanning Electro
Braz. arch. biol. technol.. Publicado em: 25/11/2019
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19. Influence of doping with Sm3+ on photocatalytic reuse of ZnO thin films obtained by spin coating
ABSTRACT The difficulty in the powder reuse favors the study of materials in the form of thin films. ZnO based films have high photocatalytic potential. In this work, ZnO:xSm3+ (x = 0, 1, 2 and 4 %mol) thin films were prepared by spin coating method. The resins obtained to manufacture the thin films were prepared by complex polymerization method. The samples
Matéria (Rio J.). Publicado em: 25/11/2019
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20. Does height catch-up in schoolchildren have an effect on bone mass in adolescents? Analysis in a Brazilian birth cohort,
Resumo: Objetivo: Analisar o efeito do catch-up de estatura na idade escolar na massa óssea em adolescentes em uma coorte brasileira de nascimento. Métodos: Estudo de coorte, utilizando dados dos três momentos (nascimento, aos 7/9 anos e 18/19 anos) da pesquisa Coortes-RPS. Catch-up de estatura foi definida a partir da diferença entre o Z-score do esco
J. Pediatr. (Rio J.). Publicado em: 28/10/2019
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21. Silver nanoparticles incorporated PVC films: evaluation of structural, thermal, dielectric and catalytic properties
Abstract In this work, silver nanoparticle – polyvinylchloride (SNC-PVC) composites were synthesized by loading 2.5% to 10.0% silver ions to PVC using simple solution casting technique. Material properties including dielectric, thermal stability were discussed in some detail. Incorporation of silver nanoparticles (SNPs) in the PVC matrix was confirmed by U
Polímeros. Publicado em: 03/10/2019
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22. Catalytic Removal of Toluene from Air Streams by Cobalt Oxide Supported on Sepiolite
Removal of toluene using cobalt oxide supported on sepiolite catalysts was investigated. Deposition precipitation method was used to prepare the catalysts. The catalysts were characterized using X-ray diffraction, field emission scanning electron microscopy, energy dispersive X-ray spectroscopy, thermogravimetric analysis (TGA) and Brunauer-Emmet-Teller meth
J. Braz. Chem. Soc.. Publicado em: 16/09/2019
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23. Study of behavior alloy Ti and 316L in to simulated body fluid by electrochemical techniques
ABSTRACT In this work, Ti-316L stainless steel was produced, and its electrochemical behavior was characterized. Ti-steel alloys were produced using an induction furnace, by mixing commercial Ti and 316L stainless steel. X-ray diffraction analyses showed the presence of both the materials, Ti and 316L, in the samples produced. The elemental composition of th
Matéria (Rio J.). Publicado em: 16/09/2019
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24. Caracterização do composto de CuCr2O4 obtido pelo método da reação de combustão em solução
RESUMO O material CuCr2O4 foi sintetizado pela reação de combustão em solução e tratado termicamente na faixa de 600 à 1100oC, afim de verificar a evolução das fases. O composto foi carcterizado estrutural e morfologicamente por meio das técnicas de Difração de Raios X (DRX), refinamentos pelo método de Rietveld, Microscopia Eletrônica de Varred
Matéria (Rio J.). Publicado em: 16/09/2019