Test Of X Ray Diffraction
Mostrando 1-12 de 157 artigos, teses e dissertações.
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1. Study of rhombohedral tricalcium phosphate in hexagonal crystal structure family on the sample prepared by the sol-gel route and the effect of calcination temperature
Abstract The effect of the calcination temperature at 800 and 1000 °C on the stable formation of the tricalcium phosphate with rhombohedral structure in the system of the hexagonal crystal family was determined, while its precursor was made from limestone obtained from nature in the Lumajang district, Indonesia. The rhombohedral tricalcium phosphate samples
Cerâmica. Publicado em: 2023
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2. Carbon Dots from Pilosocereus gounellei for Fluorimetric Determination of Tannin in Tea Using a Flow-Batch System
In this study, xiquexique (Pilosocereus gounellei) native endemic cactus from the Brazilian semiarid was used for the first time as a natural carbon source (“green precursor”) for the synthesis of highly fluorescent carbon dots (CDs). These CDs were successfully used to develop a fast, low-cost, eco-friendly fluorescence method for the determination of t
Journal of the Brazilian Chemical Society. Publicado em: 2023
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3. Microstructure and diametral fracture strength of spark plasma sintered WC-6Co-0.2B and WC-6Co-0.5B ceramic composites from nanosized and metastable WC powders
Abstract The present work aimed at evaluating the microstructures and mechanical properties of spark plasma sintered WC-6 wt% Co ceramic composites doped with boron (0.2 and 0.5 wt%). W-50 at% C (W-6.13 wt% C) powders produced under different milling times (20, 60, 180, and 600 min) were used as starting materials and subsequently mixed with Co (6 wt%) and B
Cerâmica. Publicado em: 2022
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4. Study of soils used with subgrade and sub-ballast in Brazilian railways
Abstract Brazil has an extremely limited railroad network compared to other developed and developing countries. There are projects to expand this mesh. Knowing that the cost of implementing a railroad is high, research for solutions that allow cost reduction is of great importance. But the parameters of the materials used in the subgrade and sub-ballast laye
REM - International Engineering Journal. Publicado em: 2022
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5. An alternative route to extract nickel and cobalt from non-commercial laterite ore
Abstract Laterite ores, which represent around two-thirds of nickel reserves, became an important source of nickel and cobalt metals. The objective of the present study was to investigate the efficiency of a hybrid route to extract nickel and cobalt present in a laterite ore sample which was not commercially attractive to be processed through the current rou
REM - International Engineering Journal. Publicado em: 2022
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6. Organophilic clays and their application in atrazine adsorption
Abstract Atrazine’s adsorptive capabilities make the use of clays practical and effective. Three types of organophilic clays modified by cationic surfactants with the ability of one of these clays to adsorb atrazine in an aqueous medium are discussed in this work. The modification in clays was done with the surfactants cetyltrimethylammonium bromide, cetyl
Cerâmica. Publicado em: 2021-06
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7. Geological - geotechnical characterization of different lithotypes in an underground mine
Abstract A mineralogical, geological and geotechnical characterization of several rock types (phyllite, dolomite, breccia and marl) from an underground mine site aimed, among other things, to identify its mineral composition and to provide parameters to support the understanding of rock mass behavior. For this purpose, it was possible to perform laboratory a
REM, Int. Eng. J.. Publicado em: 2021-01
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8. Mechanical behavior and durability of mortars with quartzite and Portland cement after sulfate attack
RESUMO Os resíduos de rochas ornamentais, especialmente quartzito, causam grande impacto ambiental. Mais impulso tem sido dado à pesquisa sobre a reciclagem desses resíduos nos últimos anos, particularmente para uso como agregados em concreto e argamassa. No entanto, os estudos realizados até o momento não mencionam o comportamento da argamassa mistura
Matéria (Rio J.). Publicado em: 25/11/2019
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9. Produção, caracterização e avaliação in vitro de partículas de quitosana e hidroxiapatita para substituição óssea
Resumo Objetivou-se desenvolver, caracterizar e avaliar in vitro biomateriais compósitos de quitosana com hidroxiapatita (CHI/HA) para atuarem como substitutos ósseos. As quitosanas de baixa (L-CHI) e média (M-CHI) massa molecular foram previamente caracterizadas por gravimetria, viscosimetria e espectrofotometria ultravioleta. Os compósitos de CHI/HA fo
Cerâmica. Publicado em: 14/11/2019
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10. Influence of the Pre-Treatments and Process Temperature on the Adhesion of TiN Films Deposited by PBII&D Over Nitrided Austenitic Stainless Steel
In this work the influence of pre-treatment cleaning processes in the adhesion of TiN films deposited by the plasma based ion implantation and deposition (PBII&D) process over plasma nitrided AISI 316L stainless steel was investigated, varying the gas composition, the duration of the sputtering process and the temperature in the same deposition chamber. The
Mat. Res.. Publicado em: 28/10/2019
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11. Effect of Ca Content on Properties of Extruded Mg-3Zn-0.5Sr-xCa Alloys for Medical Applications
Mg-3Zn-0.5Sr-xCa(wt.%) (x=0, 0.2, 0.5) alloys were fabricated by casting and hot extrusion. X-ray diffraction (XRD) and optical microscopy observation showed that the microstructure of Mg-3Zn-0.5Sr-xCa alloys was composed of α-Mg matrix and Mg17Sr2 phase precipitated along grain boundaries. The tensile strength of the alloy increased from 255MPa to 305MPa w
Mat. Res.. Publicado em: 30/09/2019
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12. Ballistic Behavior of New Alumina Composites Reinforced with Niobo-Phosphate Glass
This work aimed to produce and evaluate the ballistic behavior of niobo-phosphate glass-doped alumina composites. The niobo-phosphate glass (30% Nb2O5- 30% P2O5- 20% CaO - 20% CaF2, by mol) were added to the alumina in six different weight percentages. The composite with the highest densification, measured by the Archimedes assay, was used for the ballistic
Mat. Res.. Publicado em: 23/09/2019