2019-01

PRÉ-CONCENTRAÇÃO BASEADA NA COPRECIPITAÇÃO USANDO CROMATO DE PRATA COMO CARREADOR PARA DETERMINAÇÃO DE COBRE POR FAAS

In the present paper, a preconcentration procedure based in the coprecipitation of copper by silver dichromate (Ag2CrO4) and consecutive determination by flame atomic absorption spectrometry (FAAS) was proposed. The experimental factors were optimized from application of the Doehlert matrix and the conditions set: chromate concentration 5.8 × 10-4 mol L-1, silver concentration 1.1 × 10-3 mol L-1, pH 7.3 and disperser concentration HNO3 0.38 mol L-1. Under these conditions, analytical parameters of the procedure were obtained, with the quantification limits of 0.76 µg L-1, precision (based i...

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