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Mostrando 1-12 de 158 artigos, teses e dissertações.
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1. Proposta de avaliação da Política Nacional de Segurança da Informação por Processo de Análise Hierárquica
RESUMO Relatórios recentes de segurança cibernética evidenciam que o Brasil é um dos países com a maior quantidade de crimes cibernéticos, afetando mais de 60 milhões de pessoas e causando prejuízos estimados em mais de 20 bilhões de dólares. No âmbito da Administração Pública Federal, a Política Nacional de Segurança da Informação (PNSI) a
Perspectivas em Ciência da Informação. Publicado em: 2022
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2. Development of a Simple and Fast Procedure Based on Acid Dilution for Determination of Macro and Microelements in Guarana-Based Beverages by ICP OES
A simple analytical procedure is proposed for the direct analysis of guarana-based beverages in order to determine nutrient elements by inductively coupled plasma optical emission spectrometry (ICP OES). A Box-Behnken design, combined with Derringer’s desirability function, was applied to the simultaneous optimization of the ICP OES radiofrequency (RF), sa
J. Braz. Chem. Soc.. Publicado em: 2021-07
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3. What to Expect for the New Year?
In this work, an analytical method for determination of Ba, Cu, Ni, V, and Zn, in medicinal herbs, through direct solid sample analysis by energy dispersive X-ray fluorescence spectrometry (EDXRF), was applied. Accuracy and precision (intra and inter day) of the analytical method were confirmed through analysis of certified reference material, tomato leaves
J. Braz. Chem. Soc.. Publicado em: 2021-01
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4. Direct Solid Sample Analysis of Medicinal Herbs for Determination of Ba, Cu, Ni, V and Zn by EDXRF
In this work, an analytical method for determination of Ba, Cu, Ni, V, and Zn, in medicinal herbs, through direct solid sample analysis by energy dispersive X-ray fluorescence spectrometry (EDXRF), was applied. Accuracy and precision (intra and inter day) of the analytical method were confirmed through analysis of certified reference material, tomato leaves
J. Braz. Chem. Soc.. Publicado em: 2021-01
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5. Determining Mercury in Sediment Samples by Extraction Using a Novel-Chelating Reagent Dithiothreitol (DTT) Followed by Cold Vapor Atomic Fluorescence Spectrometry (CV-AFS)
A new analytical protocol has been developed for the determination of mercury in surface sediments using dithiothreitol (DTT) as a new chelating reagent for the extraction. This protocol requires a small sample mass (250 mg), 4.0 mL of a 0.1 M (pH = 9.0) aqueous DTT solution, and sonication for 30 min, followed by cold vapor atomic fluorescence spectrometry
J. Braz. Chem. Soc.. Publicado em: 2020-12
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6. SPECIATION ANALYSIS OF ARSENIC IN RICE USING HIGH PERFORMANCE LIQUID CHROMATOGRAPHY COUPLED WITH HYDRIDE GENERATION ATOMIC FLUORESCENCE SPECTROMETRY (HPLC-HG-AFS)
The aim of this work was to develop a method using high performance liquid chromatography coupled with hydride generation atomic fluorescence spectrometry (HPLC-HG-AFS) for the determination and speciation analysis of the inorganic and organic species of arsenic found most often in rice samples: As(V), As(III), monomethylarsonic acid (MMA), and dimethylarsin
Quím. Nova. Publicado em: 2020-06
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7. Por que Desenvolvemos Modelos – Da Prática Clínica de Cardiologia a Epidemias de Doenças Infecciosas
This work describes the bioaccessibility in vitro simulated gastric digestion for levels of Zn, Ca, and P in milk and soybean extract samples. Total and dialyzed levels were determined by ICP OES. According to results of the dialyzed samples, it can be concluded that in 250 mL of milk (a glass) the body can be absorb about 1.2 ± 0.2 mg, 14.8 ± 1.2 mg, 4.5
Arq. Bras. Cardiol.. Publicado em: 2020-06
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8. BIOACESSIBILIDADE DE ZINCO, CÁLCIO E FÓSFORO EM EXTRATO DE SOJA E AMOSTRAS DE LEITE BOVINO, CAPRINO E OVINO
This work describes the bioaccessibility in vitro simulated gastric digestion for levels of Zn, Ca, and P in milk and soybean extract samples. Total and dialyzed levels were determined by ICP OES. According to results of the dialyzed samples, it can be concluded that in 250 mL of milk (a glass) the body can be absorb about 1.2 ± 0.2 mg, 14.8 ± 1.2 mg, 4.5
Quím. Nova. Publicado em: 2020-06
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9. Application of Mixture Design Using Diluted Acid for Extraction of Inorganic Components in Fruits of Casearia fasciculata and Determination by ICP OES: Evaluation by PCA and HCA
This study is the first to propose the simultaneous quantification of 10 elements in fruits of Casearia fasciculata by inductively coupled plasma optical emission spectrometry (ICP OES). A method of digestion using dilute nitric acid was optimized by mixture design for extraction of elements in the seed, peel, and pulp of Casearia fasciculata cultivated in t
J. Braz. Chem. Soc.. Publicado em: 2020-06
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10. Use of Arduino in the Development of a New and Fast Automated Online Preconcentration System Based on Double-Knotted Reactor for the Mn Determination in Tea Samples by Flame Atomic Absorption Spectrometry (F AAS)
In the present paper, an automated online preconcentration system based on the use of two knotted reactors (KR) was developed for Mn determination in tea samples by flame atomic absorption spectrometry (F AAS). The system automation was performed by using four solenoid valves to switch sample streams and reagents. Valves were driven electronically by an inte
J. Braz. Chem. Soc.. Publicado em: 2020-01
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11. Cardanols detected in non-polar propolis extracts from Scaptotrigona aff. postica (Hymenoptera, Apidae, Meliponini)
Resumo A própolis elaborada pelas abelhas sem ferrão (Apidae, Meliponini) é um material resinoso extraído de brotos, folhas e exsudatos de plantas, que são misturados com secreções salivares, cera e solo. A espécie Scaptotrigona aff. postica (Latreille, 1807), (Hymenoptera, Apidae, Meliponini), popularmente conhecida como “tubi”, no estado do Mar
Braz. J. Food Technol.. Publicado em: 17/10/2019
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12. Galanthamine and other Amaryllidaceae related alkaloids are inhibitors of α7, α4β2 and α3β4 nicotinic acetylcholine receptors
Abstract Galanthamine is an Amaryllidaceae-derived acetylcholinesterase inhibitor used to treat memory impairment in Alzheimer's disease and vascular dementia. There is evidence that galanthamine, in addition to its effects on acetylcholinesterase, may enhance or inhibit brain nicotinic acetylcholine receptors, which could increase or decrease the therapeuti
Rev. bras. farmacogn.. Publicado em: 17/10/2019