Mid Infrared
Mostrando 1-12 de 65 artigos, teses e dissertações.
-
1. Study of Catalytic Pyrolysis of Biomass Sorghum (Sorghum bicolor L. Moench) Using Design of Experiments and Surface Response Methodology
This study proposes a screen of variables that have an influence on the modification of the bio-oil chemical composition as a unique critical quality attribute (CQA) throughout the pyrolytic process (zeolite, ZSM-5) by using a 24 full factorial design, followed by optimization through a response surface methodology (RSM) based on central composite design (CC
Journal of the Brazilian Chemical Society. Publicado em: 2023
-
2. QUANTITATIVE SPECIATION OF THE LIQUID PHASE BY FTIR SPECTROSCOPY IN THE SYSTEM AMP-PZ-CO2-H2O
This work reports a multivariate calibration partial least square regression (PLS) model to quantify the liquid-phase concentrations of 2-amino-2-methyl-1-propanol (AMP), piperazine (PZ), bicarbonate, PZ monocarbamate, and PZ dicarbamate during the absorption/desorption process by Fourier Transform Mid-Infrared spectroscopy (mid-FTIR). The model could predic
Química Nova. Publicado em: 2022
-
3. Production of nanostructured crystalline composite using residual ashes from flocculated sludge burning process in a poultry slaughterhouse wastewater treatment system
Abstract Nanostructured crystalline composite (activated carbon) was synthesized from residual ashes of the burning process of the sludge generated in the flotation step of a poultry slaughterhouse and was used for Allura red dye adsorption. The ashes were chemically activated using two types of reagents, H2O2 and H3PO4, and the structure, morphology, and su
Cerâmica. Publicado em: 2022
-
4. Determination of Ethanol in Gel Hand Sanitizers Using Mid and Near Infrared Spectroscopy
Alcohol-based gel hand sanitizers became very popular during the COVID-19 (coronavirus disease 2019) pandemic. In Brazil, several irregular factories emerged requiring an efficient control by the police and regulatory agencies to guarantee product quality. This problem required a method to determine ethanol content, which led to the development of two method
J. Braz. Chem. Soc.. Publicado em: 2020-09
-
5. FASE SENSORA DE POLI(CLORETO DE VINILA) NA DETECÇÃO DE 17β-ESTRADIOL EM MEIO AQUOSO UTILIZANDO ESPECTROSCOPIA NO INFRAVERMELHO MÉDIO E QUIMIOMETRIA
In recent years, estrogens have gained notable attention among emerging pollutants, increasingly leading to the need for less laborious analytical methods. Optical sensors are a promising technology for the determination of chemical contaminants in water, acting as an alternative screening method. The aim of this work was to evaluate the performance of poly(
Quím. Nova. Publicado em: 2020-09
-
6. Fast Verification of Buffalo’s Milk Authenticity by Mid-Infrared Spectroscopy, Analytical Measurements and Multivariate Calibration
Mid-infrared spectroscopy (MID), chemical composition and physicochemical characteristics associated with chemometrics were used to rapidly detect and quantify the amount of cow’s milk added in buffalo’s milk. A total of 165 samples, divided into buffalo’s milk, buffalo’s milk added with cow’s milk (10 to 90%) and cow’s milk were evaluated to obt
J. Braz. Chem. Soc.. Publicado em: 2020-07
-
7. Double or triple-expressor lymphomas: prognostic impact of immunohistochemistry in patients with diffuse large B-cell lymphoma
Mid-Infrared absorption spectroscopy associate with the Partial Least Squares regression is the official method to monitor Brazilian commercial diesel quality. This method, however, uses solvents and a large number of samples for the construction of the calibration curves, which generates waste and increases the time needed for the analysis. In order to deve
Hematol., Transfus. Cell Ther.. Publicado em: 2020-06
-
8. QUANTIFICAÇÃO DO TEOR DE BIODIESEL DE CRAMBE EM MISTURAS COM DIESEL UTILIZANDO ESPECTROSCOPIA MIR E SELEÇÃO DE VARIÁVEIS
Mid-Infrared absorption spectroscopy associate with the Partial Least Squares regression is the official method to monitor Brazilian commercial diesel quality. This method, however, uses solvents and a large number of samples for the construction of the calibration curves, which generates waste and increases the time needed for the analysis. In order to deve
Quím. Nova. Publicado em: 2020-06
-
9. IDENTIFICAÇÃO DE ADULTERANTES DE BIODIESEL METÍLICO DE CRAMBE EM MISTURAS COM DIESEL, USANDO FT-MIR E CARTAS DE CONTROLE MULTIVARIADAS BASEADAS NO SINAL ANALÍTICO LÍQUIDO
Adulterants in biodiesel/diesel blends modifies its physical and chemical properties. In this work, Fourier Transform Mid-Infrared spectrometry (FT-MIR) and multivariate control charts based on Net Analyte Signal (NAS) were used to monitor the quality of Crambe methyl biodiesel in relation to the biodiesel content and the presence of adulterants. The calibra
Quím. Nova. Publicado em: 2020-01
-
10. Estimation of elemental composition of agricultural soils from West Azerbaijan, Iran, using mid-infrared spectral models
RESUMO A caracterização da composição elementar fornece informações úteis para caracterizar o grau de alteração dos solos. Em Miandoab, norte do Irã, esta caracterização não existe. Os objetivos deste trabalho foram avaliar o grau de intemperismo dos solos típicos da região usando a sua composição elementar e estimar esta composição usando
Rev. bras. eng. agríc. ambient.. Publicado em: 01/07/2019
-
11. Avaliação do uso de argilas montmorilonitas modificadas na adsorção de nitrato em meio aquoso
RESUMO Este estudo investigou a eficiência da remoção de nitrato em meio aquoso usando adsorção em argilas montmorilonitas comerciais, comparativamente a uma resina aniônica comumente usada nessa operação. Algumas dessas argilas foram intercaladas como o íon hexadeciltrimetilamônio para avaliação. Áreas superficiais específicas, capacidades de
Eng. Sanit. Ambient.. Publicado em: 21/03/2019
-
12. Composition Determination of Rubber Blends by Applying Differential Scanning Calorimetry and SPA-PLS Treatment
This paper proposes an innovative approach to determine the composition of natural rubber (NR) and styrene butadiene rubber (SBR) blends from the analysis of the data provided by the differential scanning calorimetry (DSC) technique. DSC registers are post-processed, based on a multivariate chemometric approach, consisting in the application of the successiv
Mat. Res.. Publicado em: 07/01/2019