Polycrystalline Samples
Mostrando 1-12 de 51 artigos, teses e dissertações.
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1. Microstructural Analysis of AgIn5VI8 (VI: S, Se, Te) Ternary Semiconductors by X-Ray Diffraction
This work is a study of the microstructural properties of the polycrystalline ternary compounds AgIn5S8, AgIn5Se8, and AgIn5Te8 by X-ray diffraction technique (XRD). The full-width-half-maximum (FWHM) of the XRD profile is measured as function of the diffraction angle and used to estimate the microstructural parameters. In general, a microstructural characte
Mat. Res.. Publicado em: 14/11/2019
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2. Analysis of substrate coverage of hybrid halide perovskite thin films deposited on glass
ABSTRACT In this work we have studied coverage characteristics of organo-metal lead halide perovskite thin films deposited through the spin-coating technique onto glass substrates that were subjected to different predeposition treatments. Samples were deposited at room temperature using different spinning speeds and two different solvents, namely, dimethylfo
Matéria (Rio J.). Publicado em: 19/07/2018
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3. Structural, optical and electrical properties of Ni-doped Co3O4 prepared via Sol-Gel technique
In this article, Nickel doped Cobalt oxide thin films and powders have been prepared on glass substrates using sol gel based dip coating process in order to investigate their optical, structural and electrical properties. The Ni concentration was changed from 0 to 9 wt(%).The synthesized samples were characterised by Ultraviolete visible analysis, X-ray diff
Mat. Res.. Publicado em: 07/02/2018
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4. Growth and Characterization of Graphene on Polycrystalline SiC Substrate Using Heating by CO2 Laser Beam
The thermal decomposition of silicon carbide (SiC), with the subsequent formation of graphene, can be achieved by heating treatment. Several heating processes have been applied for this purpose by using SiC, either in form of powder particles or monocrystalline substrate. In this work, instead of using an expensive commercially available SiC wafer, a polycry
Mat. Res.. Publicado em: 26/09/2016
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5. Effects of hematite surface characteristicson filtration process
Abstract In iron ore pelletizing plants a range of process parameters such as particle size distribution, specific surface area, and moisture, must be controlled to achieve optimized operation conditions. Particle size distribution and specific surface area are controlled during the grinding operations. Moisture, however, is controlled during filtration of t
Rem: Rev. Esc. Minas. Publicado em: 2016-06
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6. A study on the microstructural parameters of Zn (1-x)LaxZrxO nanopowders by X-ray line broadening analysis
In the present study, the pure and La-Zr co-doped ZnO nanoparticles were prepared by sol–gel technique using zinc acetate dehydrate (Zn(Ac)2·2H2O), lanthanum nitrate hexahydrate (La(NO3)3 ·6H2O) and zirconium chloride (ZrCl4) as precursor. The structure and morphology of the prepared nanoparticle samples were studied using X-ray diffraction and transmiss
Mat. Res.. Publicado em: 08/04/2016
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7. Estudio de estructuras de cis- y trans-estilbeno mediante microscopiade fuerza atómica
ABSTRACTNanotechnology is a multidisciplinary field that emerged in recent years due to the development of tools to "see", study and manipulate matter at atomic and molecular levels. Stilbene and some of its derivatives are organic molecules found in nature, which have chemical structures of interest in nano-fabrication of molecular machine building blocks (
Matéria (Rio J.). Publicado em: 2015-09
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8. Plasma Carburizing of Sintered Pure Iron at Low Temperature
In this work, plasma carburizing of sintered pure iron at low temperature was investigated. Samples were carburized under a dc abnormal glow discharge in two mixed atmospheres (5%CH4 + 95%H2 and 20%CH4 + 80%H2) at 500 °C and 700 °C for 3 and 6 hours. The influence of these parameters was investigated by Scan Electron Microscopy (SEM), X-ray Diffraction (DR
Mat. Res.. Publicado em: 2015-04
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9. Development and test of a small resistive fault current limiting device based on Hg, Re-1223 and Sm-123 ceramics
Several reports describing Superconducting Fault Current Limiter (SFCL) containing members of the bismuth or yttrium ceramics were already described. However, none of these included the mercury and samarium cuprates. Consequently, we have conducted a study of a resistive-type superconductor fault current limiter based on Hg0.82Re0.18Ba2Ca2Cu3O8+d samples and
Mat. Res.. Publicado em: 03/06/2014
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10. Influence of microhybrid resin and etching times on bleached enamel for the bonding of ceramic brackets
The aim of this study was to evaluate the shear bond strength (SBS) of polycrystalline ceramic brackets (PCB) bonded after bleaching treatment using different composite resins and enamel etching times. A total of 144 bovine incisors were randomly divided into two study groups (n = 72, each) as follows: G1, enamel bleached with 35% hydrogen peroxide, and G2 (
Braz. oral res.. Publicado em: 2013-04
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11. PROCESSAMENTO, CARACTERIZAÇÃO E ESTUDO DOS FENÔMENOS CRÍTICOS NO SUPERCONDUTOR (Gd1 xCex)Ba2Cu3O7- δ
This work presents a systematic study of the effects of CeO2 addition to the superconductor system (Gd1-xCex)Ba2Cu3O7δ, with 0,0 x 0,05, in polycrystalline form. Samples were obtained following the solid state reaction standard technique in which high purity chemical precursors (99,99%) were employed, Gd2O3, CeO2, BaCO3 and CuO. For the structural chara
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 09/03/2012
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12. CARACTERIZACÃO DAS PROPRIEDADES ESTRUTURAIS E MAGNÉTICAS DA SÉRIE SmFe1xMnxO3. / CHARACTERIZATION OF THE PROPERTIES STRUCTURAL MAGNETIC AND SERIES SmFe1 xMnxO3.
In this work we synthesized sample of the series SmFe1xMnxO3 , in which 1 x 0 whit variation of x = 0:1. Our main objective was the structural and magnetic characterization of the compounds. First, to the best of our knowledge, these samples were obtained by the combustion reaction method, with which we achieve success in obtaining unique polycrystalline pha
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 10/02/2012