Multiresidue Analysis
Mostrando 1-12 de 22 artigos, teses e dissertações.
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1. Multiresidue Determination of Endocrine Disrupting Compounds in Sewage Treatment Plants (SPE-HPLC-DAD)
This work focuses on the validation and application of solid phase extraction followed by high-performance liquid chromatography (SPE-HPLC) analysis of important endocrine disruptors compounds (EDC) from different classes in highly complex wastewater matrix. The endocrine disruptors investigated included three different categories: pharmaceuticals (sulfameth
J. Braz. Chem. Soc.. Publicado em: 2020-12
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2. Multi-Residue Method for Determination of Thirty-Five Pesticides, Pharmaceuticals and Personal Care Products in Water Using Ionic Liquid-Dispersive Liquid-Liquid Microextraction Combined with Liquid Chromatography-Tandem Mass Spectrometry
Ionic liquid-dispersive liquid-liquid microextraction (IL-DLLME) was used for the determination of different chemical classes of analytes for the first time. Limits of quantification (LOQs) ranged from 0.5 to 2.5 µg L-1, and the linearity ranged from the LOQ of each compound to 50 µg L-1. Recoveries ranged from 70 to 120% for the compounds, with relative s
J. Braz. Chem. Soc.. Publicado em: 2018-06
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3. Validation of a LC-MS/MS Multiresidue Methodology Based on a QuEChERS Approach for the Determination of Fluoroquinolones, Sulfonamides and Trimethoprim in Poultry and Porcine Kidney According to the Normative Instruction 24/2009-MAPA
This work involved the validation of a multiresidue method according to the Normative Instruction 24/2009-MAPA for determining 25 analytes, among fluoroquinolones, sulfonamides and trimethoprim in samples of poultry and porcine kidney. The extraction procedure was based on a QuEChERS approach. A liquid chromatography-tandem mass spectrometry (LC-MS/MS) metho
J. Braz. Chem. Soc.. Publicado em: 2017-01
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4. Optimization of a multi-residue method for 101 pesticides in green tea leaves using gas chromatography–tandem mass spectrometry
ABSTRACT A method for analysis of 101 pesticide residues in tea leaves was developed and validated for the first time. Pure acetonitrile was used as extraction solvent rather than acetonitrile after matrix hydration based on the amount of co-extracts and recoveries performance. During clean-up procedure, primary-secondary amine/graphitized carbon black (500
Rev. bras. farmacogn.. Publicado em: 2016-08
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5. Development of a Multiresidue Method for Pesticide Analysis in Drinking Water by Solid Phase Extraction and Determination by Gas and Liquid Chromatography with Triple Quadrupole Tandem Mass Spectrometry
In this work, a method for multiclass determination of 70 pesticides residues with different properties in drinking water using solid phase extraction (SPE) with polymeric sorbent and determination by gas and liquid chromatography coupled to tandem mass spectrometry (GC-MS/MS and LC-MS/MS) was developed and validated. Different sample volumes, sorbents and e
J. Braz. Chem. Soc.. Publicado em: 2015-10
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6. Optimization of chromatographic conditions and comparison of extraction efficiencies of four different methods for determination and quantification of pesticide content in bovine milk by UFLC-MS/MS
This paper describes the optimization of a multiresidue chromatographic analysis for the identification and quantification of 20 pesticides in bovine milk, including three carbamates, a carbamate oxime, six organophosphates, two strobilurins, a pyrethroid, an oxazolidinedione, an aryloxyphenoxypropionate acid/ester, a neonicotinoid, a dicarboximide, and thre
Quím. Nova. Publicado em: 2014
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7. Multiresidue determination and uncertainty analysis of pesticides in soil by ultrafast liquid chromatography coupled to mass spectrometry
Este trabalho apresenta os resultados da validação de um método simples, rápido e de baixo custo de preparação de amostras para a determinação de resíduos de pesticidas em solo por cromatografia líquida ultrarrápida acoplada a espectrometria de massas com ionização por electrospray. O método se baseia na extração com acetonitrila assistida po
J. Braz. Chem. Soc.. Publicado em: 2013-07
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8. Validação de método de análises multiresíduo para determinação de pesticidas em morango (Fragaria ananassa Duch) e quinoa (Chenopodium quinoa Willd), por técnicas cromatográficas CG-μECD e LC-MS/MS / Validation of multiresidue analysis method for determination of pesticides in strawberry (Fragaria ananassa) and quinoa (Chenopodium quinoa Willd), by chromatographic techniques GC-μECD and LC-MS/MS.
O método de extração QuEChERS, foi ajustado, validado e utilizado para a determinação de doze agrotóxicos organoclorados em 37 amostras de quinoa provenientes da colheita 2010-2011 de Puno - Peru e 36 amostras de morango provenientes de três varejões da cidade de Piracicaba do Estado de São Paulo - Brasil coletadas durante o período de outubro de 2
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 03/09/2012
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9. MÉTODOS INDIVIDUAL E MULTIRRESIDUAL PARA DETERMINAÇÃO DE PESTICIDAS EM GRÃOS E DERIVADOS POR GC-PFPD, GC-ITD-MS E LC-MS/MS / SINGLE AND MULTI-RESIDUE METHODS FOR PESTICIDE ANALYSIS IN GRAINS AND DERIVATES BY GC-PFPD, GC-ITD-MS AND LC-MS/MS
Due to the complexity of grains like soybean, corn and rice, and the very low pesticide concentration expected for these samples, it is really necessary to develop efficient and reliable analytical methods to identify and quantify their residues. The possibility to perform the determination of a large number of pesticides in just a single chromatographic ana
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 29/08/2011
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10. Monitoramento de agrotóxicos em áreas irrigadas por pivô central na microbacia do Tijunqueiro, município de Morrinhos, Goiás / Pesticides monitoring in irrigated areas by central pivot in the Tijunqueiro Watershed municipality of Morrinhos, Goias
The importance of pesticides to the agricultural system production is indisputable, since they are part of the basics inputs, however, it is essential that they be used properly to be preserved not only the quality of the growing product, but also of their own natural resources, especially soil and water. In this study was conducted the pesticides monitoring
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 12/08/2011
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11. Desenvolvimento de métodos cromatográficos hifenados (in-tube SPME/LC-FLD e GCxGC/qMS) para análises de fármacos e agrotóxicos em amostras complexas / Development of hyphenated chromatographic methods (in-tube SPME/LC-FLD and GCxGC/MS) for analysis of drugs and pesticides in complex samples.
Determination of trace levels of drugs in biological fluids and multiresidue (contaminants) in food samples is extremely important because this generates valuable data for therapeutic drug monitoring (individualization of dosage regimen) and quality control (food safety), respectively. Because of the demand for analytical methods with high resolution and low
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 25/07/2011
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12. Extração sólido-líquido com partição a baixa temperatura e seu emprego na análise multirresíduos de agrotóxicos em uva e derivados / Solid-liquid extraction with partition at low temperature and its use in multiresidue analysis of pesticides in grapes and its derivates
The objectives of this work were to optimize and validate the solid-liquid extraction technique with partition at low temperature (ESL-PBT) for multiresidue analysis of samples of grapes by gas chromatography with electron capture detector (GC-ECD). During the optimization procedure of solid-liquid extraction technique with partition at low temperature, fact
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 11/02/2011