Medium Infrared
Mostrando 1-12 de 203 artigos, teses e dissertações.
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1. Synthesis of delafossite CuCrO2 via solution combustion method and its acid functionalization for biodiesel production
Abstract CuCrO2 was synthesized by solution combustion synthesis (SCS) and applied as a heterogeneous catalyst to produce soybean biodiesel. The combustion reaction was carried out using urea as a fuel, and copper (II) and chromium (III) nitrates as precursors. After the powders’ obtention, these were calcined and functionalized in an acidic medium. The po
Cerâmica. Publicado em: 2023
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2. Synthesis of Triazoles by Electro-Assisted Click Reaction Using a Copper Foil Electrode
This paper presents an innovative pathway for the synthesis of triazoles using the well-known “click chemistry” assisted by the electrochemical oxidation of metallic Cu0. The click reaction is used to couple a wide range of biological interest compounds. In this case, faster and less polluting methods for a biological environment was achived by in situ C
J. Braz. Chem. Soc.. Publicado em: 2021-07
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3. Liquid Phase Nitration of Benzene Catalyzed by a Novel Salt of Molybdovanadophosphoric Heteropolyacid
A highly efficient and reusable catalyst QA-HPMV was successfully prepared by the reaction of quinoline-2-formic acid (QA) with molybdovanadophosphoric heteropolyacid (H4PMo11VO40, HPMV) for the nitration of benzene. The physical and chemical properties of the sample was characterized by X-ray diffraction analysis (XRD), Fourier transform infrared spectrosco
J. Braz. Chem. Soc.. Publicado em: 2021-06
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4. DIFERENCIAÇÃO CATIÔNICA DE BENTONITAS POR INFRAVERMELHO: UM ESTUDO DOS EFEITOS DA HIDRATAÇÃO DOS CÁTIONS TROCÁVEIS
In the bentonite industry, the most common procedure for quality control of the ore and the sodium activation process is the swelling method. However, this tool is restricted only to the differentiation of the sodium and non-sodium types, not considering the other cationic varieties. The objective of this study was to establish parameters for cationic differ
Quím. Nova. Publicado em: 2021-03
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5. Yellow Mombin (Spondias mombin L.) Seeds from Agro-Industrial Waste as a Novel Adsorbent for Removal of Hexavalent Chromium from Aqueous Solutions
The objective of this study was to develop a low-cost and eco-friendly adsorbent from agro-industrial waste for the removal of hexavalent chromium in the aqueous medium. The adsorbent (BMC) produced from yellow mombin (Spondias mombin L.) seeds was characterized by the determination of the chemical composition, thermal analysis (thermogravimetric (TG) analys
J. Braz. Chem. Soc.. Publicado em: 2021-02
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6. Chitosan-Sodium Alginate Polyelectrolyte Complex Coating Pluronic® F127 Nanoparticles Loaded with Citronella Essential Oil
Pluronic® F127 nanoparticles were loaded with citronella essential oil (CEO) and then covered with chitosan-sodium alginate polyelectrolyte complex (PEC). The system was characterized according to size, zeta potential and stability over time. Dynamic light scattering (DLS) in different proportions of water/ethanol as a dispersive medium was important in con
J. Braz. Chem. Soc.. Publicado em: 2020-04
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7. Characteristics of glucose oxidase immobilized on Magnetic Chitosan Nanoparticles
Abstract Immobilization process is used to facilitate the enzyme recovery and reusability. The aims of this study were to evaluate the effect of different amounts of chitosan on immobilization efficiency of Glucose Oxidase (GOX), pH effect on enzyme activity and changes of kinetic characteristics of enzyme immobilized on Magnetic Chitosan Nanoparticles (MCNP
Food Sci. Technol. Publicado em: 2020-03
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8. Preparation and Delayed Release Study on Pancreatin Encapsulated into Alginate, Carrageenan and Pectin Hydrogels
In this study, biopolymer-based pH-sensitive hydrogels have been successfully prepared using alginate, κ-carrageenan and pectin aimed at the encapsulation of pancreatin (hydrolytic enzymes like α-amylase, lipase and protease) so as to preserve enzymatic activities. Hydrogels have been characterized by Fourier transform infrared spectroscopy (FTIR), thermog
J. Braz. Chem. Soc.. Publicado em: 2020-02
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9. POLYETHERIMIDE/POLYVINYLPYRROLIDONE HOLLOW-FIBER MEMBRANES FOR USE IN HEMODIALYSIS
Abstract In this study, polyetherimide/polyvinylpyrrolidone (PEI/PVP) hollow fiber membranes (HFMs) were synthesized by the phase inversion method. The synthesized PEI/PVP membranes were characterized by morphological analysis and transport properties (hydraulic permeability and solute rejection coefficient). Their performance in uremic solutes separation wa
Braz. J. Chem. Eng.. Publicado em: 13/01/2020
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10. Performance eletrocatalítica frente a nitrito de um filme híbrido de fosfomolibdato e sílica organomodificada
RESUMO Materiais híbridos orgânico-inorgânicos nanoestruturados são produzidos com a finalidade de desenvolver e/ou aprimorar uma propriedade de interesse. Uma forma de obtenção de materiais híbridos é através da imobilização de um componente inorgânico em uma rede de sílica organicamente modificada (ormosil). Neste trabalho, um polioxometalato
Matéria (Rio J.). Publicado em: 25/11/2019
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11. Produção, caracterização e avaliação in vitro de partículas de quitosana e hidroxiapatita para substituição óssea
Resumo Objetivou-se desenvolver, caracterizar e avaliar in vitro biomateriais compósitos de quitosana com hidroxiapatita (CHI/HA) para atuarem como substitutos ósseos. As quitosanas de baixa (L-CHI) e média (M-CHI) massa molecular foram previamente caracterizadas por gravimetria, viscosimetria e espectrofotometria ultravioleta. Os compósitos de CHI/HA fo
Cerâmica. Publicado em: 14/11/2019
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12. Nanoparticles of Fe2O3 and Co3O4 as Efficient Electrocatalysts for Oxygen Reduction Reaction in Acid Medium
This paper presents a comparative study about the oxygen reduction reaction (ORR) catalyzed by nanoparticles of Fe2O3 and Co3O4 applied on the surface of glassy carbon electrodes (GCE). The nanoparticles were synthesized using the modified polymeric precursor method (Pechini). These two nanomaterials were characterized by Fourier transform infrared spectrosc
J. Braz. Chem. Soc.. Publicado em: 24/10/2019