Citrate Precursor
Mostrando 1-12 de 43 artigos, teses e dissertações.
-
1. Silver and gold nanoparticles from tannic acid: synthesis, characterization and evaluation of antileishmanial and cytotoxic activities
Abstract Gold (Au0) and silver (Ag0) nanoparticles were synthesized using tannic acid (TA) as both reducing and stabilizer. Nanoparticles formation, stability, and interaction with TA were compared to citrate-coated nanoparticles and monitored by UV-Vis, zeta potential, and transmission electron microscopy. TA coating resulted in a red-shift and broadening o
An. Acad. Bras. Ciênc.. Publicado em: 19/07/2018
-
2. Nanoestructura de perovskita doble La2NiMnO6 obtenido por ruta de citrato para supercapacitores
ABSTRACT In this paper, the study of double perovskite La2NiMnO6 as electrode material for supercapacitors is presented. The mixed oxide was prepared by citrate precursor route (CIT). The sample was calcined for 4 hours at 800 °C. The material was characterized by PXRD, SEM and FTIR spectroscopy. Cyclic voltammetry and galvanostatic charge/discharge measure
Matéria (Rio J.). Publicado em: 19/07/2018
-
3. Preparation of Au/TiO2 Catalyst by a Liquid-Phase Reduction Method for Preferential Oxidation of Carbon Monoxide in a Hydrogen Rich-Stream (CO-PROX reaction)
Au nanoparticles supported on TiO2 were prepared by a liquid-phase reduction method using HAuCl4.3H2O as the Au precursor, TiO2 as the support, a solution of ethylene glycol/water as solvent and reducing agent and sodium citrate as reducing agent and stabilizer. The Au/TiO2 catalysts were prepared using different routes and characterized by Energy-dispersive
Mat. Res.. Publicado em: 18/12/2017
-
4. Synthesis and Characterization of Cerium Molybdate Semiconductor Nanoparticles
Cerium molybdate semiconductive nanoparticles were synthesized by the EDTA-citrate combined complexation method. Gel thermal degradation behavior, phase formation, morphology, composition and band gap of cerium molybdate powders were characterized by TG/DSC, XRD, SEM/EDS and DRS analysis, respectively. The nanoparticles were synthesized by fixing the pH of t
Mat. Res.. Publicado em: 19/10/2017
-
5. Effect of La 0.8 Sr 0.2 MnO 3 powder addition in the precursor solution on the properties of cathode films deposited by spray pyrolysis
ABSTRACT Films of lanthanum strontium manganite, LSM (La0.8Sr0.2MnO3) were deposited on yttria stabilized zirconia (YSZ) substrates by different methods aiming to establish the most suitable route to prepare cathodes for solid oxide fuel cells (SOFC). Samples were obtained by using a solution of lanthanum, strontium and manganese nitrates or a dispersion of
Matéria (Rio J.). Publicado em: 11/05/2017
-
6. Innovative Coating Method of MgAl2O4 or ZnAl2O4 on α-Al2O3 Spheric Nuclei
Structured materials composed of α-Al2O3 spheres covered with a porous and thin layer of MgAl2O4 or ZnAl2O4 were obtained. The innovative coating method developed consists in the formation of a precursor gel of MgAl2O4 or ZnAl2O4 by citrate-nitrate combustion method. The alumina spheres are submerged in this gel and then submitted to a drying process in vac
Mat. Res.. Publicado em: 2015-04
-
7. A new electrochemical sensor containing a film of chitosan-supported ruthenium: detection and quantification of sildenafil citrate and acetaminophen
Este trabalho apresenta a construção de um novo sensor eletroquímico para detecção de analitos orgânicos, usando um eletrodo de carbono vítreo (GCE) modificado com um filme de rutênio suportado em quitosana. O filme de rutênio suportado em quitosana foi obtido a partir da síntese do complexo mer-[RuCl3(dppb)(H2O)] como precursor de [1,4-bis(difenil
J. Braz. Chem. Soc.. Publicado em: 2014-03
-
8. INSERÇÃO DE NANOPARTÍCULAS METÁLICAS EM RESINA EPÓXI: estudos espectroscópicos. / INSERTION OF METAL NANOPARTICLES IN EPOXY RESIN: spectroscopic studies.
This work describes the production and characterization of colloidal solution of silver nanoparticles (AgNPs) and insertion of this colloidal solution in a polymeric ma-trix of epoxy resin. The first stage of this work was the preparation of AgNPs in colloi-dal solution, using AgNO3 as the precursor, ethylene glycol as a medium and dispersant sodium citrate
Publicado em: 2011
-
9. Citrato de ródio(II): síntese, caracterização, adsorção em nanopartículas de maghemita e preparação de fluidos magnéticos / Rhodium(II) citrate: synthesis, characterization, adsorption on maghemita nanoparticles, and preparation magnetic fluids
Neste trabalho estão descritos a síntese e a caracterização do complexo dimérico citrato de ródio(II), estudo de sua adsorção em nanopartículas de maghemita e a preparação de fluidos magnéticos á base de nanopartículas modificadas com o complexo. O citrato de ródio (II) apresenta significante atividade antitumor sendo promissor para aplicaçã
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 10/03/2010
-
10. Síntese e caracterização de nanopartículas de TiO2 pelo método do precursor polimérico
Currently, scientific research in the field of nanotechnology has attracted growing interest because of its several applications, either through design of new products, materials characterization, production and application of structures, devices and systems in the form or function are features of the nanoscale. Thus, there is advancement in technology and i
Publicado em: 2010
-
11. Rhodium(II) citrate: synthesis, characterization, adsorption on maghemita nanoparticles, and preparation magnetic fluids / Citrato de ródio(II): síntese, caracterização, adsorção em nanopartículas de maghemita e preparação de fluidos magnéticos
Neste trabalho estão descritos a síntese e a caracterização do complexo dimérico citrato de ródio(II), estudo de sua adsorção em nanopartículas de maghemita e a preparação de fluidos magnéticos á base de nanopartículas modificadas com o complexo. O citrato de ródio (II) apresenta significante atividade antitumor sendo promissor para aplicaçã
Publicado em: 2010
-
12. Co2Z hexaferrite obtained by the citrate precursor method in an inert atmosphere
Nanoparticles of Co2Z hexaferrite were synthesized by the citrate sol-gel process under an inert atmosphere, then thermally analyzed by Thermogravimetric and Differential Thermal Analysis and characterized by X-ray Diffraction, Scanning Electron Microscopy, Atomic Force Microscopy, X-ray Fluorescence and Vibration Sample Magnetometry. Z-type barium hexaferri
Matéria (Rio de Janeiro). Publicado em: 2008-06