Calorimetry
Mostrando 25-36 de 1010 artigos, teses e dissertações.
-
25. Synthesis, Characterization, and Synergic Photocatalytic Activity of Amorphous TiO2/Chitosan Carbon Microspheres
In this work, we report the synthesis and characterization of new amorphous graphene-like TiO2/chitosan carbon microspheres and its performance as photocatalyst. Four different carbon chitosan microspheres materials were obtained based on the distinctive procedure to incorporate TiO2 and TiOSO4 to chitosan structure by pyrolysis at 600 °C. Detailed characte
J. Braz. Chem. Soc.. Publicado em: 2020-06
-
26. Pyrolysis of the Caupi Bean Pod (Vigna unguiculata): Characterization of Biomass and Bio-Oil
The use of agricultural residues for the production of bio-oil is an important alternative to the use of fossil fuels. In this study, the Caupi bean pod (Vigna unguiculata) was characterized and used as biomass in the production of bio-oil. This biomass was evaluated in terms of physicochemical, morphological (scanning electron microscopy (SEM)), and thermal
J. Braz. Chem. Soc.. Publicado em: 2020-06
-
27. Theoretical and Experimental Investigations on Inclusion Complex β-Cyclodextrin and Sulcatone: A Cardiovascular Activity Evaluation
In this paper, we have applied state-of-the-art technologies and new investigations were developed focusing on obtaining simple and inexpensive molecules for treating cardiovascular diseases, as they are considered the leading cause of death in the world. For the first time, the inclusion complex of sulcatone (SU) and β-cyclodextrin (β-CD) was achieved (us
J. Braz. Chem. Soc.. Publicado em: 2020-05
-
28. BACTERIAL NANOCELLULOSE BIOMEMBRANE AS A SUPPORT FOR HUMAN INSULIN AIMING AT TRANSDERMAL PERMEATION
Production of bacterial nanocellulose was pursued as a matrix system for the stabilization of human insulin. The biomembranes produced by Gluconacetobacter hansenii were washed with 2% aqueous sodium dodecylsulfate solution, rinsed with ultrapure water and immersed in 1 mol L-1 NaOH aqueous solution at 60 °C for 90 min until neutralization. For the insulin
Quím. Nova. Publicado em: 2020-05
-
29. Structural and Functional Stabilization of Sericin from Bombyx mori Cocoons in a Biopolysaccharide Film: Bioorigami for Skin Regeneration
Development and optimization of a bioorigami film with silk sericin was pursued for skin regeneration. Several formulations were produced, with varying integrated sericin contents, viz. 0, 1, 2, 5, 10, 20 and 50 mgsericin mLfilm-1. The physico-chemical characteristics of the bioorigami films produced were evaluated via infrared spectrophotometry, X-ray diffr
J. Braz. Chem. Soc.. Publicado em: 2020-04
-
30. Glass Formation of Null-Matrix Cu-Hf-(Zr, Ti) Alloys
An approach following the null-matrix, Ti/Zr ratio of 2.08, for neutron diffraction was used to calculate the glass formation in Cu-Ti-(Hf,Zr) alloys. The Cu55Zr14.6Ti30.4, Cu61.48Hf18.52Zr6.48Ti13.52, Cu58.1Hf16.9Zr8.1Ti16.9 and Cu52.46Hf14.2Zr10.8Ti22.54 compositions (at. %), were calculated and prepared by argon arc melting. Copper die suction casting was
Mat. Res.. Publicado em: 13/01/2020
-
31. Preformulation of a liquid dosage formulation of captopril for pediatric use: drug-excipient compatibility and stability studies
Currently, medications used in children are typically modified from pharmaceutical dosage forms designed for adults. Captopril is widely adapted to liquid formulations for use in hospitals. Its stability in the aqueous medium is reduced since it undergoes oxidation producing captopril disulfide (its main metabolite). The aim of this formulation study was to
Braz. J. Pharm. Sci.. Publicado em: 20/12/2019
-
32. Physicochemical, Thermal, Structural and Pasting Properties of Unconventional Starches from Ginger (Zingiber officinale) and White Yam (Dioscorea sp.)
Abstract Ginger and white yam starches were investigated and compared with maize starch. Proximal composition, thermogravimetry, differential scanning calorimetry, microscopy, colourimetry, X-ray powder diffractometry and pasting profile were analysed. The unconventional starches presented higher protein and ash contents than the maize starch, that had the h
Braz. arch. biol. technol.. Publicado em: 20/12/2019
-
33. IMPACT OF TEMPERATURE ON THE STABILITY OF SILKWORM COCOON FIBERS
In this study raw and processed silkworm (Bombyx mori) cocoons were investigated using confocal Raman spectroscopy in conjunction with differential scanning calorimetry (DSC) in order to examine the effect of temperature on the molecular conformation of silk fiber structures. Using DSC, a broad endothermic curve was observed at moderate temperatures, sheddin
Quím. Nova. Publicado em: 05/12/2019
-
34. Microstructure and Thermal Analyses of Cu87-xAl13Nbx High-Temperature Shape Memory Alloys
This paper presents a thermal and microstructural characterization of Cu87-xAl13Nbx (wt%) high temperature shape memory alloys (HTSMA), with Nb contents ranging from 1 to 3%. The alloys were obtained by arc melting under argon atmosphere. Thermal characterization was performed by differential scanning calorimetry (DSC), revealing that the phase martensitic t
Mat. Res.. Publicado em: 28/11/2019
-
35. Characterization of Breast Meat Collected from Spent Lohmann Brown Layers in Comparison to Commercial Ross Broilers
ABSTRACT The objective of this study was to compare characteristics and properties of breast meat from spent Lohmann Brown layers (SP, 90 weeks old, n = 24) and those of commercial broilers (BR, 6 weeks old, n = 24). The breasts of both SP and BR were collected from a local processing plant, vacuum-packed in a plastic bag, and stored at -18ºC until further
Braz. J. Poult. Sci.. Publicado em: 25/11/2019
-
36. Experimentos de Calorimetria em Cursos Universitários
Resumo Neste trabalho investigamos em detalhes o experimento de calorimetria tipicamente realizado em cursos universitários. A motivação foi a consistente ocorrência de problemas na determinação por parte dos(as) estudantes do calor específico de uma peça de teste, muitas vezes obtendo-se valores negativos. Exploramos diversas variações do método
Rev. Bras. Ensino Fís.. Publicado em: 31/10/2019