Synchrotron
Mostrando 1-12 de 186 artigos, teses e dissertações.
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1. Green Synthesis of Upconverting NaYF4 and NaGdF4 Materials and Energy Levels Determination
An alternative green route using a domestic microwave oven to synthesize NaGdF4:Yb,Tm and NaYF4:Yb,Er was successfully developed. Decreasing dopants concentration increased the β-NaREF4/α-NaREF4 ratio in NaGdF4. The scanning electron microscopy (SEM) images of NaGdF4 showed particles ranging from 500 nm to 1 μm with formation of aggregates up to 100 μm,
J. Braz. Chem. Soc.. Publicado em: 2021-08
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2. Crystallographic Changes Accompanying the Verwey Transition in a Magnetite from Steatite
The crystallographic structural analysis of the magnetite of a steatite rock at 298 K, (saturation magnetization, σ = 95.0 J T-1 kg-1) showed two cubic networks and, below Verwey temperature (TV ca.120 K) a monoclinic structure, basing on their cell dimensions and different transitional behaviors when reducing the temperature. A monoclinic structure was ide
J. Braz. Chem. Soc.. Publicado em: 2020-09
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3. Elemental Composition of Particulate Matter in the Southeastern Brazilian Ceramic Pole by Synchrotron Radiation X-ray Fluorescence Technique (SR-XRF)
In the present study, the elemental content of the particulate matter PM2.5 (particulate matter with diameters lower than 2.5 µm) and PM10 (particulate matter with diameters lower than 10 µm) of the Brazilian city of Rio Claro (SP) were analyzed by synchrotron radiation X-ray fluorescence (SR-XRF) in the Brazilian Synchrotron Light Laboratory (LNLS). A fra
J. Braz. Chem. Soc.. Publicado em: 2020-06
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4. LABORATORY INVESTIGATION OF X-RAY PHOTOLYSIS OF METHANOL ICE AND ITS IMPLICATION ON ASTROPHYSICAL ENVIRONMENTS
Methanol (CH3OH) is one of the most abundant organic molecules in astrophysical environments. It has been found in cold regions such as surfaces of comets, ices near young stellar objects and protoplanetary disks, as well as in the gas phase in different regions in space. In this work, we experimentally simulate the methanol ice and its behavior when irradia
Quím. Nova. Publicado em: 2020-05
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5. NANOESPECTROSCOPIA DE ABSORÇÃO DE RADIAÇÃO SÍNCROTRON NO INFRAVERMELHO PARA NANOESPECIAÇÃO DE PRODUTOS DE CORROSÃO METÁLICA
The understanding of chemical and physical behavior of materials, especially metals and their alloys, is of utmost importance for industrial and technological applications, development of new materials and preservation of cultural heritage. The use of complementary analytical techniques has allowed a better understanding of corrosion mechanisms, and results
Quím. Nova. Publicado em: 05/12/2019
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6. Scientific Literature of Small-Angle X-Ray and Neutron Scattering Applied to the Characterization of Materials at the Nanometer Scale
The SAXS and SANS techniques are widely applied to the structural characterization of materials at the nanometer scale. We here report quantitative analyses of the published literature related to these techniques and to relevant features of the International SAS Conferences. A total number of 42,048 articles related to SAXS and SANS were retrieved. The annua
Mat. Res.. Publicado em: 25/11/2019
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7. Effect of α/β Forging on Microstructure and Texture Inhomogeneity in a Ti-1023 Forged Disk
The microstructure and texture distribution of a Ti-1023 forged disk were investigated by scanning electron microscopy and synchrotron-based high-energy X-ray diffraction. The finite element method was used to simulate temperature and strain distribution in order to investigate the relationship of the α/β forging process with microstructure and texture dis
Mat. Res.. Publicado em: 30/09/2019
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8. Elemental Concentration and Sulfur Chemical Speciation in the Amazonian Plant Andira surinamensis Using Synchrotron Radiation Techniques (SR-XRF, XANES), RBS and WD-XRF
The inorganic composition of the bark and leaf of a plant from the Amazon rainforest, Andira surinamensis, was determined using two non-destructive, multi-element techniques: X-ray fluorescence (XRF) and Rutherford backscattering spectrometry (RBS). XRF measurements were made using both a conventional X-ray source and synchrotron radiation. It was observed t
J. Braz. Chem. Soc.. Publicado em: 16/09/2019
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9. Análisis arqueométrico de pigmentos del sitio arqueológico Tambo Colorado por difracción de rayos X sincrotrón
ABSTRACT Despite the exceptional architecture and polychromy of archaeological site of Tambo Colorado, there has been no conservation work or in the architectural structures of raw earth, nor on the surfaces. These jobs require a proper understanding of the state of conservation of the site architecture and the analysis of the materials used. With this purpo
Matéria (Rio J.). Publicado em: 20/05/2019
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10. Local piezo-response for lead-free Ba0.9Ca0.1Ti0.9Zr0.1O3 electro-ceramic by switching spectroscopy
The purpose of this work is to determine the effective piezoelectric coefficient (d33) and the macro ferroelectric hysteresis behavior for the Ba0.9Ca0.1Ti0.9Zr0.1O3 (BCZT). The sample was prepared by the modified Pechini method and it was sintered at 1250 ºC for 5 h. The refinements of X-ray diffraction (XRD) patterns obtained by the Rietveld method sugges
Mat. Res.. Publicado em: 11/01/2018
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11. In Situ Synchrotron Radiation Measurements During Axial Strain In Hydrogen Cathodically Charged Duplex Stainless Steel SAF 2205
The objective of this work is the evaluation of hydrogen effects on the martensitic transformation and strain hardening in Duplex Stainless Steels (DSS) SAF 2205 (UNS S32205/S31803). DSS are two-phase alloys (austenite and ferrite), which are used for applications requiring high mechanical strength, in corrosive environments. Therefore, it is necessary a bet
Mat. Res.. Publicado em: 18/12/2017
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12. In vitro effect of amorphous calcium phosphate paste applied for extended periods of time on enamel remineralization
Abstract Dental applications based on the unique characteristics of amorphous calcium phosphate stabilized by casein phosphopeptides (CPP-ACP) have been proposed, as well as the improvement of its properties. Objectives: The objective of this study was to determine the ability of topically applied CPP-ACP from a commercial product to remineralize subsurface
J. Appl. Oral Sci.. Publicado em: 2017-12