Sample Pretreatment
Mostrando 13-24 de 105 artigos, teses e dissertações.
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13. ON-LINE SOLID PHASE EXTRACTION COUPLED WITH LIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY FOR THE DETERMINATION OF CODEINE IN HUMAN PLASMA
A specific LC-MS/MS method was developed and validated for automated determination of codeine in human plasma, using on-line solid phase extraction (SPE) system coupled with positive ion electrospray ionization tandem mass spectrometry. The method allowed plasma direct injection onto cartridge without sample pre-treatment. Total analysis time per run was 3 m
Quím. Nova. Publicado em: 2017-01
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14. Clinical Significance of Preoperative Neutrophil – to - Lymphocyte Ratio in Renal Cell Carcinoma
ABSTRACT Introduction: We investigated the prognostic significance of the neutrophil-to-lymphocyte ratio on tumor stage and Fuhrman nuclear grade in renal cell carcinoma. Methods: The records of 432 patients with RCC who underwent radical or partial nephrectomy between 2005 and 2014 were retrospectively reviewed. Patients were classified as group lower tum
Int. braz j urol.. Publicado em: 2016-08
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15. Enhancement of pigment extraction from B. braunii pretreated using CO2 rapid depressurization
Abstract Extraction of compounds from microalgae requires cell disruption as a pretreatment to increase extraction yield. Botryococcus braunii is a microalga with a significant content of carotenoids and other antioxidant compounds, such as chlorophylls. Cell disruption of B. braunii using CO2 rapid depressurization was studied as a pretreatment for the extr
Braz. J. Microbiol.. Publicado em: 2016-06
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16. VALIDAÇÃO INTRALABORATORIAL DA DETERMINAÇÃO DE METILTESTOSTERONA EM ÁGUAS NATURAIS POR VOLTAMETRIA USANDO ELETRODO DE GOTA PENDENTE DE MERCÚRIO
17α-methyltestosterone (17α-MT) is a hormone used in medicine and aquaculture which can be found in natural waters. It is considered an emerging organic pollutant and its accurate and precise analysis is required. Therefore, this study presents the in-house validation of a new voltammetric methodology for 17α-MT analysis in natural waters. A hanging mercu
Quím. Nova. Publicado em: 2015-03
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17. New Sol-gel Formulations to Increase the Barrier Effect of a Protective Coating Against the Corrosion and Wear of Galvanized Steel
This study proposes a new pretreatment method that uses alkoxide precursors with a plasticizing agent; the purpose of this study is to improve the electrochemical and mechanical properties of a galvanized steel surface. Galvanized steel was covered with a hybrid film obtained from a sol that consisted of two alkoxide precursors, 3 - (trimethoxysilylpropyl) m
Mat. Res.. Publicado em: 2015-02
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18. Characterization of xylanase from Streptomyces sp. FA1 and its application for bamboo hydrolysis
Native cellulose can be disintegrated into substructures with nano-size dimension through electronspinning. Typically, the most common source material available for cellulose nano-fiber production is wood. More attempts are employed to find new suitable resources to produce nano-cellulose at present. Bamboo boasts the abundant resource in China and possesses
Matéria (Rio J.). Publicado em: 2014-12
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19. Postretention stability after orthodontic closure of maxillary interincisor diastemas
Anterior spaces may interfere with smile attractiveness and compromise dentofacial harmony. They are among the most frequent reasons why patients seek orthodontic treatment. However, midline diastema is commonly cited as a malocclusion with high relapse incidence by orthodontists. Objectives: This study aimed to evaluate the stability of maxillary interinci
J. Appl. Oral Sci.. Publicado em: 10/06/2014
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20. Bolton ratio in subjects with normal occlusion and malocclusion
AIM: To verify the presence of Bolton anterior and total discrepancy in Brazilian individuals with natural normal occlusion and Angle's Class I and Class II, division 1 malocclusions. METHODS: The sample was divided in three groups (n=35 each): natural normal occlusion; Class I malocclusion; Class II, division 1 malocclusion. Of the 105 Caucasian Brazilian i
Braz. J. Oral Sci.. Publicado em: 2013-12
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21. Análise exploratória rápida e não destrutiva (screening) da presença de elementos químicos tóxicos em material escolar por fluorescência de raios x
Compulsory in Brazil, toy certification aims to prevent possible risks in toy use. The Brazilian National Institute of Metrology (INMETRO) establishes the maximum concentration of toxic elements (TE) that may be present in toys. This study evaluates the presence of TE in different crayons, gouache and modeling clays using X-ray fluorescence. This technique i
Quím. Nova. Publicado em: 2013
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22. Determinação espectrofotométrica de sulfato em álcool etílico combustível empregando dibromosulfonazo III
A sensitive spectrophotometric method was developed for sulphate determination in automotive ethanol fuel. The method based on the reaction of the analyte with barium-dibromosulphonazo(III) complex lead to a decrease in the magnitude of the absorbance signals monitored at 649 nm. No sample pretreatment is required and the proposed method allows sulphate dete
Quím. Nova. Publicado em: 2013
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23. Aperfeiçoamento de sistema de preparo de amostras em microescala por processamento fotoeletrocatalítico de matéria orgânica em célula eletroquímica irradiada com UV-LED, visando à análise de traços de metais / Enhancement of a microscale sample preparation system for photoelectrocatalytic degradation of organic matter in a UV-LED irradiated electrochemical cell, aiming the trace metal analysis
A aplicação do processo de fotoeletrocatálise à eliminação de interferentes orgânicos em baixa concentração na eletroanálise de metais foi abordada tomando o quelato Cu(II)-EDTA como sistema modelo e o restabelecimento da onda voltamétrica do cobre como indicador de efetividade. Desenvolveram-se células eletroquímicas de camada delgada (espessur
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 23/04/2012
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24. Determinação de etanol e metanol em álcool combustível e gasolina empregando métodos eletroanalíticos
In this present work two analytical procedures are presented. The first deals with the simultaneous determination of ethanol (EtOH) and methanol (MetOH) in fuel ethanol samples using Cyclic Voltammetry (CV) and the second, the determination of EtOH in fuel ethanol and gasohol using Batch Injection Analysis with Multiple Pulses Amperometric detection (BIA-MPA
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 16/02/2012