Capillary Electrophoresis
Mostrando 1-12 de 300 artigos, teses e dissertações.
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1. A Rational Procedure to Increase Selectivity in the Determination of an Elicitor as Salicylic Acid in Polygala Extracts Using Capillary Electrophoresis
Considering the economic potential of secondary metabolites, researches have been focusing several strategies in order to explore and enhance the accumulation of these metabolites in plant matrices in a broad context. One of those strategies is the development of suitable methodologies for the determination of some elicitors, such as salicylic acid (SA). Sin
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. A Simple Approach to Analyze Sugar Nectar Composition in Flowers Using Capillary Electrophoresis and Enzymatic Assays
Despite the obvious importance of nectar, the composition of this solution remains surprisingly understudied to most of the flowers. Here we describe a simple, low-cost, and reliable methodology to analyze the three main sugars present in 210 nectar samples of Christmas Bellflowers using capillary electrophoresis (CE) and enzymatic assays. CE separation (-16
J. Braz. Chem. Soc.. Publicado em: 2020-10
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3. CHARACTERIZATION OF INTERACTION BETWEEN BUDDLEOSIDE AND BOVINE SERUM ALBUMIN
The primary objective of this study was to investigate the binding of buddleoside to bovine serum albumin (BSA) by different analytical techniques. The analytical principles of affinity capillary electrophoresis (ACE) and fluorescence spectroscopy used in the experiments were different. Mobility (M) that is independent of viscosity of the operating buffer an
Quím. Nova. Publicado em: 20/07/2020
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4. Prevalence of hemoglobin abnormalities in an apparently healthy population in Benin
ABSTRACT Background: Sickle cell disease is the most common monogenic disorder in humans and is a major public health concern in sub-Saharan Africa. In Benin, the prevalence of sickle cell disease is estimated to be 4.8%. Our study aimed to describe the prevalence of hemoglobin abnormalities in an apparently healthy Benin population. Methods: One thousand
Hematol., Transfus. Cell Ther.. Publicado em: 2020-06
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5. Retraction notice for: “Risk factors for early-onset ventilator-associated pneumonia in aneurysmal subarachnoid hemorrhage patients” [Braz J Med Biol Res (2018) 51(7): e6830]
Due to its various structures in bio-compounds, snake venom is the indisputable result of evolutionary stages of molecules with an increasingly complex structure, high specificity, and of great importance for medicine because of their potential. The present study proposed an underpinning examination of venom composition from nine species of venomous snakes u
Braz J Med Biol Res. Publicado em: 2020-01
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6. Protein structure of the venom in nine species of snake: from bio-compounds to possible healing agents
Due to its various structures in bio-compounds, snake venom is the indisputable result of evolutionary stages of molecules with an increasingly complex structure, high specificity, and of great importance for medicine because of their potential. The present study proposed an underpinning examination of venom composition from nine species of venomous snakes u
Braz J Med Biol Res. Publicado em: 2020-01
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7. Development of a generic method for the determination of proton-pump inhibitors by capillary zoneelectrophoresis
A generic capillary zone electrophoresis method was developed for the analysis of four proton pump inhibitors: omeprazole, pantoprazole, lansoprazole and rabeprazole. During preliminary analysis screening of phosphate buffers at different pH levels was performed, in order to determine the optimum pH domain suitable for the simultaneous determination of all s
Braz. J. Pharm. Sci.. Publicado em: 30/09/2019
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8. A NEW VALIDATED METHOD FOR DETERMINATION OF ROFLUMILAST IN TABLET BY CZE-UV
This paper reports a new and validated capillary electrophoresis method to determine Roflumilast (RFL) with an internal standard in tablet. The separation was made on an uncoated fused-silica capillary column 50 cm effective length and 75 µm i.d. 20 mmol L-1 of Na2B4O7 buffer including 15% (v/v) methanol (pH=9.5) was used as background electrolyte. A potent
Quím. Nova. Publicado em: 18/07/2019
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9. Determination of Short Chain Fatty Acids in Mice Feces by Capillary Electrophoresis
Short-chain fatty acids (SCFA) are compounds produced during fermentation of gut microbiota. Acetic, propionic and butyric acids are the most important SCFA produced from non-digestible foods. We developed and validated a rapid and low-cost capillary electrophoretic (CE) method for determination of acetic, propionic and butyric acids in mice feces (100 mg of
J. Braz. Chem. Soc.. Publicado em: 23/05/2019
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10. Mating system analysis of Açaí-do-Amazonas (Euterpe precatoria Mart.) using molecular markers
Abstract Euterpe precatoria (Açaí-do-Amazonas) produces fruits of which the fresh pulp is consumed. It is almost exclusively collected by extractivist farmers, because no selected genotypes are available for the establishment of plantations. For the domestication and breeding of the species, mating system studies are needed for strategy formulation. This s
Crop Breed. Appl. Biotechnol.. Publicado em: 11/04/2019
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11. Stability-indicating capillary zone electrophoresis assay for the analysis of linezolid in tablets
A simple and fast alternative methodology using capillary zone electrophoresis (CZE) to analyze linezolid and its cationic photodegradation products in tablets has been developed. The separation was carried out on fused silica capillary and conducted using 100 mM formic acid (pH 3.0) and by applying 30 KV voltage. Detection was performed at UV 254 nm. The op
Braz. J. Pharm. Sci.. Publicado em: 08/04/2019
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12. Fast Determination of Iodine Number of Biodiesel Using Capillary Zone Electrophoresis with Multi- and Single-Point Calibration
A new and fast method was developed to determine the iodine number of biodiesel samples by capillary zone electrophoresis (CZE). In this procedure, the biodiesel sample reacts with Wijs solution in the presence of a catalyst and all the remaining iodine monochloride is converted to the iodide ion, which is quantified by CZE. Only small amounts of sample and
J. Braz. Chem. Soc.. Publicado em: 2019-02