Solid Phase Extraction C18
Mostrando 1-12 de 57 artigos, teses e dissertações.
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1. DETERMINATION OF CHEMICAL PROFILE OF Eugenia dysenterica ICE CREAM USING PS-MS AND HS-SPME/GC-MS
The incorporation of Cerrado fruits in food products such as ice cream has many advantages because it represents a source of nutrients and bioactive compounds. Given the demand for less laborious methods to analyze food, the paper spray ionization mass spectrometry technique was applied for the first time for a rapid characterization of the chemical componen
Quím. Nova. Publicado em: 2021-02
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2. HPLC-PDA method validated for the determination of hibalactone in Hydrocotyle umbellata subterraneous parts and its ultrasound-assisted extraction optimization
ABSTRACT In this work, we developed and validated a HPLC-PDA method for the quantification of hibalactone in Hydrocotyle umbellata L., Araliaceae, subterraneous parts extracts and optimized its ultrasound-assisted extraction. Chromatographic separations were carried out with an isocratic mobile phase of acetonitrile/methanol/water (10:65:25), a flow of 0.8 m
Rev. bras. farmacogn.. Publicado em: 27/05/2019
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3. Determination of Phenolic Compounds in Red Sweet Pepper (Capsicum annuum L.) Using a Modified QuEChERS Method and UHPLC-MS/MS Analysis and Its Relation to Antioxidant Activity
In the present work, a fast, easy and efficient analytical method was developed and validated for the determination of phenolic compounds (4-hydroxybenzoic, vanillic, caffeic, p-coumaric, sinapic, ferulic and ellagic acids, and naringenin) in red sweet pepper. Extraction of phenolic compounds was carried out using the quick, easy, cheap, effective, rugged an
J. Braz. Chem. Soc.. Publicado em: 23/05/2019
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4. EXTRAÇÃO EM FASE SÓLIDA DE RESÍDUOS DE AGROTÓXICOS DE ÁGUA SUPERFICIAL, EMPREGANDO UM SORVENTE DE MENOR RETENÇÃO
Solid phase extraction (SPE) is one of the main sample preparation techniques. However, the cost of cartridges and the strong retention of hydrophobic compounds in traditional solid phases are limiting factors for their use. This paper describes the application of lab-made SPE cartridges with low retention material as solid phase, Si(PDAS) - poly(dimethyl-co
Quím. Nova. Publicado em: 2018-06
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5. Determination of Target Pesticide Residues in Tropical Fruits Employing Matrix Solid-Phase Dispersion (MSPD) Extraction Followed by High Resolution Gas Chromatography
A simple method based on matrix solid-phase dispersion (MSPD) extraction and gas chromatography with electron-capture detection (GC-ECD) is employed to determine pesticide residues in the following tropical fruits: banana, mango, melon, papaya and pineapple. In the MSPD proposed method, C18, silica gel and ethyl acetate presented the best results in the extr
J. Braz. Chem. Soc.. Publicado em: 2018-05
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6. Determination of Six Synthetic Dyes in Sports Drinks by Dispersive Solid-Phase Extraction and HPLC-UV-Vis
A simple, fast and efficient method was developed for determination of six synthetic dyes (Tartrazine, Sunset Yellow, Amaranth, Ponceau 4R, Indigo Carmine and Brilliant Blue) in sports drinks using dispersive solid-phase extraction (d-SPE) with the polymeric sorbent Oasis® HLB. Sample preparation using d-SPE permitted to simplify the procedure and use less
J. Braz. Chem. Soc.. Publicado em: 2018-03
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7. Influence of growth regulators on distribution of trichomes and the production of volatiles in micropropagated plants of Plectranthus ornatus
ABSTRACT The profile of volatile organic compounds, the glandular and non-glandular trichomes of Plectranthus ornatus, obtained by in vitro cultivation, was evaluated in plants grown in Murashide and Skoog medium supplemented with benylaminopurine at 4.5, 9.0, and 18.0 µM + naphthaleneacetic acid at 5.37 µM, kinetin at 4.7, 9.3 and 18.5 µM + naphthaleneac
Rev. bras. farmacogn.. Publicado em: 2017-12
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8. Sensitive Estrogens Determination in Wastewater Samples by HPLC and Fluorescence Detection
A sensitive high-performance liquid chromatography-fluorescence detection method (HPLC-FLD) was developed and validated for 17β-estradiol (E2) and 17α-ethinylestradiol (EE2) determination in wastewater samples. Sample preparation was performed by solid-phase extraction (SPE) on Hypersep C18 cartridges. Conditioning and elution solvents and sample volume we
J. Braz. Chem. Soc.. Publicado em: 2017-08
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9. Evaluation of QuEChERS Sample Preparation for Determination of Avermectins Residues in Ovine Muscle by HPLC-FD and UHPLC-MS/MS
A fast and sensitive method using high performance liquid chromatography-fluorescence detection (HPLC-FD) and ultra-high performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) was developed and validated for the determination of avermectins residues in ovine muscle samples. QuEChERS (quick, easy, cheap, effective, rugged and safe) sample pr
J. Braz. Chem. Soc.. Publicado em: 2017-05
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10. Quantificação de alquilbenzeno linear sulfonato em estação de tratamento de efluentes e rios por cromatografia líquida de alta eficiência e extração em fase sólida
The procedures to implement a chromatographic method for the quantification of linear alkyl benzene sulfonate (LAS) in the influent, effluent and sludge of a wastewater treatment plant (WWTP), and in river water and sediment, are described and evaluated. The columns octylsilane (C8) and octadecylsilane (C18) for high performance liquid chromatography were ev
Quím. Nova. Publicado em: 2017-04
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11. Determination of Moxidectin in Serum by Liquid Chromatography-Tandem Mass Spectrometry and Its Application in Pharmacokinetic Study in Lambs
The widespread use of moxidectin (MOX), a parasiticide used in the sheep breeding, has induced the parasite resistance in Brazilian farms. As a consequence, the farmers often increase the dose and frequency of drug utilization, and disregards safety of meat or milk. In order to establish adequate therapeutic treatment it is necessary to know the pharmacokine
J. Braz. Chem. Soc.. Publicado em: 2017-02
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12. ON-LINE SOLID PHASE EXTRACTION COUPLED WITH LIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY FOR THE DETERMINATION OF CODEINE IN HUMAN PLASMA
A specific LC-MS/MS method was developed and validated for automated determination of codeine in human plasma, using on-line solid phase extraction (SPE) system coupled with positive ion electrospray ionization tandem mass spectrometry. The method allowed plasma direct injection onto cartridge without sample pre-treatment. Total analysis time per run was 3 m
Quím. Nova. Publicado em: 2017-01