Lle
Mostrando 1-12 de 61 artigos, teses e dissertações.
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1. SIMPLE AND FAST DETERMINATION FOR GAMMA-HYDROXYBUTYRATE (GHB) IN URINE SAMPLE BY LLE AND GC-MS
Gamma-hydroxybutyrate (GHB) is a depressant of the central nervous system able to promote disinhibition, anterograde amnesia and its use is related to Drug-Facilitated Crimes (DFC). Urine is the biological matrix of choice for toxicological analysis in victims of rape and/or theft in suspected victims of DFC. The aim of this work was the development of a sim
Quím. Nova. Publicado em: 2021-02
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2. Optimization and Validation of LLE-LTP and QuEChERS Methodologies for Determining 2,4-D in Water Samples
2,4-Dichlorophenoxyacetic acid (2,4-D) has been one of the main herbicides used to control weeds, however, due to its high use it can promote episodes of environmental contamination. Therefore, this study aimed to optimize and validate the liquid-liquid extraction with low-temperature partition (LLE-LTP) and the quick, easy, cheap, effective, rugged, and saf
J. Braz. Chem. Soc.. Publicado em: 2020-09
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3. [Atividade antibacteriana de biofilme de quitosana para conservação de ovos férteis e de mesa]
RESUMO O presente estudo teve como objetivo desenvolver um biofilme de quitosana contra Salmonella enteritidis, para conservação de ovos férteis e de mesa. Dois experimentos foram realizados. Experimento 1: 400 ovos de mesa livres de patógenos especificados foram divididos em delineamento inteiramente casualizado em quatro tratamentos, cinco repetições
Arq. Bras. Med. Vet. Zootec.. Publicado em: 2020-01
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4. Validação de método analítico por ELL-CG-EM para detecção de trialometanos decorrentes da cloração de águas contendo Microcystis
RESUMO Estudos demonstram que a utilização do cloro em estações de tratamento de água (ETA) pode contribuir para a formação de subprodutos orgânicos halogenados indesejados, tais como os trialometanos (TAM), quando há presença de matéria orgânica algogênica, composta de algas e cianobactérias. A Microcystis aeruginosa é uma espécie de cianoba
Eng. Sanit. Ambient.. Publicado em: 25/11/2019
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5. Simultaneous Determination of 2,3,7,8-TCDD and 2,3,7,8-TCDF in Water Samples by LLE-LTP and HPLC-DAD
Polychlorinated dibenzo-p-dioxins and dibenzofurans are persistent organic pollutants which can mainly be found in the environment in water. These compounds are highly toxic and therefore developing new extraction methodologies that are simpler and cost less is highly desirable. This study aimed to optimize and validate the liquid-liquid extraction with low-
J. Braz. Chem. Soc.. Publicado em: 23/05/2019
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6. EXPERIMENTAL DATA, THERMODYNAMIC MODELING AND SENSITIVITY ANALYSES FOR THE PURIFICATION STEPS OF ETHYL BIODIESEL FROM FODDER RADISH OIL PRODUCTION
Abstract The goals of this work were to present original liquid-liquid equilibrium data of the system containing glycerol + ethanol + ethyl biodiesel from fodder radish oil, including the individual distribution of each ethyl ester; to adjust binary parameters of the NRTL; to compare NRTL and UNIFAC-Dortmund in the LLE representation of the system containing
Braz. J. Chem. Eng.. Publicado em: 2017-01
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7. Determination of Amphetamine, Amfepramone and Fenproporex in Urine Samples by HPLC-DAD: Application to a Population of Brazilian Truck Drivers
Commercially available immunoassay tests are designed to detect the presence of amphetamine/methamphetamine or methylenodioxyamphetamines. However, it is known that Brazilian truck drivers also report the use of other illicit amphetamines, such as amfepramone and fenproporex. Thus, a method was developed and validated in order to quantify amphetamine-type st
J. Braz. Chem. Soc.. Publicado em: 2016-03
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8. LIQUID-LIQUID EQUILIBRIUM FOR TERNARY SYSTEMS CONTAINING ETHYLIC BIODIESEL + ANHYDROUS ETHANOL + REFINED VEGETABLE OIL (SUNFLOWER OIL, CANOLA OIL AND PALM OIL): EXPERIMENTAL DATA AND THERMODYNAMIC MODELING
Abstract Phase equilibria of the reaction components are essential data for the design and process operations of biodiesel production. Despite their importance for the production of ethylic biodiesel, the reaction mixture, reactant (oil and ethanol) and the product (fatty acid ethyl esters) up to now have received less attention than the corresponding system
Braz. J. Chem. Eng.. Publicado em: 2015-09
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9. IDENTIFICAÇÃO DE COMPOSTOS ORGÂNICOS EM LIXIVIADO DE ATERRO SANITÁRIO MUNICIPAL POR CROMATOGRAFIA GASOSA ACOPLADA A ESPECTROMETRIA DE MASSAS
The organic compounds present in leachate can contaminate soil, superficial and underground water, and the majority is considered harmful to the environment and human health. The objective of this study was to identify organic compounds present in landfill leachate located in Maringá-PR by gas chromatography coupled to mass spectrometry (GC-MS). The raw
Quím. Nova. Publicado em: 2015-07
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10. Residual feed intake and hematological and metabolic blood profiles of lle de France lambs
The objectives of this study were to estimate the phenotypic correlations of residual feed intake (RFI) and gross feed efficiency (GFE) with hematological and metabolic blood profiles of lambs and to determine the differences for these traits in animals of different RFI classes. Twenty Ile de France male lambs, 115±8 days of age and 31.3±4.1 kg of body wei
R. Bras. Zootec.. Publicado em: 2013-11
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11. Determination of liquid-liquid equilibrium data for biodiesel containing ternary systems using near infrared technique
This work is focused on the determination of liquid-liquid equilibrium data for systems containing methyl and ethyl fatty acid esters, water, glycerol and ethanol at temperatures of 303.15 K and 318.15 K using a near-infrared spectroscopy technique (NIR). The NIR method used in this investigation provided quite satisfactory results when compared to conventio
Braz. J. Chem. Eng.. Publicado em: 2013-03
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12. Avaliação das técnicas de microextração e eletroforese capilar em meio não aquoso (NACE) para determinação de antidepressivos em amostras de plasma para fins de monitorização terapêutica / Evaluation of microextractions techniques and nonaqueous capillary electrophoresis (NACE) for the determination of antidepressants in plasma samples for therapeutic drug monitoring
A monitorização terapêutica tem sido descrita como um recurso clínico valioso, na individualização do regime de dosagem, de acordo com a concentração do fármaco em amostras de plasma ou soro. O objetivo da monitorização terapêutica é assegurar a eficácia clínica e minimizar os efeitos adversos dos fármacos prescritos na clínica. A química a
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 02/03/2012