Nano Sized Crystallites
Mostrando 1-4 de 4 artigos, teses e dissertações.
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1. Experimental and Theoretical Study of LiMn2O4 Synthesized by the Solution Combustion Method Using Corn Starch as Fuel
Lithium manganese oxide, LiMn2O4, was synthesized in two temperature stages, where the first consisted by an ecofriendly solution combustion method at 300 °C. Finally, the as-burned powders were thermal treated at 500 and 700 °C. The structural and morphological changes were evaluated by the Rietveld method and density functional theory (DFT) calculations.
J. Braz. Chem. Soc.. Publicado em: 2020-02
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2. Mechanosynthesis, Crystal Structure and Magnetic Characterization of Neodymium Orthoferrite
Neodymium orthoferrite NdFeO3 was obtained at room temperature by mechanosynthesis with a stoichiometric ratio of Nd2O3 and Fe2O3 powders, whereas the traditional synthesis requires a temperature of approximately 1000 °C. The crystal structure was analyzed by X-ray diffraction analysis using Cu radiation and a LynxEye XE detector, whose strong fluorescence
Mat. Res.. Publicado em: 01/03/2016
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3. XRD, AFM, IR and TGA study of nanostructured hydroxyapatite
In this work, the synthetic hydroxyapatite (HAP) was studied using different preparation routes to decrease the crystal size and to study the temperature effect on the HAP nano-sized hydroxyapatite crystallization. X-ray diffraction (XRD) analysis indicated that all samples were composed by crystalline and amorphous phases . The sample with greater quantity
Materials Research. Publicado em: 03/07/2012
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4. Influência da razão combustível-oxidante nas características de óxidos nanoestruturados sintetizados por combustão em solução
Com o aumento do uso do método de síntese por combustão em solução para obtenção de pós cerâmicos, há uma crescente percepção da necessidade de se entender as características únicas deste processo. Esta tese apresenta uma investigação baseada na obtenção de diferentes pós nanoestruturados: Al2O3-α (alumina), Cr2O3 (crômia), Fe2O3-α (hem
Publicado em: 2009