Diffuse Reflectance
Mostrando 13-24 de 114 artigos, teses e dissertações.
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13. Facile Preparation and Characterization of Nanostructured BiOI microspheres with certain adsorption-photocatalytic properties
A novel adsorbent based nanostructured bismuth oxyiodide (BiOI) microspheres combining the highly effective adsorption and green photocatalytic regeneration were fabricated by a facile and rapid low-temperature chemical bath method. The resultant products were characterized by X-ray diffraction (XRD), Scanning electron microscopy (SEM), energy dispersive spe
Mat. Res.. Publicado em: 12/04/2018
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14. Synthesis, Characterization and Enhanced Photocatalytic Activity of Iron Oxide/Carbon Nanotube/Ag-doped TiO2 Nanocomposites
A novel magnetically recoverable catalyst (Fe/MWCNT/TiO2-Ag) was prepared in this study by a process that involves few steps. Titanium dioxide doped with silver and iron oxide was deposited on support of multi-walled carbon nanotubes (MWCNT). The synthesized catalysts were characterized by inductively coupled plasma mass spectrometry (ICP-MS), N2 adsorption/
J. Braz. Chem. Soc.. Publicado em: 2017-12
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15. Synthesis and Characterization of LiCoO2 from Different Precursors by Sol-Gel Method
Lithium cobalt oxide, LiCoO2, widely used as cathode in lithium ion batteries was synthesized and their structural and electronic properties investigated. The crystalline powders were prepared by the sol-gel method with four complexing agents: citric acid, glycine, starch and gelatin. These syntheses were compared with the blank test (without complexing agen
J. Braz. Chem. Soc.. Publicado em: 2017-11
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16. Preparation of Zinc Oxide-Nanoclay Hybrids by Alkaline Ion Exchange Method
Abstract ZnO/nanoclay hybrids are synthesized by a single-step solid-state reaction using ZnCl2 as a reagent. These hybrids were prepared by a simple alkaline ion exchange method, without using any surfactant or chelating agents. By adjusting the reagent’s immersion time in molten salt, production of pure ZnO/nanoclay hybrids was achieved. Synthesized hybr
Braz. J. Chem. Eng.. Publicado em: 2017-10
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17. Synthesis, Characterization, and Photocatalytic Activity of Pure and N-, B-, or Ag- Doped TiO2
This article reports the synthesis and characterization of pure and N-, B-, and Ag-doped TiO2 and the ability of these oxides to photodegrade methylene blue (MB) under sunlight or UV-ABC radiation. The compounds were synthesized using the sol-gel method and characterized by scanning electron microscopy, X-ray diffraction, diffuse reflectance spectroscopy, Fo
J. Braz. Chem. Soc.. Publicado em: 2017-09
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18. Structure and Physical Properties of the LaBiFe2O6 Perovskite Produced by the Modified Pechini Method
In this paper the synthesis of the LaBiFe2O6 material by the modified Pechini method is reported. Structural, morphologic, magnetic and optic experimental studies were performed. Rietveld refinement of x-ray diffraction patterns revealed that LaBiFe2O6 crystallizes in an orthorhombic perovskite structure (space group Pnma, # 62). Scanning electron microscopy
Mat. Res.. Publicado em: 24/07/2017
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19. In Situ Photoactivated Plasmonic Ag3PO4@silver as a Stable Catalyst With Enhanced Photocatalytic Activity Under Visible Light
Silver orthophosphate (Ag3PO4) had been reported as an excellent candidate to split water or decompose pollutants with high efficiency in visible light region, yet is not stable due to the reduction of silver ion. In this work, an easy-fabricated method (in situ photoinduced reduction) was provided to enhance the stability of Ag3PO4 for its possible applicat
Mat. Res.. Publicado em: 03/04/2017
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20. Photocatalytic Activity and RNO Dye Degradation of Nitrogen-doped TiO2 Prepared by Ionothermal Synthesis
This work concerns the preparation a nitrogen-doped TiO2 by ionothermal synthesis methods and the photocatalytic studies. In this procedure, alkoxide was used as a titanium source, and a deep eutectic mixture of choline chloride and urea (molar ratio 1:2) served as a solvent and source of nitrogen. Different samples were synthesized varying the percentages o
Mat. Res.. Publicado em: 20/03/2017
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21. CdMoO4 Micro-ellipsoids: Controllable Synthesis, Growth Mechanism, and Photocatalytic Activity
CdMoO4 micro-ellipsoids were synthesized by a simple hydrothermal route with the assistance of nonionic surfactant Triton X-100 and characterized by X-ray diffraction, scanning electron microscopy and UV-Vis diffuse reflectance spectroscopy. The effects of hydrothermal pH, temperature, and time on the morphology and photocatalytic activity of CdMoO4 were inv
Mat. Res.. Publicado em: 21/11/2016
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22. Synthesis and Structural Properties of Niobium Pentoxide Powders: A Comparative Study of the Growth Process
Powders Nb2 O5 were prepared by two different synthesis method, Sol-Gel and polymeric precursors (Pechini). In the Pechini method before adding the citric acid in the process, four different solutions were used to get the samples. For Sol-gel method, two different processes were also used in obtaining powders. The precursor was completely solubilized in etha
Mat. Res.. Publicado em: 10/10/2016
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23. Cr/S/TiO2-LOADED HOLLOW GLASS MICROSPHERES AS AN EFFICIENT AND RECYCLABLE CATALYST FOR THE PHOTOCATALYTIC DEGRADATION OF INDIGO CARMINE UNDER VISIBLE LIGHT
Chromium and sulfur co-doped nanometer TiO2 hollow glass microspheres (Cr/S/TiO2-HGM) were synthesized by a sol-gel method. Characterization used X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), N2 adsorption-desorption (Brunauer-Emmett-Teller (BET) measurements) and UV-Vis diffuse reflectance spectrosc
Quím. Nova. Publicado em: 2016-09
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24. Structural, Optical and Photocatalytic Properties of Co-Tio2 Prepared by Sol-Gel Technique
In the present work, the Co/TiO2 nanocomposite was prepared by sol-gel method. The structural and optical properties of nanocomposite were studied using, X-ray diffraction (XRD) and diffuse reflectance UV-VIS spectrometry. The XRD spectra revealed its tetrahedral anatase structure. The grain size and optical properties of composite are also reported. Syntesi
Mat. Res.. Publicado em: 10/05/2016