Microwave Induced Combustion
Mostrando 1-12 de 21 artigos, teses e dissertações.
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1. Halogen Determination in Polymeric Waste of Electrical and Electronic Equipment: Overcoming Limitations in Sample Preparation
Sample preparation of polymers for halogen determination requires special attention because they are difficult to bring into solution and due to the risk of analyte losses when using acid digestion. A method using microwave-induced combustion (MIC) was optimized for accurate determination of halogens in polymeric parts obtained in waste of electrical and ele
J. Braz. Chem. Soc.. Publicado em: 24/10/2019
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2. Chlorine and Fluorine Determination in Eye-Pencil: Development of an Eco-Friendly Sample Preparation Method for Ion Chromatography Analysis
In this paper, a feasible method was proposed for the chlorine and fluorine determination in eye-pencil samples using ion chromatography (IC). The microwave-induced combustion (MIC) was used to digest up to 200 mg of a sample, with 50 mg of microcrystalline cellulose as a combustion aid and only water for analytes absorption. Cl and F recoveries were 105 ±
J. Braz. Chem. Soc.. Publicado em: 21/10/2019
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3. Feasibility of DLLME for the Extraction and Preconcentration of As and Cd in Sugar for Further Determination by ICP-MS
A method for determining low levels of As and Cd by dispersive liquid-liquid microextraction (DLLME) and inductively coupled plasma mass spectrometry (ICP-MS) was proposed. The following parameters that affect extraction efficiency were investigated: type and volume of extraction solvent (1000 µL acetone), type and volume of dispersive solvent (75 µL carbo
J. Braz. Chem. Soc.. Publicado em: 2017-09
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4. DETERMINAÇÃO SIMULTÂNEA DE METAIS E ENXOFRE POR ICP-OES EM RESÍDUOS DE DESTILAÇÃO DE PETRÓLEO
A method for digestion of crude oil distillation residues (atmospheric residue, AR and vacuum residue, VR) using microwave-induced combustion (MIC) was developed for simultaneous determination of metals (Ba, Co, Fe, Mg, Mn, Ni and V) and sulfur by inductively coupled plasma optical emission spectrometry (ICP-OES). Samples were wrapped in polyethylene films a
Quím. Nova. Publicado em: 2016-11
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5. Microwave-Induced Combustion of Coal for Further Sulfur Determination by Inductively Coupled Plasma Optical Emission Spectrometry or Ion Chromatography
In this work, a method using microwave-induced combustion (MIC) was optimized in order to obtain a fast, simple, efficient and greener sample preparation method for coal digestion and further determination of sulfur by inductively coupled plasma optical emission spectrometry (ICP OES). Accuracy was evaluated by comparison of the results with those obtained u
J. Braz. Chem. Soc.. Publicado em: 2016-09
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6. Alternative Igniters Based on Oxidant Salts for Microwave-Induced Combustion Method
In this work, solutions of oxidant salts were evaluated as alternative to nitrate solution for the ignition step in microwave-induced combustion (MIC) method. Aqueous solutions of KClO4, K2Cr2O7, KMnO4 and K2S2O8 in several concentrations were evaluated and it was observed that the ignition was dependent on the concentration and type of igniter solution. Mor
J. Braz. Chem. Soc.. Publicado em: 2016-03
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7. Nickel-based Catalyst Precursor Prepared Via Microwave-induced Combustion Method: Thermodynamics of Synthesis and Performance in Dry Reforming of CH4
Nickel-based catalyst precursor for dry reforming of methane was successfully prepared by a self-combustion method. Three different amino acids: urea, glycine and citric acid were tested as fuels in the redox reaction with metal nitrates. For each fuel, a thermodynamic modeling of the combustion reaction was performed. The samples were characterized by X-ray
Mat. Res.. Publicado em: 25/08/2015
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8. Element Determination in Pharmaceuticals Using Direct Solid Analysis- Electrothermal Vaporization Inductively Coupled Plasma Optical Emission Spectrometry
A solid sampling electrothermal vaporization inductively coupled plasma optical emission spectrometry (ETV-ICP OES) method for determination of As, Cd, Cr, Cu, Mn, Mo, Ni, Pb, Pd, Pt, Rh, Ru and V in pharmaceuticals is proposed. Tricyclic pharmaceuticals were directly analyzed due to their difficult decomposition with acids. Pyrolysis and vaporization temper
J. Braz. Chem. Soc.. Publicado em: 2015-03
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9. Determinação de bromo e iodo em alga marinha comestível por ICP-MS após decomposição por combustão iniciada por micro-ondas
A method based on microwave-induced combustion (MIC) was applied for the decomposition of different types of edible seaweed (Nori, Hijiki and Wakame) for subsequent determination of bromine and iodine by inductively coupled plasma mass spectrometry (ICP-MS). Decomposition of 500 mg of each sample was achieved in less than 30 min. A single and diluted solutio
Quím. Nova. Publicado em: 2014-07
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10. Avaliação de métodos de preparo de amostra para a determinação de halogênios em alumina de alta pureza / Evaluation of sample preparation methods for halogens determination in high-purity alumina
The presence of trace elements in high purity alumina (e.g. halogens) can compromise the final product characteristics. In this work, different sample preparation methods based on alkaline fusion, halogen extraction in water with and without microwave heating, alkaline extraction, microwave-induced combustion and pyrohydrolysis for further halogens determina
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 08/04/2011
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11. Bromine and chlorine determination in cigarette tobacco using microwave-induced combustion and inductively coupled plasma optical emission spectrometry
A combustão iniciada com micro-ondas (MIC) foi aplicada para decomposição de amostras de tabaco de cigarro e subsequente determinação de bromo e cloro por espectrometria de emissão óptica com plasma indutivamente acoplado (ICP OES). Massas de amostra de até 500 mg foram decompostas em frascos fechados e pressurizados com 20 bar de oxigênio. A combus
Journal of the Brazilian Chemical Society. Publicado em: 2011-09
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12. DETERMINAÇÃO DE ELEMENTOS TRAÇO EM SOLO POR ICP-MS APÓS VOLATILIZAÇÃO EMPREGANDO COMBUSTÃO INICIADA POR MICRO-ONDAS
In this work the microwave-induced combustion (MIC) method was proposed for the decomposition of soil samples and subsequent determination of As, Bi, Cd, Hg, Pb and Se by inductively coupled plasma mass spectrometry (ICP-MS). Soil samples (up to 300 mg) were mixed with microcrystalline cellulose (300 or 500 mg), homogenized and pressed as pellets. Pellets we
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 2011