Spme Solid Phase Micro Extraction
Mostrando 1-12 de 16 artigos, teses e dissertações.
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1. Biologically Active Volatile Organic Compounds (VOCs) Produced by Rhizospheric Actinobacteria Strains Inhibit the Growth of the Phytopathogen Colletotrichum musae
The antifungal potential of volatile organic compounds (VOCs) produced by actinobacterial strains Streptomyces sp. (ACTB-77) and Amycolatopsis sp. (ACTB-290) from the rhizosphere of Caatinga plants against Colletotrichum musae was investigated. VOCs produced by these microorganisms (axenic and co-culture) were investigated using headspace-solid phase micro-e
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Quality of olive oils from southeastern Brazil
ABSTRACT This study aimed to characterize the volatile composition and sensory characteristics of virgin olive oils (VOOs) from eight olive cultivars grown in the southeast region of Brazil. The volatiles were extracted by Solid Phase Micro Extraction (SPME) and analyzed by Gas Chromatography coupled to MassSpectrometry (GC-MS). The dominant sensory attribut
Bragantia. Publicado em: 04/11/2019
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3. Maturation and Maceration Effects on Tropical Red Wines Assessed by Chromatography and Analysis of Variance - Principal Component Analysis
Effects of grape maturity, maceration length during winemaking and interaction of both of them on physicochemical parameters, phenolic and volatile composition were investigated in tropical Syrah wines with the aim of finding the best conditions to produce wines that are rich in phenols and positive aroma active compounds. A headspace solid phase micro extra
J. Braz. Chem. Soc.. Publicado em: 04/07/2019
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4. Measurement of Activity Coefficients at Infinite Dilution for Alcohols in [BMIM][CH3SO4] using HS-SPME/GC-FID
ABSTRACT The activity coefficient at infinite dilution (&IN1) and distribution ratios at infinite dilution (&IN2) were determined for alkanols (methanol, ethanol, 1-propanol, 1-butanol, 2-butanol, and 2-methyl-2-propanol) in the ionic liquid (IL) 1-butyl-3-methylimidazolium methyl sulfate ([BMIM][CH3SO4]) by HS-SPME (Headspace - Solid Phase Micro Extraction
Braz. J. Chem. Eng.. Publicado em: 2017-07
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5. Volatile Organic Compounds from Filamentous Fungi: a Chemotaxonomic Tool of the Botryosphaeriaceae Family
Volatile organic compounds (VOCs) from ten endophytic fungal species belonging to the Botryosphaeriaceae family were extracted by headspace-solid phase micro-extraction (HS-SPME) and analyzed by gas chromatography-mass spectrometry (GC-MS). Thirty-four VOCs were identified. Most of the compounds are sesquiterpenes (14 non-oxygenated and 10 oxygenated), and t
J. Braz. Chem. Soc.. Publicado em: 2015-11
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6. Folatos, capacidade antioxidante e trans-2-nonenal em cerveja brasileira / Folate, antioxidant capacity and E-2-nonenal in Brazilian beer
In the present study methods were adapted and applied to quantify levels of folate, antioxidant capacity assessment and E-2-nonenal quantification in Brazilian beers. 5 brands of Pilsen, non-alcoholic and Malzbier beers were used, in can and amber bottle. For determination of folates (folic acid - FA, 10-methyl-folic acid - 10Methyl, 5-methyltetrahydrofolate
Publicado em: 2010
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7. Avaliação de fragrancia em detergente em po por cromatografia gasosa e metodos quimiometricos / Evaluation of fragrance in powder detergent by gas chromatography and chemometrics
Fragrância é uma mistura de moléculas orgânicas como ésteres, cetonas, aldeídos, hidrocarbonetos, alcoóis, entre outras, tendo como fontes substâncias de origem natural ou sintética, que quando combinadas em proporções harmônicas conferem uma característica odorífera ímpar em um perfume ou em um produto perfumado. Considerando essa caracterís
Publicado em: 2009
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8. Determinação de metil-etil-cetona em amostras de urina com amostragem por micro extração em fase sólida (MEFS) em headspace associada à cromatografia gasosa com detector de ionização de chama (CG-DIC)
Methyl ethyl ketone (MEK) is a solvent commonly used in chemical, paint and shoe industry. The aim of this study was to develop and validate a method for urinary quantification of MEK, employing headspace solid phase micro extraction sampling (SPME) coupled to gas chromatography with flame ionization detection (GC-FID). The calibration curve (y=4.6851x-0.001
Química Nova. Publicado em: 2008
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9. Determinação do coeficiente de atividade na diluição infinita (g¥) através da micro-extração em fase sólida (SPME)
In this study a new approach, solid phase micro extraction (SPME), is used in the evaluation of the infinite dilution activity coefficient of the solute in a given solvent. It is the purpose of the current work to demonstrate a different approach to obtain the data needed for studying the solution thermodynamics of binary liquid mixtures as well as for desig
Química Nova. Publicado em: 2007
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10. "Analysis of pharmaceutical compounds in biological fluids using on-line SPME-LC/MS" / "Análise de fármacos em fluidos biológicos empregando o acoplamento SPME-LC/MS"
Conventional methods used for the determination of drugs in biological fluids are based on chromatographic and immunochemical techniques. The biological samples treatment - which includes extraction, pre-concentration and clean up steps has been required in drugs analysis in order to increase both analytical sensitivity and selectivity. Nevertheless, late
Publicado em: 2006
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11. Characterization of Brazilian honeys by solid phase microextraction gas chomatography (SPME-CG) / Tipificação de meis brasileiros por micro-extração em fase solida combinada com cromatografia gasosa (SPME-CG)
O mel é uma das misturas mais complexas de carboidratos produzida pela natureza. É um alimento energético muito importante pelas suas propriedades nutritivas, pelo seu aroma e sabor que dependem fortemente das plantas, flores e condições climáticas presentes na região geográfica onde está localizada a colméia. Não existem metodologias que possibil
Publicado em: 2006
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12. Otimização dos parâmetros de extração para determinação multiresíduo de pesticidas em amostras de água empregando microextração em fase sólida
In this study the factors that affect the extraction of pesticide residues from water samples for their determination by solid-phase micro-extraction (SPME) and GC/MS were optimized. The fiber polymer, the extraction mode, the ionic strength, the stirring rate, the pH and the extraction time were the most significant parameters evaluated. The recovery obtain
Química Nova. Publicado em: 2004-10