Method Of Rietveld
Mostrando 13-24 de 90 artigos, teses e dissertações.
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13. Microstructure and Electrical Characterization of Thermoelectric Nanocrystalline Bi2 Te3 Synthesized by Mechanical Alloying
Nanocrystalline bismuth telluride, Bi2Te3 has been synthesized by mechanical alloying (MA) the powder mixture composed of Bi and Te in the inert gas atmosphere within a short duration of 15 min. Microstructure characterization of the prepared powder has been investigated adopting the Rietveld’s method using X-Ray diffraction (XRD) data and analyzing high-r
Mat. Res.. Publicado em: 28/10/2019
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14. Nanoparticles of Ni1-x Znx Fe2 O4 used as Microwave Absorbers in the X-band
Ferrites nanoparticles of Ni1-xZnxFe2O4 ferrites with x varying between 0 and 1, in steps of 0.2, were obtained by solution combustion synthesis (SCS) and dispersed in oil paint at the concentrations of 10, 20, 30 and 40% by ferrite weight of ferrite, with the aim of producing electromagnetic wave absorbing composites, in the X band (8-12 GHz). The ferrite p
Mat. Res.. Publicado em: 21/10/2019
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15. Síntese e caracterização de cobaltita de níquel (NiCo2O4) obtida pelométodo dos precursorespoliméricos
RESUMO A cobaltita de níquel (NiCo2O4) de estrutura do tipo espinélio apresenta baixa estabilidade térmica em torno dos 400 °C, que ocasiona a perda de NiO, afetando de maneira significativa as propriedades físicas e estruturais do material produzido. Neste trabalho a cobaltita de níquel foi preparada pelo método dos precursores poliméricos. O materi
Matéria (Rio J.). Publicado em: 16/09/2019
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16. Dielectric Behavior of α-Ag2WO4 and its Huge Dielectric Loss Tangent
The microwave-assisted hydrothermal method was used to obtain α-Ag2WO4. Rietveld refinement confirmed that α-Ag2WO4 is stable in the orthorhombic phase, without secondary phase. However, field-effect scanning electron microscope analysis showed that α-Ag2WO4 nanorods surfaces contain silver nanoparticles, confirmed by the X-ray photoelectron spectroscopy
Mat. Res.. Publicado em: 02/09/2019
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17. Influence of grinding on the pozzolanic activity of granite residue
Abstract This study explores the potential of the granite residue to be applied as a supplementary cementitious material. Furthermore, the efficiency of grinding methods in the improvement of the residue reactivity was also evaluated. The granite residue was collected in a facility located in Brazil and used as a Portland cement replacement with a substituti
REM, Int. Eng. J.. Publicado em: 19/06/2019
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18. Evaluation of the Rietveld method for the mineralogical characterization of airborne dust in a mining area
Abstract In this article, we present the results of the mineralogical quantification of airborne dust from an urban area located in the Brazilian state of Minas Gerais in the vicinity of a gold mine. Three samples were collected at different points to assess spatial consistency. Results showed that the mineralogy, in relation to both major minerals and acces
REM, Int. Eng. J.. Publicado em: 2019-06
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19. Análisis arqueométrico de pigmentos del sitio arqueológico Tambo Colorado por difracción de rayos X sincrotrón
ABSTRACT Despite the exceptional architecture and polychromy of archaeological site of Tambo Colorado, there has been no conservation work or in the architectural structures of raw earth, nor on the surfaces. These jobs require a proper understanding of the state of conservation of the site architecture and the analysis of the materials used. With this purpo
Matéria (Rio J.). Publicado em: 20/05/2019
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20. Performance evaluation of NiCo2O4 spinel as a catalyst for partial oxidation of methane
ABSTRACT The NiCo2O4 catalyst with spinel structure was prepared by a modified polymeric-precursor method using gelatin as an organic-directing agent. The obtained powder was characterized by XRD, TPR and tested on the partial oxidation of methane. The Rietveld analysis performed on the XRD pattern confirmed the crystallization of two phases, the spinel NiCo
Matéria (Rio J.). Publicado em: 20/05/2019
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21. Thermal, Mechanical and Microstructural Analysis of Metakaolin Based Geopolymers
In the present work, geopolymer matrices were developed by alkali activation of metakaolin, using NaOH and sodium silicate as activators. The samples of metakaolin and matrices were studied by thermal analysis (TGA/DTA) at temperatures between 22°C and 1000°C in a nitrogen atmosphere with a heating rate of 10°C/min. The analyses showed gradual mass losses
Mat. Res.. Publicado em: 20/05/2019
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22. Síntese e caracterização das fases minerais C3S, C2S, C3A e C4AF para utilização em cimento tipo Portland
Resumo As principais fases contidas no cimento Portland são 3CaO.SiO2 (C3S), 2CaO.SiO2 (C2S), 3CaO.Al2O3 (C3A) e 4CaO.Al2O3.Fe2O3 (C4AF). No processo industrial estas apresentam incorporações de outros elementos que dependem das matérias-primas e dos combustíveis utilizados na queima. O uso das fases puras auxilia na compreensão dos fenômenos envolvid
Cerâmica. Publicado em: 2019-01
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23. Structural, Thermal, Optical, and Photoacoustic Study of Mechanically Alloyed Nanocrystalline SnTe
A nanostructured SnTe phase was produced by mechanical alloying after 2 h of milling. Part of the as-milled powder was annealed and its X-ray diffraction (XRD) pattern was recorded. The XRD patterns of the as-milled and annealed samples were refined using the Rietveld method. After annealing, partial decomposition of the SnTe phase was observed and corrobora
Mat. Res.. Publicado em: 07/06/2018
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24. Tunable Magnetic and Electrical Properties of Cobalt and Zinc Ferrites CO1-XZnXFe2O4 Synthesized by Combustion Route
Co and Zn ferrites with general formula CO1-XZnXFe2O4 (x = 0; 0,2 and 0,8) were synthesized by combustion reaction method, using urea as fuel. The structure of inverse-spinel-type ferrite were characterized through XRD using Rietveld refinement method to identify, quantify phases and determine lattice parameters. The crystallites had mean size of 37,33 nm, 4
Mat. Res.. Publicado em: 12/03/2018