Validation Of Method
Mostrando 1-12 de 1095 artigos, teses e dissertações.
-
1. ANALYSIS OF BENZODIAZEPINES IN PLASMA SAMPLES BY DLLME AND LC-DAD: CRITICAL ASPECTS, FLAWS AND ISSUES ENCOUNTERED - A DISCUSSION
Dispersive liquid-liquid microextraction (DLLME) is a fast and simple technique and applicable procedure for the analysis of xenobiotics in different biological matrices. We have developed a DLLME method for the determination of benzodiazepines in plasma samples using liquid chromatography-diode-array detection (LC-DAD). During method validation, relative st
Química Nova. Publicado em: 2022
-
2. Contribution to the forecast of horizontal displacements in continuous fight auger piles in granular soil profile
Abstract This article presents a series of propositions for the prediction of horizontal displacements for continuous fight auger piles in granular soil profiles through modifying the parameters Ay and By from the method proposed by Matlock and Reese (1961). Empirical proposals were also presented for calculating the horizontal soil reaction coefficient (nh)
REM - International Engineering Journal. Publicado em: 2022
-
3. Cross-Cultural Adaptation, Validation, and Arabic Translation of the Eustachian Tube Dysfunction Questionnaire (ETDQ-7)
Abstract Introduction The Eustachian Tube Dysfunction Patient Questionnaire (ETDQ-7) scale is used to assess the effectiveness of the treatment and to determine the severity of the eustachian tube dysfunction (ETD). There is currently no validated Arabic version of the ETDQ-7. Objectives The aim of the present study is to test the validity and the reliabil
International Archives of Otorhinolaryngology. Publicado em: 2022
-
4. Translation, Cultural Adaptation and Validation to Brazilian Portuguese of the Tinnitus Functional Index Questionnaire
Abstract Introduction Tinnitus affects a large portion of the world’s population. There are several questionnaires being used for the evaluation of the severity of tinnitus and its impact in quality of life; however, they do not measure treatment-related changes. So, a new self-reported questionnaire was developed, the Tinnitus Functional Index (TFI), whi
International Archives of Otorhinolaryngology. Publicado em: 2022
-
5. Eco-friendly multivariant green analytical technique for the estimation of ketoconazole by UV spectroscopy in bulk and cream formulation
The pharmaceutical industries are focusing on Green Analytical Chemistry principles like miniaturization, eco-friendly solvent usage, waste recycling, and analyst safety for sustainable results. A simple, eco-friendly sensitive and effective extraction and multivariant green analytical method to estimate ketoconazole in bulk and cream formulation were develo
Química Nova. Publicado em: 2022
-
6. Mathematical Modeling of the Film Influence on the Salting Time of Mozzarella Cheese in a Static and Dynamic System: Application of Artificial Neural Networks of the Multilayer Perceptron Type
The NaCl and KCl diffusion in the film formed on the cheese surface during salting was simulated by the finite element method. The time and salts concentration values on the cheese surface were determined, tabulated, and presented to the multilayer perceptron neural network (MLP) for the regression modeling. The samples were divided into 70, 15 and 15% for t
Journal of the Brazilian Chemical Society. Publicado em: 2022
-
7. Development and Validation of a Rapid and Reliable HPLC-FLD Method for the Quantification of Ciprofloxacin and Enrofloxacin Residues in Zea mays
The accumulation of antibiotics by plants is a currently concern associated to yield reduction and transference of antibiotic residues along the food web. Maize is a staple food in many parts of the world; it is also considered an important ingredient in animal nutrition. Considering the lack of validated analytical methods for the analysis of ciprofloxacin
Journal of the Brazilian Chemical Society. Publicado em: 2022
-
8. Simultaneous GC-NCI-MS Determination of Persistent Organic Pollutants and Current-Use Pesticides in Breast Milk Samples
To preserve human health, persistent organic pollutants (POPs) and current-use pesticides (CUPs) should be monitored in fatty tissues, including breast milk. Therefore, this study aimed to optimize sample preparation conditions using a 32 factorial design for the determination of POPs and CUPs by gas chromatography coupled to mass spectrometry with negative
Journal of the Brazilian Chemical Society. Publicado em: 2022
-
9. An Eco-Friendly Proposal by Integrating Chromatographic Fingerprinting and Multivariate Control Chart in a Non-Target Analysis to Evaluate Grape Juices from Different Farming Practices
A potential eco-friendly method without organic solvents is presented by integrating a chromatographic fingerprint and multivariate control chart based on Q residuals to differentiate grape juices from different farming practices. The sample preparation was only water dilution, and the mobile phase was water acidified with sulfuric acid, which can be readily
Journal of the Brazilian Chemical Society. Publicado em: 2022
-
10. Estimation of body fat in children with intellectual disability: development and cross-validation of a simple anthropometric method
Abstract Objective Population-level monitoring of body composition requires accurate, biologically-relevant, yet feasible methods for estimating percent body fat (%BF). The aim of this study was to develop and cross-validate an equation for %BF from Body Mass Index (BMI), age, and sex among children with intellectual disability (ID). This study further aime
Jornal de Pediatria. Publicado em: 2022
-
11. Validation of the psychological safety, psychological empowerment, intrapreneurial behaviour and individual performance measurements
Abstract Purpose The purpose of this study is to assess the validity of the psychological safety (PS), psychological empowerment (PE), intrapreneurial behaviour (IB) and individual performance (IP) construct measurements originally developed in Western individualistic cultures. Design/methodology/approach Proportionate stratified systematic sampling was us
RAUSP Management Journal. Publicado em: 2022
-
12. Validation and Application of a Methodology for Quantifying Levels of Parabens in Sports Supplements from Brazil Using Liquid Chromatography-Mass Spectrometry
Although parabens have been reported to be used as antimicrobial preservatives in personal care products, pharmaceuticals, and foodstuffs, little is known about the occurrence of these compounds in sports supplements. In this study, a simple, fast and sensitive liquid chromatography tandem mass spectrometry method for simultaneous determination of five commo
Journal of the Brazilian Chemical Society. Publicado em: 2022