Electron Microscopy Analysis
Mostrando 13-24 de 2235 artigos, teses e dissertações.
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13. Microstructure and diametral fracture strength of spark plasma sintered WC-6Co-0.2B and WC-6Co-0.5B ceramic composites from nanosized and metastable WC powders
Abstract The present work aimed at evaluating the microstructures and mechanical properties of spark plasma sintered WC-6 wt% Co ceramic composites doped with boron (0.2 and 0.5 wt%). W-50 at% C (W-6.13 wt% C) powders produced under different milling times (20, 60, 180, and 600 min) were used as starting materials and subsequently mixed with Co (6 wt%) and B
Cerâmica. Publicado em: 2022
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14. Synergy between Experimental and Theoretical Investigations Reveals the Anti‑Corrosion Efficiency of Imine-Chalcones
The inhibitory action of three imine-chalcones on carbon steel corrosion in HCl was investigated by theoretical and experimental methods. Quantum descriptors were calculated at the conductor-like polarizable continuum model (CPCM)-Becke-3 Parameter-Lee-Yang-Parr (B3LYP)-D3/def2-TZVPP level allowing the prediction of efficiency inhibition ranking. Electrochem
J. Braz. Chem. Soc.. Publicado em: 2021-08
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15. A Comparison of the Photolytic and Photocatalytic Degradation of Triclosan: Identification of Transformation Products and Ecotoxicity Evaluation
Triclosan (5-chloro-2-(2,4-dichlorophenoxy)phenol) is commonly used as an antibacterial agent in various industrial products and is often detected in wastewater effluent. Comparison was made for triclosan degradation by photolysis and TiO2 photocatalysis (under UV irradiation (125 W)) based on analysis of transformation products, together with ecotoxicity ev
J. Braz. Chem. Soc.. Publicado em: 2021-08
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16. Agro-Industrial Waste Valorization: Transformation of Starch from Mango Kernel into Biocompatible, Thermoresponsive and High Swelling Nanogels
Mango industry processing disposes 40-60% of this fruit as residues, such as peels and kernels. The exploration of bioproducts from these industrial rejects can reduce environmental impact besides of producing high value-added materials. In this scenario, carboxymethyl starch nanoparticles were produced from mango (Mangifera indica L.) kernel starch. These n
J. Braz. Chem. Soc.. Publicado em: 2021-08
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17. Purification of raw palygorskite: a comparative study involving different processes and dispersing agents
Abstract Palygorskite (Pal) is a natural clay mineral with fibrous morphology and high surface area. Depending on the geological origin, it presents impurities, such as quartz and carbonates, which can harm some of its properties. Therefore, this work seeks to define a viable methodology for the purification of a Brazilian Pal. Two types of mixing processes
Cerâmica. Publicado em: 2021-06
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18. Dolomite-zirconia reaction sintered bonded coarse magnesia ceramics: effect of the bonding proportion
Abstract Refractory ceramic materials were manufactured, mainly composed of magnesia grains (coarse and medium fraction) and CaZrO3/MgO as a binding phase produced from the reaction sintering between CaMg(CO3)2 (dolomite) and m-ZrO2 (monoclinic zirconia), which constituted the finer fraction. Different relationships between the proportion and the size of the
Cerâmica. Publicado em: 2021-06
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19. Editorial Comment: Luts-V: A new simplified score for assessing lower urinary tract symptoms in men
Abstract Refractory ceramic materials were manufactured, mainly composed of magnesia grains (coarse and medium fraction) and CaZrO3/MgO as a binding phase produced from the reaction sintering between CaMg(CO3)2 (dolomite) and m-ZrO2 (monoclinic zirconia), which constituted the finer fraction. Different relationships between the proportion and the size of the
Int. braz j urol.. Publicado em: 2021-06
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20. Oxidative Stress & Male Infertility - A necessary and conflicted indissociable marriage: How and when to call for evaluation?
Abstract Refractory ceramic materials were manufactured, mainly composed of magnesia grains (coarse and medium fraction) and CaZrO3/MgO as a binding phase produced from the reaction sintering between CaMg(CO3)2 (dolomite) and m-ZrO2 (monoclinic zirconia), which constituted the finer fraction. Different relationships between the proportion and the size of the
Int. braz j urol.. Publicado em: 2021-06
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21. Editorial Comment: Vasectomy re-reversal: effectiveness and parameters associated with its success
Abstract Refractory ceramic materials were manufactured, mainly composed of magnesia grains (coarse and medium fraction) and CaZrO3/MgO as a binding phase produced from the reaction sintering between CaMg(CO3)2 (dolomite) and m-ZrO2 (monoclinic zirconia), which constituted the finer fraction. Different relationships between the proportion and the size of the
Int. braz j urol.. Publicado em: 2021-06
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22. Dysplasia of the fibrous sheath with axonemal and centriolar defects combined with lack of mitochondrial activity as associated factors of ICSI failure in primary ciliary dyskinesia syndrome
Abstract Refractory ceramic materials were manufactured, mainly composed of magnesia grains (coarse and medium fraction) and CaZrO3/MgO as a binding phase produced from the reaction sintering between CaMg(CO3)2 (dolomite) and m-ZrO2 (monoclinic zirconia), which constituted the finer fraction. Different relationships between the proportion and the size of the
Int. braz j urol.. Publicado em: 2021-06
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23. Acid matrix production from treated natural vermiculite-hydrobiotite
Abstract Given the potential of acid-activated clays in adsorptive and catalytic processes, several studies focusing on acid matrices have grown over the years, making it possible to study vermiculite, a mineral composed of a type 2:1 unit cell with tetrahedral and octahedral sheets. Therefore, this work aimed to study vermiculite treated with acids for the
Cerâmica. Publicado em: 2021-06
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24. Reduced Graphene Oxide/Ruthenium Oxide Hexacyanoferrate Nanocomposite for Electrochemical Determination of Ethanol in Commercial Samples
Reduced graphene oxide/ruthenium oxide hexacyanoferrate (rGO/RuOHCF) modified electrode showed synergic activity between the materials attested by the increase of electrochemical current and stability. The preparation of the nanocomposite was made by a simple two-step electrochemical approach. The material structure was characterized by spectroscopic techniq
J. Braz. Chem. Soc.. Publicado em: 2021-06