Phase Separation
Mostrando 1-12 de 809 artigos, teses e dissertações.
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1. Per-Aqueous Liquid Chromatography for the Separation of Polar Compounds Preparation and Characterization of Poly(ethylene oxide co dimethylsiloxane) Based Stationary Phase
Poly(ethylene oxide-co-dimethylsiloxane) was thermally immobilized on silica particles-Si(PEO)-to separate small polar compounds with water-rich mobile phases. Poly(ethylene oxide-co-dimethylsiloxane) content on Si(PEO) stationary phase was optimized using a central composite design. Infrared spectroscopy, scanning electron microscopy, and thermogravimetric
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Experimental Loss Segregation in a Solid Rotor Induction Motor
Abstract Solid rotor induction motors (SRIMs) are asynchronous motors suited for high speed applications. This work presents an experimental case study where standard loss segregation procedures for induction motors are performed with a two-phase smooth solid rotor induction motor in order to verify their applicability. Even though the machine is supposed to
Journal of Microwaves, Optoelectronics and Electromagnetic Applications. Publicado em: 2022
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3. Preparation of Silicon Oxycarbide (SiCO) Ceramics from Different Polymer Architectures and Assessment on the Performance as Electrodic Materials for Voltammetric Sensing of Antioxidant Phenolic Compounds
Silicon oxycarbide (SiCO) ceramics obtained from polymer pyrolysis and with varied carbon contents were prepared and evaluated as new electrodic materials for sensing of tert butylhydroquinone (TBHQ) and butylated hydroxyanisole (BHA) antioxidants. Three polymers were synthesized varying molecular architecture and aromatic carbon groups, followed by pyrolysi
Journal of the Brazilian Chemical Society. Publicado em: 2022
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4. ERRATUM
This study described the morphology, crystallinity, thermal and mechanical characterization of Polyamide 11 (PA11) porous film prepared by non-solvent induced phase separation (NIPS) method using formic acid (FA) as solvent. In addition, the miscibility of PA11/FA/H2O system was performed to generate a ternary phase diagram. The porous films morphology was i
Arq. Neuro-Psiquiatr.. Publicado em: 2021-06
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5. Polyamide 11 porous films by NIPS: the influence of miscibility and polymer crystalline formation in pores structure and morphology
This study described the morphology, crystallinity, thermal and mechanical characterization of Polyamide 11 (PA11) porous film prepared by non-solvent induced phase separation (NIPS) method using formic acid (FA) as solvent. In addition, the miscibility of PA11/FA/H2O system was performed to generate a ternary phase diagram. The porous films morphology was i
Quím. Nova. Publicado em: 2021-06
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6. Heterotopic Heart Transplant History and Concepts Cannot Be Neglected - Witnessing the History and Learning with Previous Practices
This study described the morphology, crystallinity, thermal and mechanical characterization of Polyamide 11 (PA11) porous film prepared by non-solvent induced phase separation (NIPS) method using formic acid (FA) as solvent. In addition, the miscibility of PA11/FA/H2O system was performed to generate a ternary phase diagram. The porous films morphology was i
Braz. J. Cardiovasc. Surg.. Publicado em: 2021-06
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7. DETERMINATION OF FOUR ARSENIC SPECIES IN ALGAE BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY COUPLED WITH HYDRIDE GENERATION ATOMIC FLUORESCENCE SPECTROMETRY
A rapid method has been developed for the determination of silver arsenite As(III), dimethylated arsenic DMA, monomethylated arsenic MMA, and arsenate As(V) in algae sample using liquid chromatography coupled with hydride generation atomic fluorescence spectrometry (LC-HG-AFS). Types, flow rate and pH of mobile phase were optimized. Under the optimal conditi
Quím. Nova. Publicado em: 2020-09
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8. A SALTING-OUT ASSISTED LIQUID-LIQUID EXTRACTION FOR THE DETERMINATION OF TEBUCONAZOLE, CARBOFURAN AND IMIDACLOPRID IN WHITE AND ROSÉ WINES
Food safety is a constant and necessary concern due to the worldwide increase of the food demand. The monitoring of quality parameters demands the development of accurate, easy and fast procedures. The aim of this work was to develop a cheap, miniaturized and trustworthy salting-out assisted liquid-liquid extraction (SALLE) procedure for the determination of
Quím. Nova. Publicado em: 20/07/2020
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9. A Choline Chloride-Ethylene Glycol Deep Eutectic Solvent Based on Magnetic Polydopamine with Preconcentration and Determination for Sulfonylurea Herbicides in Water Samples
In this study, a novel deep eutectic solvent (DES) containing choline chloride and ethylene glycol was synthesized, and the magnetic polydopamine (PDA) was modified with this deep eutectic solvent to form Fe3O4@PDA-DES. Fourier transformed infrared spectroscopy, scanning electron microscopy, and vibrating sample magnetometer were used to characterize the pro
J. Braz. Chem. Soc.. Publicado em: 2020-07
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10. Determinação de docetaxel e metabólitos em plasma por UPLC-MS/MS: desenvolvimento de metodologia analítica e aplicação clínica
A highly sensitive ultra-performance liquid chromatography tandem mass spectrometry method for the determination of Docetaxel and metabolites (M1+M3) in human plasma samples was developed and validated. The method employs a liquid-liquid extraction and a reversed phase separation Acquity® C18 column BEH C18 (150 x 2.1 mm, 1.7 µm). Mobile phase was a mixtur
Quím. Nova. Publicado em: 2020-04
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11. AVALIAÇÃO DE ADITIVOS DE FASE MÓVEL E TEMPERATURA NA VIDA ÚTIL DE COLUNAS PARA CROMATOGRAFIA LÍQUIDA DE ALTA EFICIÊNCIA
Buffered solutions, additives, and column temperature are widely used in high-performance liquid chromatography to promote adequate retention of compounds and to improve the chromatographic separation. However, these factors can dramatically reduce the column lifetime. In this work, the effect of column temperature, pH and the salt type and concentration in
Quím. Nova. Publicado em: 2020-03
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12. Separation of gadolinium and europium from chloride media by the solvent extraction technique
Abstract Obtaining rare earth elements (REE) is a complicated task, due mainly to the difficulty of separating and purifying them. Solvent extraction is the most widely used technique for separating REE, and the most common extractants used are organophosphorus acids. The low selectivity of this technique leads to the need for a high number of extraction cel
REM, Int. Eng. J.. Publicado em: 2020-03