Materials Synthesis
Mostrando 1-12 de 529 artigos, teses e dissertações.
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1. Catalysts Derived from Thermal Treatments of Hydrocalumite-Type Compounds: Synthesis and Application in Transesterification Reactions
Catalyst performance is a relevant factor in biodiesel production because it can affect the efficiency of the process. This work provides a study of the performance of heterogeneous catalysts for biodiesel production derived from thermal-treated hydrocalumite-type compounds. This work aimed to synthesize and characterize hydrocalumite-type compounds intercal
Journal of the Brazilian Chemical Society. Publicado em: 2023
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2. Sustainable and Reusable Sulfonic Acid-Functionalized Task-Specific Ionic Liquid Catalysts for Multicomponent Reactions. A Review
Improvements in Sustainable Organic Synthesis are usually related to the investigation of less hazardous, non-corrosive and renewable materials, as well as waste prevention, energy efficiency, solvent-free reactions, and the development of efficient reusable catalysts. In this context, multicomponent reactions emerged as important strategies for the rapid an
Journal of the Brazilian Chemical Society. Publicado em: 2022
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3. Chemometric Evaluation of Poly(3-hexylthiophene) Electrochemical Aging Path as a Function of Electrochemical Synthesis Variables
Conductive polymers are versatile materials that can be applied in many different technology fields, especially green energy. They have several advantages, such as easy synthesis, low density, and cost. However, its electric conduction property is also related to material aging with great loss of their characteristics, limiting their applicability. The in-de
Journal of the Brazilian Chemical Society. Publicado em: 2022
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4. Spectrofluorimetric Determination of Hydrochlorothiazide by a Carbon Dots-Based Probe via Inner Filtering Effect and Resonance Rayleigh Scattering
Synthesis of carbon dots (CDs) from natural resources not only enables green synthesis and production of environmentally friendly materials, but also provides a cost-effective probe as a fluorescence nanosensor. The proposed sensor introduces a unique one-pot hydrothermal CDs synthesis from alfalfa leaves, which is promising for sensing hydrochlorothiazide (
Journal of the Brazilian Chemical Society. Publicado em: 2022
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5. Avanços recentes na síntese do Remdesivir, Molnupiravir (EIDD-2801) e Tenofovir: moléculas promissoras no tratamento da COVID-19
RECENT ADVANCES IN THE SYNTHESIS OF REMDESIVIR, MOLNUPIRAVIR (EIDD-2801) AND TENOFOVIR: PROMISING MOLECULES IN THE TREATMENT OF COVID-19. The search for new treatments to contain the Covid-19 pandemic has highlighted the importance of nucleoside antivirals, such as Remdesivir, Tenofovir and Molnupiravir. Over the last two years, these molecules have been int
Química Nova. Publicado em: 2022
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6. Green Synthesis of Upconverting NaYF4 and NaGdF4 Materials and Energy Levels Determination
An alternative green route using a domestic microwave oven to synthesize NaGdF4:Yb,Tm and NaYF4:Yb,Er was successfully developed. Decreasing dopants concentration increased the β-NaREF4/α-NaREF4 ratio in NaGdF4. The scanning electron microscopy (SEM) images of NaGdF4 showed particles ranging from 500 nm to 1 μm with formation of aggregates up to 100 μm,
J. Braz. Chem. Soc.. Publicado em: 2021-08
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7. Effect of Preparation Additives on the Antimicrobial Activity and Cytotoxicity of Polypyrrole
The search for new biomaterials has increased continuously in recent years and, in this context, the application of polypyrrole (PPy) as a promising material for this function has been reported as a result of positive responses, such as bioactivity and biocompatibility. In this study, PPy was obtained through modifications/adaptations made in methodologies o
J. Braz. Chem. Soc.. Publicado em: 2021-06
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8. Thermal decomposition and reaction sintering for synthesis of mullite-zirconia composite using kaolin, γ-alumina and zirconia
Abstract The refractory materials used in the wall of the furnaces for glass melting can be prepared from mullite-zirconia composite material. The composite of mullite/zirconia was synthesized from Iraqi kaolin, γ-alumina, and zirconia using thermal decomposition with reaction sintering at 1600 °C. Several batches were prepared with various ratios of kaoli
Cerâmica. Publicado em: 2021-03
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9. Properties of Cu-Co Composite Catalysts for Synthesis of Aliphatic Alcohols
Cu-Co-containing cellulose-based carbon composite materials (Cu-Co/Cel) were formed by a matrix isolation method. Using X-ray diffraction (XRD), transmission electron microscopy (TEM), infrared-Fourier spectroscopy (IR-Fourier spectroscopy), and non-isothermal research methods, the physicochemical properties of the composites were established. The catalysts
J. Braz. Chem. Soc.. Publicado em: 2021-02
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10. Synthesis, Characterization and Exchange Reactions of Layered Double Hydroxides of Copper and Aluminum, Intercalated with Sulfate
Layered double hydroxides (LDHs) of Cu:Al in the molar ratio of 2:1, intercalated with sulfate, sulfate/(Li+, Na+, K+ or NH4+), NO3- and CO32-, were synthesized by co-precipitation with increasing pH. The materials were submitted to exchange reactions using B2SO4 (B = Li+, Na+, K+, NH4+) solutions in an attempt to replace previously intercalated cations or i
J. Braz. Chem. Soc.. Publicado em: 2021-01
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11. BIONANOCOMPÓSITOS POLIMÉRICOS À BASE DE MONTMORILLONITA – MATERIAIS DE INTERESSE CONTÍNUO
Polymeric bionanocomposites are versatile materials that have many practical applications. The wide use of these materials is mainly due to their structure and properties, which combine at nanometric scale, the functionality of biopolymers with the excellent stability of inorganic solids, such as the clay minerals family. Montmorillonite is the most widely e
Quím. Nova. Publicado em: 2020-12
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12. The 3C’s: COVID-19, Children, and Cardiac Surgery - Do we know enough?
ABSTRACT Objective The aim of this study was to translate and cross-culturally adapt the Insulin Delivery System Rating Questionnaire (IDSRQ) for Brazilian users. Validation and reliability analysis of measures were also performed. Materials and methods Methodological study comprising the following stages: forward translation, synthesis, back-translation
Braz. J. Cardiovasc. Surg.. Publicado em: 2020-12