Gold Nanoparticles
Mostrando 1-12 de 92 artigos, teses e dissertações.
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1. Atomic Absorption Spectrometry as an Alternative to Determine the Presence of Gold Nanoparticles on or in Silica Matrix
Two different gold-silica-based nanomaterials were prepared: (i) silica-supported gold nanoparticles (AuNP/SiO2); and (ii) gold-silica core-shell nanoparticles (AuNP@SiO2). Three strategies for sample treatment (S), consisting in acid treatments, were employed: (S1) HNO3; (S2) HNO3 + HCl; and (S3) HF + HNO3 + HCl, applying microwave oven digestion for S2 and
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. A Colorimetric and Fluorescent Dual-Signal Sensor for Detecting Lipase Activity Based on Inner Filter Effect
We developed a colorimetric and fluorescence dual-signal sensor for detecting lipase activity based on methyl thioglycolate (MT) functionalized gold nanoparticles (MT-AuNPs) and CdS quantum dots (CdS QDs). It is the first time that was developed a dual-signal sensing strategy for lipase activity based on the inner-filter effect (IFE) between MT-AuNPs and CdS
Journal of the Brazilian Chemical Society. Publicado em: 2022
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3. Analytical method validation for the identification and quantification of dissolved gold and gold nanoparticles in cosmetics products by single particle inductively coupled plasma mass spectrometry
Nanoparticle (NP) applications have recently gained more space in the development of many products, especially in cosmetology. The aim of the present study was to validate a single particle inductively coupled plasma mass spectrometry technique for the detection and quantification of gold nanoparticles (AuNPs) and gold ions (Au (i)) in different cosmetics cu
Quím. Nova. Publicado em: 2021-06
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4. Device for Streptavidin Detection Using LSPR and Electrochemical Transductions on the same Platform
Research in biosensing currently occupies an important role among biomolecular detection techniques, especially with respect to medical diagnoses. Is this sense, the development of biosensors based on the localized surface plasmon resonance (an optical transducer) or electrochemical transductions have been highlighted. However, optical and electrochemical de
J. Braz. Chem. Soc.. Publicado em: 2021-04
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5. [5]Helicene-Scaffold Fluorescence Sensing for Selective Detection of Au3+ Ions and Gold Nanoparticle
A new quenching fluorescence sensor (MDP) with high productivity was easily synthesized from a [5]helicene anhydride derivative and propargyl bromide. This MDP sensor has significant photophysical properties, including high fluorescence emission and a large Stokes shift, and it exhibits selectivity and an excellent detection response in distinguishing Au3+ i
J. Braz. Chem. Soc.. Publicado em: 2021-04
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6. Molecularly Imprinted Polypyrrole on Glassy Carbon Electrode Modified with Reduced Graphene Oxide and Gold Nanoparticles for Isoamyl Alcohol Analysis in Fusel Oil
A molecularly imprinted electrochemical sensor for determination of isoamyl alcohol was successfully constructed by modifying the glassy carbon electrode (GCE) with gold nanoparticles (AuNPs) and reduced graphene oxide (RGO). The modification of the GCE increased the electron transfer rate and the electrode surface area, which, consequently, made more room a
J. Braz. Chem. Soc.. Publicado em: 2021-02
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7. An Electrochemiluminescence Biosensor for the Determination of Mercury Ion via Dual-Amplification Strategy
A novel dual-signal amplificatory electrochemiluminescence (ECL) deoxyribonucleic acid (DNA) biosensor was designed for the determination of Hg2+. One amplification unit was gold nanoparticles (AuNPs) modified on a glassy carbon electrode, and the other was single-stranded DNA (ssDNA) (with amino at the 3’ terminal and thiol at the 5’ terminal) labeled w
J. Braz. Chem. Soc.. Publicado em: 2020-12
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8. Gold Nanoparticle/Tetrapyridylporphyrin Hybrid Material: Spectroscopic and Electrocatalytic Properties and Sensor Application
An electrocatalytic active hybrid material prepared by successive stepwise coordinative deposition of 20 nm diameter gold nanoparticles (AuNP) with 5,10,15,20-tetra(4-pyridyl)-21H,23H-porphine (TPyP) on fluorine-doped tin oxide (FTO) substrates previously modified with 3-mercaptopropylsilane is described. Their interaction and assembly were studied by UV-Vis
J. Braz. Chem. Soc.. Publicado em: 2020-11
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9. Ações contra a Covid-19 na População com Síndrome de Down
An electrocatalytic active hybrid material prepared by successive stepwise coordinative deposition of 20 nm diameter gold nanoparticles (AuNP) with 5,10,15,20-tetra(4-pyridyl)-21H,23H-porphine (TPyP) on fluorine-doped tin oxide (FTO) substrates previously modified with 3-mercaptopropylsilane is described. Their interaction and assembly were studied by UV-Vis
Arq. Bras. Cardiol.. Publicado em: 2020-11
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10. Synthesis, Characterization and Photocatalytic Activity of Au/SiO2@TiO2 Core-Shell Microspheres
By using HAuCl4 as the gold precursor, spherical Au@SiO2/TiO2 core-shell nanostructures were prepared with the sol-gel method and ethanol reflux. The preparation process was convenient and fast. The obtained samples were characterized by UV-Vis, X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TE
J. Braz. Chem. Soc.. Publicado em: 2020-03
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11. CONSTRUÇÃO DE MINI FORNO PARA FUNCIONALIZAÇÃO TÉRMICA DE FASES ESTACIONÁRIAS MONOLÍTICAS
The present work describes a mini oven built to be applied in the preparation of monolithic stationary phase through the thermal polymerization approach. The developed device was successfully tested for functionalization of monolithic stationary phase in the internal surface of the silica capillary column fused with gold nanoparticles.
Quím. Nova. Publicado em: 2020-03
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12. HOTSPOT STABILIZATION OF GOLD NANOPARTICLES FOR APPLICATION OF QUANTITATIVE SERS IN BIOANALYTICAL SYSTEMS
A complete procedure including synthesizing gold nanoparticles and further hotspots stabilization is presented. Colloidal gold synthesis followed a citrate reducing reaction, then, an ideal condition for SERS enhancement with quantitative purposes was reached by searching equilibrium between salt- and analyte-induced aggregation. Under this condition, a mild
Quím. Nova. Publicado em: 05/12/2019