Liquid Liquid Extraction
Mostrando 1-12 de 758 artigos, teses e dissertações.
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1. Honey of Tetragonisca angustula from Southwestern Bahia: Influence of Seasonality on the Physicochemical Profile and Glioma Cell Inhibitory Effect
This study aims to analyze Tetragonisca angustula honey from southwestern Bahia for its physicochemical characteristics, phenolic compounds and glioma cell inhibitory effect, in samples from different periods of the year, dry (DP) and rainy (RP) period. The analyses showed that samples obtained in the DP and RP are statistically different for the physicochem
Journal of the Brazilian Chemical Society. Publicado em: 2023
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2. A Green Analytical Method Using Polyurethane Foam for The Extraction and Determination of Lauryl Ether Sulfate in Personal Care Hygiene Products
A green methodology was developed for the extraction and determination of lauryl ether sulfate in raw materials and commercial liquid soap and shower gel samples. The method avoids the use of organic solvents, offering a simple, cheap, and safe analysis. The methodology is based on the sorption of an ionic pair consisting of a cationic dye and an anionic sur
Journal of the Brazilian Chemical Society. Publicado em: 2022
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3. A New Approach for Histamine Functionalized Nanoparticles as Sorbent Phase for Bar Adsorptive Microextraction (BAµE) and Determination of Parabens in Water by HPLC-DAD
In this study, for the first time, histamine-functionalized magnetic nanoparticles (HIS-MNP) were used as sorbent phase combined with bar adsorptive microextraction (BAµE) for the determination of methylparaben (MP), ethylparaben (EP), propylparaben (PP), and butylparaben (BP) in water samples by high performance liquid chromatography coupled with diode arr
Journal of the Brazilian Chemical Society. Publicado em: 2022
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4. Use of Direct Aqueous Injection and Solid Phase Extraction Coupled with Hydrophilic Interaction Chromatography to Analyze Haloacetic Acids in Drinking Water Samples
In this study, two analytical methods were evaluated to determine haloacetic acids (HAAs) in drinking water samples. Direct aqueous injection (DAI) and solid phase extraction (SPE) were evaluated and determination was performed by liquid chromatography tandem mass spectrometry (LC-MS/MS) with a hydrophilic interaction chromatography (HILIC) analytical column
Journal of the Brazilian Chemical Society. Publicado em: 2022
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5. CYP450 Metabolism of a Semisynthetic Naphthoquinone, an Anticancer Drug Candidate, by Human Liver Microsomes
CNFD (6b,7-dihydro-5H-cyclopenta[b]naphtho[2,1-d]furan-5,6(9aH)-dione) is a semisynthetic naphthoquinone derived from lawsone that has cytotoxic action in different tumor lines and anticancer activity in vivo. Therefore, this molecule is a relevant candidate for drug development, but there is still no information on its human metabolism and systemic eliminat
Journal of the Brazilian Chemical Society. Publicado em: 2022
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6. Innovative gas chromatographic determination of formaldehyde by miniaturized extraction and on-fiber derivatization, via SPME and SPME Arrow
Formaldehyde (FA) is a carbonyl compound, ubiquitous in the environment and among the most widespread pollutants: it has exhibited toxic properties and is classified as a human carcinogen. FA is released from several sources, both temporary (e.g., combustion processes) and permanent (e.g., building products). This work proposes an innovative fully-automated
Química Nova. Publicado em: 2022
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7. Phytocomponents, Evaluation of Anticholinesterase Activity and Toxicity of Hydroethanolic Extracts of Parkia platycephala Benth.
This study evaluated the chemical composition, antioxidant and anticholinesterase activities, and the toxicity of hydroethanolic extracts of the Parkia platycephala Benth. Hot extraction with 70% hydroethanolic solution was used to obtain crude extracts of the leaf (LE), bark (BE), flower (FE), and seed (SE). Separation and identification of the compounds we
Journal of the Brazilian Chemical Society. Publicado em: 2022
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8. Stability Analyses by HPLC-MS of Guanitoxin Isolated from Sphaerospermopsis torques-reginae
Guanitoxin (GNT) is a natural organophosphate produced by some species of freshwater cyanobacteria, which inhibits the active site of acetylcholinesterase, preventing the hydrolysis of cholinesterases and consequently causing serious disturbances in the neuromuscular system. Despite having a chemical structure like synthetic organophosphates, there is still
J. Braz. Chem. Soc.. Publicado em: 2021-08
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9. A Systematic Pipeline to Enhance the Fecal Metabolome Coverage by LC-HRMS
The comprehended knowledge of the metabolic profile of the fecal matter has been recognized as an important point for understanding metabolic changes in the human systemic metabolism and it can provide precious information about host-gut microbiota interactions. However, few analytical strategies have been addressed for a broad analysis of metabolites with d
J. Braz. Chem. Soc.. Publicado em: 2021-07
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10. In vitro metabolism of copalic and kaurenoic acids in rat and human liver microsomes
Copalic (CA) and kaurenoic (KA) acids are the main diterpenes found in the oleoresin extracted from the copaiba tree (Copaifera sp). This study aimed to characterize the metabolism of CA and KA in rat and human liver microsomes using liquid chromatography with tandem mass spectrometry (LC-MS/MS). The in vitro assays showed deviations from the Michaelian kine
Quím. Nova. Publicado em: 2021-06
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11. An Online Solid Phase Extraction-Liquid Chromatography Tandem Mass Spectrometry Method for the Analysis of Parabens in Urban Waters
In this work, we report a method to quantify methylparaben, ethylparaben, propylparaben and butylparaben in urban waters of São Carlos (São Paulo State, Brazil) by online solid phase extraction-liquid chromatography tandem mass spectrometry (SPE-LC-MS/MS) system. The method achieved ng L-1 limits with good accuracy and precision (internal standards for eac
J. Braz. Chem. Soc.. Publicado em: 2021-05
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12. OPTIMIZATION OF BREWING WASTE’S (TRUB) PHENOLIC COMPOUNDS EXTRACTION BY ULTRASOUND ASSISTED USING RESPONSE SURFACE METHODOLOGY
The brewing waste, also known as trub, is an abundant by-product of the brewing industry. Such material presents high levels of phenolic compounds, which promote antioxidant, antimicrobial and antifungal effects, turning the trub economically attractive. In this study, the trub’s phenolic compounds were extracted by ultrasound-assisted extraction technolog
Quím. Nova. Publicado em: 2021-04