Template Synthesis
Mostrando 13-24 de 1429 artigos, teses e dissertações.
-
13. Nano and Micro Ceramic Membranes from Degradable Templates
Abstract The nano/microstructures with highly porous surface area have attracted tremendous attention, particularly the synthesis and tailoring of porous and hollow materials of high performance. In this paper, an easy method of cost-effective synthesis of hollow ceramic fiber membranes based on Hydroxyapatite, TiO2 and ZrO2 stabilized with Yttrium, is propo
Mat. Res.. Publicado em: 28/07/2016
-
14. USE OF A LOW-COST TEMPLATE-FREE ZSM-5 FOR ATMOSPHERIC PETROLEUM RESIDUE PYROLYSIS
To understand the physicochemical properties and catalytic activity during the pyrolysis of atmospheric petroleum residue, a template-free ZSM-5 zeolite was synthesized using a direct method without additional seeds or an organic structure director and compared with conventionally synthesized ZSM-5. The crystallinities of the two zeolites were evaluated by X
Quím. Nova. Publicado em: 2016-04
-
15. Insights into the posttranslational structural heterogeneity of thyroglobulin and its role in the development, diagnosis, and management of benign and malignant thyroid diseases
ABSTRACT Thyroglobulin (Tg) is the major glycoprotein produced by the thyroid gland, where it serves as a template for thyroid hormone synthesis and as an intraglandular store of iodine. Measurement of Tg levels in serum is of great practical importance in the follow-up of differentiated thyroid carcinoma (DTC), a setting in which elevated levels after total
Arch. Endocrinol. Metab.. Publicado em: 2016-02
-
16. Production of Copper and Cobalt Aluminate Spinels and Their Application As Supports for Inulinase Immobilization
AbstractCopper and cobalt aluminates were obtained through the use of chitosan as template. In this synthesis route, chitosan is eliminated by heating, and a porous material is produced. These oxides were used as supports for inulinase immobilization by adsorption process. Physical properties of produced particles were analyzed by X-ray diffraction (XRD) and
Mat. Res.. Publicado em: 2015-10
-
17. Comparison of Kinetic Study of CTMA+ Removal of Molecular Sieve Ti-MCM-41 Synthesized with Natural and Commercial Silica
This work aimed to determine and compare the apparent activation energy, involved in thermal decomposition of CTMA+ from the pores of Ti-MCM-41 synthesized by two different source of silica in order to evaluate their influence in the template removal. The molecular sieves Ti-MCM-41 were synthesized using rice husk ash (RHA), as alternative low cost source of
Mat. Res.. Publicado em: 2015-06
-
18. Optimization of the synthesis of SAPO-11 for the methylation of naphthalene with methanol by varying templates and template content
Zeólitas SAPO-11 foram sintetizadas com sucesso utilizando três diferentes direcionadores orgânicos (dietilamina (DEA), di-n-propilamina (DPA) e di-isopropilamina (DIPA)) e um conteúdo variável de DPA (nDPA/Al2O3 = 0,8, 1,2, 1,6 e 2,0) sob condições hidrotérmicas. As amostras foram caracterizadas por difratometria de raios X de pó (XRD), microscopia
J. Braz. Chem. Soc.. Publicado em: 2013-07
-
19. Investigation into the role of NaOH and calcium ions in the synthesis of calcium phosphate nanoshells
Calcium phosphate (CaP) nanoshells were prepared using negatively charged liposomes (1,2-dioleoyl-sn-glycero-3-phosphate sodium salt (DOPA)) as a template by base titration synthesis at various concentrations of NaOH and calcium ions. The elemental composition, morphology, particle size, particle size distribution and zeta potential of the products were dete
Brazilian Journal of Chemical Engineering. Publicado em: 2012-03
-
20. Avaliação da síntese e caracterização de zeólita ZSM-5 ausente de direcionador orgânico estrutural
Os processos catalíticos desempenham um papel vital na economia mundial, um negócio que movimenta aproximadamente US$13 bilhões por ano, pois o valor dos produtos depende dos processos catalíticos, incluindo os produtos petrolíferos, químicos, farmacêuticos, borrachas sintéticas e plásticos, entre outros. A zeólita ZSM-5 é utilizada como catalisad
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 25/02/2011
-
21. Materiais nanoestruturados sintéticos tipo esmectitas: sua síntese, caracterização e aplicação em nanocompósitos de polietileno
Materiais naturais nanoestruturados, tipo smectita, têm sido amplamente usados em nanocompósitos poliméricos, com ganhos expressivos em muitas propriedades. Porém, devido a sua natureza polar, seu uso em nanocompósitos de poliolefinas apresenta uma série de problemas. Entre esses problemas está a dificuldade de esfoliação na matriz, o que geralmente
Publicado em: 2010
-
22. Nanoparticles of metal and metal oxides: some peculiar synthesis methods, size and shape control, application to catalysts preparation
One step (direct) and multisteps synthesis methods of metal and oxide nanoparticles are presented including both bottom-up and top-down procedures. Chemical methods involving the polyol process allows to get either isotropic or anisotropic nanoparticles. Nanowires, nanorods and dumbells can be generated either by heterogeneous nucleation or by using a templa
Brazilian Journal of Physics. Publicado em: 2009-04
-
23. Polímeros com capacidade de reconhecimento molecular no controlo da libertação de fármacos. Parte 1: síntese e caracterização
Molecularly imprinted polymers (MIPs) consist of synthetic macromolecular matrix, obtained through molecular imprinting-based methods that show ability to selectively recognize important biological molecules and its application in the drug delivery field is under development. In the present review the main aspects related to the synthesis and characterizatio
Química Nova. Publicado em: 2009
-
24. Novas rotas de síntese de óxidos de titânio e mistos titânio-zircônio mesoestruturados via método sol-gel por template com surfactantes / New synthetic routes for mesostructured titanium dioxide and mixed titanium-zirconium dioxide via surfactant-templated sol-gel methods
Uma nova rota de síntese via metodo sol-gel para óxido de titânio (titânia) e óxido misto titânio/zircônio (zircônia) é proposta neste trabalho. As amostras foram submetidas ao tratamento hidrotérmico e obteve-se compostos mesoestruturados e de elevada área superficial. Algumas amostras foram submetidas à calcinação a 450°C para a verifica
Publicado em: 2009