Relative Efficiency
Mostrando 1-12 de 985 artigos, teses e dissertações.
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1. DEVELOPMENT AND OPTIMIZATION OF A SPECTROPHOTOMETRIC METHOD WITH CLOUD POINT EXTRACTION FOR DETERMINATION OF GADOLINIUM
This work describes a simple, sensible, and low-cost analytical method, based on cloud-point extraction (CPE) of the surfactant (1,1,3,3-Tetramethylbutyl)phenyl-polyethylene glycol (Triton X-114), for the efficient extraction and sensible determination of gadolinium after its complexation with 1-(2-pyridylazo)-2-naphthol (PAN) and subsequent determination by
Química Nova. Publicado em: 2022
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2. Electrochemical Determination of Trifluralin Herbicide Using Silver Solid Amalgam Electrode: Application in Fresh Food Samples
This paper reports the use of polished silver solid amalgam electrode (p-AgSAE) allied to square wave voltammetry (SWV) in the development of a simple, sensitive, fast and green electroanalytical methodology for the trifluralin herbicide determination in fresh food samples. The experimental (supporting electrolyte and potential and time accumulation) and vol
J. Braz. Chem. Soc.. Publicado em: 2021-07
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3. SEWAGE PERFORMANCE OF A NEW TYPE OF FLAP FILTER
ABSTRACT The drainage performance of a mesh filter determines the water consumption degree of the filter and the efficiency of the next work cycle. Through analysis, we found that the influent flow rate and the sediment content of the influent were important influencing factors. This experiment focused on the drainage time, pressure difference, and cleanline
Eng. Agríc.. Publicado em: 2021-04
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4. Nitrogen top-dressing fertilization of maize cultivated in single and twin-row systems
ABSTRACT The aim of this study was to evaluate the effects of cropping systems (single and twin-rows) and N fertilizer rates in the second top-dressing on the agronomic performance and relative economic returns of maize. The experiment was conducted in a randomized block design, with subplots and three repetitions. The plots were composed of two cropping sys
Rev. Ceres. Publicado em: 2021-02
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5. A Green Procedure Using Disposable Pipette Extraction to Determine Polycyclic Aromatic Sulfur Heterocycles in Water Samples and Solid Petrochemical Residues
A simple and efficient method using reduced amounts of solvents for the determination of polycyclic aromatic sulfur heterocycles (PASHs) in aqueous matrices from a lagoon and leachate solid waste from a petrochemical industry is proposed. The target analytes were previously concentrated using the disposable pipette extraction (DPX) technique applying gas chr
J. Braz. Chem. Soc.. Publicado em: 2021-02
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6. Development of a Methodology Based on Extraction Induced by Emulsion Breaking for Copper Determination in Gasohol by Graphite Furnace Atomic Absorption Spectrometry
The development of a method based on extraction induced by emulsion breaking (EIEB) aiming copper determination in gasohol using graphite furnace atomic absorption spectrometry (GF AAS) is reported. Emulsification of the gasohol samples was carried out using nitric acid solution, (1,1,3,3-tetramethylbutyl)phenyl-polyethylene glycol surfactant (Triton X-114),
J. Braz. Chem. Soc.. Publicado em: 2021-02
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7. A Facile Synthesized Polyaniline Coated Zerovalent Iron-Silica as an Efficient Sorbent for Magnetic Solid Phase Extraction of Phenolic Pollutants in Water Samples
A magnetic material based on polyaniline coated zerovalent iron-silica (Fe@SiO2@PANI) was simply synthesized using a facile manner under low energy consumption and applied for magnetic solid phase extraction of phenolic pollutants prior to analysis by high performance liquid chromatography-photodiode array detection (HPLC-PDA). The parameters which affected
J. Braz. Chem. Soc.. Publicado em: 2021-01
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8. Optimization of Methodology for Determination of Inorganic Chromium Species in Sewage Sludge Samples by HPLC-ICP-MS/MS
This study developed a methodology for extracting and speciating CrIII and CrVI in sewage sludge by high performance liquid chromatography, inductively coupled plasma tandem mass spectrometry (HPLC-ICP-MS/MS). The optimal procedure was solid-liquid extraction in a water bath with stirring at 50 °C for 16 h and 50 mmol L−1 ethylenediaminetetraacetic acid (
J. Braz. Chem. Soc.. Publicado em: 2020-12
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9. Synthesis, Characterization, Spectroelectrochemical, Photophysical and HSA-Binding Properties of Novel and Versatile meso-Tetra(4-pyridylvinylphenyl)porphyrins Coordinated to Ruthenium(II)-Polypyridyl Derivatives
The free-base meso-tetra(4-pyridylvinylphenyl)porphyrin (1a) and its zinc(II) complex were synthesized and then functionalized with [Ru(bpy)2Cl]+ units (2a and 2b) via conventional methods and evaluated in terms of photophysical, electrochemical and biological aspects. All porphyrins present moderate singlet oxygen production and fluorescence quantum yield,
J. Braz. Chem. Soc.. Publicado em: 2020-11
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10. EVALUATION OF THE RELATIVE PROTECTION FACTOR OF ROSEMARY EXTRACT IN BIODIESEL IN THE PRESENCE OF TRANSITION METAL IONS
Biodiesel contains unsaturated methyl esters making it susceptible to oxidation reaction. Among the factors that cause oxidative instability is the contamination by transition metal ions that in small quantities catalyze the oxidation reaction. The objective of this work was to evaluate the relative protection factor of rosemary extract, in biodiesel, in the
Quím. Nova. Publicado em: 2020-09
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11. Budbreak induction in kiwifruit vines cultivated in an organic system by the biological method of single node cutting
ABSTRACT Kiwifruit vines are an alternative approach to diversify Brazilian fruit farming because of the low supply and increase in the demand for their fruits. Hydrogenated cyanamide, which is the most common rest-breaking agent, is highly toxic and its use is not allowed in organic production systems. This study aimed at evaluating the efficiency of altern
Bragantia. Publicado em: 2020-06
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12. Application of a New Validated HPLC-PDA Method for Simultaneous Determination of Curcumin and Melatonin in Hyaluronic Acid-Coated Nanoemulsions
In this study, a high-performance liquid chromatography with photodiode array detector (HPLC-PDA) method was developed and validated to simultaneously determine curcumin (CUR) and melatonin (MEL) in hyaluronic acid-coated nanoemulsions, a novel targetable delivery system to CD44 receptors overexpressed in many types of tumors. Chromatographic analyses were p
J. Braz. Chem. Soc.. Publicado em: 2020-03