Solution Calorimetry
Mostrando 1-12 de 129 artigos, teses e dissertações.
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1. Incorporation of Fluorescent Dyes in Electrospun Chitosan/Poly(ethylene oxide)
Polymeric films have been increasingly investigated due to the ease of miniaturization and integration in several sensor devices. Films obtained from the electrospinning technique have a controlled diameter and homogeneity, and substances can be incorporated into the polymeric network. Electrospinning fiber of chitosan (Ch) and poly(ethylene oxide) (PEO) was
J. Braz. Chem. Soc.. Publicado em: 2021-05
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2. Blue Glow Sticks: Cinnamic Acids and Arylacrylonitriles with Liquid-Crystalline Properties and Highly Fluorescent
Five new π-conjugated chromophores derived from acrylic acid and acrylonitrile were synthesized and their thermal and photophysical behaviors were analyzed. They were designed and synthesized through Knoevenagel condensations between arylacetylenebenzaldehydes and a methylene group activated from cyanoacetic and malonic acids. The characterization of the ta
J. Braz. Chem. Soc.. Publicado em: 2021-01
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3. Antimicrobial High-Density Polyethylene (HDPE)/ZnO Nanocomposites Obtained by in situ Polymerization
Nanostructured zinc oxide (ZnO) prepared by combustion in solution was used to obtain nanocomposites. The ZnO particles were characterized by Brunauer-Emmett-Teller (BET), X-ray diffraction (XRD), and scanning electron microscopy (SEM), showing crystallite size of 32 nm and a superficial area of 32.6 m2 g-1. Nanocomposites with 1, 3, and 5 wt.% of ZnO in the
J. Braz. Chem. Soc.. Publicado em: 2020-08
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4. BACTERIAL NANOCELLULOSE BIOMEMBRANE AS A SUPPORT FOR HUMAN INSULIN AIMING AT TRANSDERMAL PERMEATION
Production of bacterial nanocellulose was pursued as a matrix system for the stabilization of human insulin. The biomembranes produced by Gluconacetobacter hansenii were washed with 2% aqueous sodium dodecylsulfate solution, rinsed with ultrapure water and immersed in 1 mol L-1 NaOH aqueous solution at 60 °C for 90 min until neutralization. For the insulin
Quím. Nova. Publicado em: 2020-05
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5. Preformulation of a liquid dosage formulation of captopril for pediatric use: drug-excipient compatibility and stability studies
Currently, medications used in children are typically modified from pharmaceutical dosage forms designed for adults. Captopril is widely adapted to liquid formulations for use in hospitals. Its stability in the aqueous medium is reduced since it undergoes oxidation producing captopril disulfide (its main metabolite). The aim of this formulation study was to
Braz. J. Pharm. Sci.. Publicado em: 20/12/2019
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6. Sustainable blends of LDPE/NR and sugarcane bagasse ashes with PE-g-MA thermomechanical relationships
RESUMO As blendas poliméricas obtidas com resíduos que antes eram chamados de lixos vêm crescendo como uma solução viável, permitindo melhorias nas propriedades mecânicas e como alternativas sustentáveis. Este trabalho relata os efeitos de misturas de polietileno de baixa densidade (PEBD) e borracha natural(NR), com cinzas de bagaço de cana-de-açú
Matéria (Rio J.). Publicado em: 16/09/2019
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7. PCL/ZnO Bio-friendly Films as Food Packaging Material.Thermal and morphological analysis
ABSTRACT Films of Poly(?-caprolactone) (PCL) and PCL/Zinc Oxide (ZnO) were obtained by solution processing. Thermal behaviour and morphological structure were analysed by means of Thermogravimetry (TGA), Differential Scanning Calorimetry (DSC), Optical Microscopy (OM) and Scanning Electron Microscopy (SEM). The addition of ZnO to PCL decreased the degradatio
Matéria (Rio J.). Publicado em: 06/12/2018
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8. Matéria Evaluation of zinc oxide nanoparticles influence on hydrophilic polymer matrix systems
ABSTRACT Hydrophilic polymer matrix systems (HPMSs) are a highly relevant tool for drugs delivery whose bioavailability is impaired by low hydrosolubility. Besides this, when associated with nanoparticles these systems can provide better control over release profile of the active drug, maintaining the posology. Since polyvinylpyrrolidone (PVP) and zinc oxide
Matéria (Rio J.). Publicado em: 06/12/2018
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9. Estabilidad de las fases U3Si5, USi2-x y USi2 al incorporar Al en solución. Experiencias de calorimetría diferencial de barrido
ABSTRACT U(Mo) alloys are being studied to be applied as a fuel for research and test reactors. When U(Mo) particles are dispersed in an Al matrix, it is known that an interdiffusion during fabrication process and / or irradiation. In this sense, irradiation tests have shown that this IL has a bad behavior under irradiation coming up the addition of Si to Al
Matéria (Rio J.). Publicado em: 19/07/2018
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10. Thermal and Conductivity Studies of VO2+ Doped Methacrylic Acid - Ethyl Acrylate (MAA:EA) Copolymer Films
New polymer electrolyte films of Methacrylic Acid - Ethyl Acrylate (MAA:EA) copolymer embedded with different concentrations of VO2+ ions were prepared by solution casting technique. Thermal properties of these films were investigated employing differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). Electrical conductivity of the films
Mat. Res.. Publicado em: 23/10/2017
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11. Wear Behaviour of Electroless heat Treated Ni-P Coatings as Alternative to Electroplated hard Chromium Deposits
In this present study was evaluated the influence of heat treatment on the wear resistance of electroless high phosphorus nickel coating (9-10% P wt.). In addition, both untreated and treated Ni-P deposits were then compared to electroplated hard chromium coatings in terms of wear behaviour. Three different heat treatment conditions were performed at tempera
Mat. Res.. Publicado em: 24/07/2017
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12. PHBV/cellulose nanofibrils composites obtained by solution casting and electrospinning process
ABSTRACT In this work, nanobiocomposites of poly (3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) reinforced with cellulose nanofibrils (CNFs) were produced by electrospinning and solution casting process. CNFs were obtained by sulfuric acid hydrolysis from Imperata brasiliensis fibers. Nanocomposites loaded with 1 (wt. %) of CNFs were prepared using a mixtur
Matéria (Rio J.). Publicado em: 20/07/2017