Ers 1
Mostrando 1-12 de 141 artigos, teses e dissertações.
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1. Determination of Ethyl Carbamate in Commercial Sweetened Sugar Cane Spirit by ESI-MS/MS Using Modified QuEChERS and 18-Crown-6/Trifluoroacetic Acid Spiking Additives
A fast, sensitive, and selective direct injection electrospray tandem mass spectrometry (DI ESI MS/MS) method that is able to quantify ethyl carbamate in commercial sweetened sugar cane spirit is described. The preparation method uses a modified QuEChERS (quick, easy, cheap, effective, rugged, and safe) with potassium carbonate added to sweetened sugar cane
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. [Moringa oleifera: um ingrediente alternativo na melhora da qualidade de ovos de codornas japonesas]
RESUMO O objetivo deste estudo foi avaliar a inclusão de Moringa oleifera na dieta de codornas japonesas sobre o desempenho, a qualidade de ovos, os parâmetros sanguíneos, o perfil bioquímico e o comportamento. Foram utilizadas 144 codornas japonesas, com aproximadamente 35 dias de idade, as quais foram distribuídas em delineamento inteiramente ao acaso
Arq. Bras. Med. Vet. Zootec.. Publicado em: 2021-05
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3. Validation of an UHPLC-MS/MS Method for the Determination of Malachite Green, Leucomalachite Green, Crystal Violet, and Leucocrystal Violet in Shrimp, Fish, and Salmon Muscle Using a Modified QuEChERS Approach
A quantitative and confirmatory method for detecting the presence of triphenylmethane dyes in shrimp muscle using ultra-high performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) and a quick, easy, cheap, effective, rugged and safe (QuEChERS) extraction approach was validated. The method exhibited linearity and selectivity and the coeffici
J. Braz. Chem. Soc.. Publicado em: 2021-04
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4. Optimization and Validation of LLE-LTP and QuEChERS Methodologies for Determining 2,4-D in Water Samples
2,4-Dichlorophenoxyacetic acid (2,4-D) has been one of the main herbicides used to control weeds, however, due to its high use it can promote episodes of environmental contamination. Therefore, this study aimed to optimize and validate the liquid-liquid extraction with low-temperature partition (LLE-LTP) and the quick, easy, cheap, effective, rugged, and saf
J. Braz. Chem. Soc.. Publicado em: 2020-09
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5. DETERMINAÇÃO DE MULTIRRESÍDUOS DE AGROTÓXICOS EM MÉIS PRODUZIDOS NA REGIÃO DO TRIÂNGULO MINEIRO POR UHPLC-MS/MS
Excessive use of pesticides can lead to the accumulation of residues in different parts of plants, endangering various species and contaminating foods. Honey can be used as an indicator of agricultural contamination and pre-mature bee mortality by pesticides. However, to quantify pesticide residues in honey, high sensitivity analytical methodologies are requ
Quím. Nova. Publicado em: 2020-03
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6. OTIMIZAÇÃO E VALIDAÇÃO DE MÉTODO BASEADO EM QuEChERS PARA DETERMINAÇÃO DE CONSERVANTES EM COSMÉTICOS POR HPLC-DAD
Parabens are widely used as preservatives in the last decades. Others preservatives such as 2-phenoxyethanol, which in addition to his good antimicrobial activity, has low allergenic potential as well others properties of interest to the cosmetic industry. In this work was developed a method for determination of methylparaben (MP), propylparaben (PP) and 2-p
Quím. Nova. Publicado em: 2020-02
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7. Influence of the mode of application of universal adhesive systems on adhesive properties to fluorotic enamel
Abstract The objective of this study is to compare the resin-enamel bond strength (mμSBS), in-situ degree of conversion (DC), and the enamel-etching pattern (SEM/EDX) of universal adhesive systems when applied to sound and fluorotic enamel. Ninety-eight human molars were sectioned into 4 parts and divided into 24 groups according to 1) enamel surface (sound
Braz. oral res.. Publicado em: 25/11/2019
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8. Força muscular respiratória e desempenho no Modified Shuttle Walk Test em escolares com fibrose cística
RESUMO O Modified Shuttle Walk Test (MSWT) é um teste de exercício potencialmente máximo que, associado à avaliação da força muscular respiratória (FMR), reflete a condição respiratória e a capacidade de exercício de escolares com fibrose cística (FC). O objetivo desta pesquisa foi investigar a relação entre FMR e distância percorrida (DP) no
Fisioter. Pesqui.. Publicado em: 18/07/2019
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9. Determination of Antibiotics Residues in Milk Using a QuEChERS Method Using Full Factorial Design and Liquid Chromatography-Tandem Mass Spectrometry
This study evaluated different methods of extraction based on quick, easy, cheap, effective, rugged and safe (QuEChERS) method for analysis of the antibiotics ceftiofur, cloxacillin and enrofloxacin in milk using ultra-performance liquid chromatography-tandem mass spectrometry. The QuEChERS acetate method has been shown to be inefficient for extracting such
J. Braz. Chem. Soc.. Publicado em: 04/07/2019
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10. Determination of Plant Growth Regulators in Chinese Herbal Medicine: A Comparison of Liquid (QuEChERS) and Solid (MSPD) Extraction Methods
This work aimed to compare the methods for the determination of twenty plant growth regulators (PGRs) from Chinese herbal medicines by applying liquid and solid extraction methods simultaneously. Quick, easy, cheap, effective, rugged and safe (QuEChERS) and matrix solid-phase dispersion (MSPD) were chosen as the liquid and solid extraction methods, respectiv
J. Braz. Chem. Soc.. Publicado em: 04/07/2019
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11. Determination of Phenolic Compounds in Red Sweet Pepper (Capsicum annuum L.) Using a Modified QuEChERS Method and UHPLC-MS/MS Analysis and Its Relation to Antioxidant Activity
In the present work, a fast, easy and efficient analytical method was developed and validated for the determination of phenolic compounds (4-hydroxybenzoic, vanillic, caffeic, p-coumaric, sinapic, ferulic and ellagic acids, and naringenin) in red sweet pepper. Extraction of phenolic compounds was carried out using the quick, easy, cheap, effective, rugged an
J. Braz. Chem. Soc.. Publicado em: 23/05/2019
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12. The Olympic Experimental Gymnasium Program and its Association with the Prevalence of Cardiovascular Risk Factors in Adolescents: A Cross-Sectional Study
Resumo Fundamento: A doença cardiovascular (DCV) é a principal causa de morte em todo o mundo. A atividade física (AF) e uma dieta adequada, quando adotadas na infância e na adolescência, podem reduzir a carga da DCV na fase adulta. O projeto “Ginásio Experimental Olímpico (GEO)” foi implementado para aumentar os níveis de AF dos estudantes por
Arq. Bras. Cardiol.. Publicado em: 08/04/2019