Optical Emission Spectroscopy
Mostrando 1-12 de 112 artigos, teses e dissertações.
-
1. Synthesis and characterization of α-SnWO4 powders obtained by microwave-assisted hydrothermal method
Abstract The structural, morphological, and optical properties of α-SnWO4 synthesized by microwave-assisted hydrothermal method at 150 °C for different times were investigated. XRD revealed the formation of the orthorhombic phase, without the presence of a secondary phase. The sample processed for 64 min showed a reduction in unit cell volume, suggesting a
Cerâmica. Publicado em: 2022
-
2. Quantification of Carbon Dioxide (CO2), Methane (CH4), and Nitrous Oxide (N2O) Using Near Infrared Spectroscopy and Multivariate Calibration in High Humidity Levels
In this work we developed a promising analytical method combining Fourier transform near-infrared (FT-NIR) spectroscopic technique and first-order multivariate calibration using partial least-squares (PLS) model to simultaneously quantify the main greenhouse gases (GHG’s): methane (CH4), carbon dioxide (CO2), nitrous oxide (N2O) and water vapor (H2O). The
Journal of the Brazilian Chemical Society. Publicado em: 2022
-
3. Preparation of SAPO-34-Based Catalyst for Conversion of Fructose to 5-Hydroxymethylfurfural
Solid acid-catalyzed dehydration of fructose to produce 5-hydroxymethylfurfural (5-HMF) has been a hotspot in biomass conversion research in recent years. In this study, a novel SAPO-34-based catalyst was prepared by consecutive steps of titanium doping, sulfuric acid impregnation, and sulfonic acid functionalization. Characterization of the catalyst with X-
J. Braz. Chem. Soc.. Publicado em: 2021-08
-
4. Blue Glow Sticks: Cinnamic Acids and Arylacrylonitriles with Liquid-Crystalline Properties and Highly Fluorescent
Five new π-conjugated chromophores derived from acrylic acid and acrylonitrile were synthesized and their thermal and photophysical behaviors were analyzed. They were designed and synthesized through Knoevenagel condensations between arylacetylenebenzaldehydes and a methylene group activated from cyanoacetic and malonic acids. The characterization of the ta
J. Braz. Chem. Soc.. Publicado em: 2021-01
-
5. Blue-Emitting MWO4:Tm3+ (M: Sr, Ba) Phosphors Prepared by Coprecipitation Method at Room Temperature
MWO4 host matrices (M: Sr, Ba) doped with different Tm3+ concentrations (0.02, 0.04, 0.06, 0.08 and 0.10 mol%) have been successfully prepared by the coprecipitation method at room temperature. The as-prepared nanophosphors were characterized by infrared spectroscopy showing intense absorption bands in the range of 700-1000 cm-1 attributed to the symmetrical
J. Braz. Chem. Soc.. Publicado em: 2020-11
-
6. Selective Entrapment of Pb2+ from Fresh Thunbergia laurifolia Leaves Extract and Thunbergia laurifolia Tea Extract
The leaves of Thunbergia laurifolia and its tea were extracted by water. The abilities to chelate heavy metal ions of the extracts were studied by inductively coupled plasma-optical emission spectroscopy (ICP-OES) and atomic absorption spectroscopy (AAS). The results showed that the extracts exhibited high selectivity for Pb2+ chelation via a favourable-sele
J. Braz. Chem. Soc.. Publicado em: 2020-03
-
7. Study of behavior alloy Ti and 316L in to simulated body fluid by electrochemical techniques
ABSTRACT In this work, Ti-316L stainless steel was produced, and its electrochemical behavior was characterized. Ti-steel alloys were produced using an induction furnace, by mixing commercial Ti and 316L stainless steel. X-ray diffraction analyses showed the presence of both the materials, Ti and 316L, in the samples produced. The elemental composition of th
Matéria (Rio J.). Publicado em: 16/09/2019
-
8. Adding value to polystyrene waste by chemically transforming it into sulfonated polystyrene
ABSTRACT Polystyrene (PS), one of the most used polymers in everyday life, has a low recycling rate due to its inexpensive virgin resin. In order to make polystyrene waste (WPS) recycling advantageous, it is possible to change it chemically, introducing heteroatoms in the polymer chain thus transforming the waste into a material with more added value. In thi
Matéria (Rio J.). Publicado em: 16/09/2019
-
9. Tuning Emitting Color of Electroluminescent Devices Containing Tris(2-acyl-1,3-indandionate)aluminum(III) Complexes as Emitting Layers
In this study, a novel type of tris(2-acyl-1,3-indandione)-aluminum(III) coordination compounds of the general formula [Al(acind)3]H2O, where 2-acyl-1,3-indandione (acind), 2-acetyl-1,3-indandione (aind), 2-benzoyl-1,3-indandione (bind), and 4-methyl-2-benzoyl-1,3-indandione (mbind), were synthesized and characterized by elemental analysis (CHN), Fourier tra
J. Braz. Chem. Soc.. Publicado em: 12/08/2019
-
10. Espectroscopia óptica de baixo custo: uma estratégia para a introdução de conceitos de física quântica no ensino médio
Resumo Neste artigo, reportamos a confecção e discutimos a aplicabilidade de um espectrômetro óptico de baixo custo como recurso didático para a introdução de conceitos de Física Quântica no ensino médio. O protótipo foi desenvolvido usando grade de difração comercial, lentes convergentes (lupas), webcam e o software Tracker para extração dos
Rev. Bras. Ensino Fís.. Publicado em: 29/04/2019
-
11. Human Hair as Adsorbent of Palladium(II) in Solution: A Precursor of Well-Dispersed Size-Controlled Pd Nanoparticles
This work describes, for the first time, the preparation of palladium nanoparticles supported in thermally-treated human hair. Human hair showed to be an efficient adsorbent of Pd2+ in aqueous media, reaching nearly 100% of adsorption from a 100 ppm solution. The thermal treatment of hair containing Pd2+ at 200 ºC under nitrogen atmosphere led to the format
J. Braz. Chem. Soc.. Publicado em: 2019-04
-
12. Synthesis and characterization of nanostructured TiO2 and TiO2/W thin films deposited by co-sputtering
ABSTRACT Nanostructured TiO2 and TiO2/W thin films were deposited on Corning glass substrates by RF and DC magnetron co-sputtering at room temperature, using three targets of TiO, Ti and W. After deposition, samples were subjected to an annealing treatment in air at 500 °C for 3 hrs. The effect of the annealing treatment and tungsten addition to the TiO2 ma
Matéria (Rio J.). Publicado em: 19/07/2018