Calibration
Mostrando 1-12 de 1189 artigos, teses e dissertações.
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1. Simultaneous Quantification of Amorphous and Crystalline Valsartan in Tablets Using Raman Spectroscopy and Chemometrics Tools
Valsartan is an antihypertensive active pharmaceutical ingredient (API), it is used in the amorphous state in the commercial products. As amorphous materials are metastable, amorphous valsartan can crystallize to valsartan E, promoting changes in the dissolution and bioavailability of the drug. Tablets containing metastable forms of APIs need special conditi
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Quantification of Carbon Dioxide (CO2), Methane (CH4), and Nitrous Oxide (N2O) Using Near Infrared Spectroscopy and Multivariate Calibration in High Humidity Levels
In this work we developed a promising analytical method combining Fourier transform near-infrared (FT-NIR) spectroscopic technique and first-order multivariate calibration using partial least-squares (PLS) model to simultaneously quantify the main greenhouse gases (GHG’s): methane (CH4), carbon dioxide (CO2), nitrous oxide (N2O) and water vapor (H2O). The
Journal of the Brazilian Chemical Society. Publicado em: 2022
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3. Nomogram for predicting post-traumatic hydrocephalus after decompressive craniectomy for traumatic brain injury
SUMMARY OBJECTIVE: This study aimed to develop and validate a practical nomogram to predict the occurrence of post-traumatic hydrocephalus in patients who have undergone decompressive craniectomy for traumatic brain injury. METHODS: A total of 516 cases were enrolled and divided into the training (n=364) and validation (n=152) cohorts. Optimal predictors w
Revista da Associação Médica Brasileira. Publicado em: 2022
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4. QUANTITATIVE SPECIATION OF THE LIQUID PHASE BY FTIR SPECTROSCOPY IN THE SYSTEM AMP-PZ-CO2-H2O
This work reports a multivariate calibration partial least square regression (PLS) model to quantify the liquid-phase concentrations of 2-amino-2-methyl-1-propanol (AMP), piperazine (PZ), bicarbonate, PZ monocarbamate, and PZ dicarbamate during the absorption/desorption process by Fourier Transform Mid-Infrared spectroscopy (mid-FTIR). The model could predic
Química Nova. Publicado em: 2022
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5. Atomic Absorption Spectrometry as an Alternative to Determine the Presence of Gold Nanoparticles on or in Silica Matrix
Two different gold-silica-based nanomaterials were prepared: (i) silica-supported gold nanoparticles (AuNP/SiO2); and (ii) gold-silica core-shell nanoparticles (AuNP@SiO2). Three strategies for sample treatment (S), consisting in acid treatments, were employed: (S1) HNO3; (S2) HNO3 + HCl; and (S3) HF + HNO3 + HCl, applying microwave oven digestion for S2 and
Journal of the Brazilian Chemical Society. Publicado em: 2022
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6. Simultaneous GC-NCI-MS Determination of Persistent Organic Pollutants and Current-Use Pesticides in Breast Milk Samples
To preserve human health, persistent organic pollutants (POPs) and current-use pesticides (CUPs) should be monitored in fatty tissues, including breast milk. Therefore, this study aimed to optimize sample preparation conditions using a 32 factorial design for the determination of POPs and CUPs by gas chromatography coupled to mass spectrometry with negative
Journal of the Brazilian Chemical Society. Publicado em: 2022
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7. Calibration of simulation parameters for wind erosion gas-solid two-phase flow in arid and semiarid soils
RESUMO Para construir um modelo de simulação acoplada da erosão eólica do solo e fluxo bifásico em regiões áridas e semi-áridas, os parâmetros de contato apropriados do modelo de simulação de elementos discretos do solo são obtidos com base no teste de calibração do ângulo de repouso (AoR). O modelo de simulação acoplado foi estabelecido atr
Revista Brasileira de Engenharia Agrícola e Ambiental. Publicado em: 2022
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8. Does successful urethral calibration rule out significant female urethral stenosis? confronting the confounder- an outcome analysis of successfully treated female urethral strictures
ABSTRACT Objective: The diagnosis and treatment of female urethral stricture disease (FUSD) are practiced variably due to the scarcity of data on evaluation, variable definitions, and lack of long-term surgical outcomes. FUSD is difficult to rule out solely on the basis of a successful calibration with 14F catheter. In this study, we have tried to character
Int. braz j urol.. Publicado em: 2021-08
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9. Editorial Comment: Does successful urethral calibration rule out significant female urethral stenosis? confronting the confounder- an outcome analysis of successfully treated female urethral strictures
ABSTRACT Objectives: To evaluate the impact of COVID-19 on clinical and surgical practice, educational activities, health and lifestyle behavior of Brazilian urology residents. Materials and Methods: A web-based survey was sent to 468 Brazilian urology residents from postgraduate years (PGY) 3 to 5 to collect data on clinical practice and training after 4
Int. braz j urol.. Publicado em: 2021-08
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10. Reliability assessment of cold-formed steel beams by the FORM method
Abstract This article presents a procedure for the reliability assessment of cold-formed steel beams based on the Direct Strength Method (DSM) and the Effective Section Method (ESM). Using a comprehensive database, a statistical analysis of the test results was performed to determine the statistical properties of the professional factor random variable. The
REM, Int. Eng. J.. Publicado em: 2021-06
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11. Risk-Prediction Model for Transfusion of Erythrocyte Concentrate During Extracorporeal Circulation in Coronary Surgery
Abstract Introduction: Our objective was to identify preoperative risk factors and to develop and validate a risk-prediction model for the need for blood (erythrocyte concentrate [EC]) transfusion during extracorporeal circulation (ECC) in patients undergoing coronary artery bypass grafting (CABG). Methods: This is a retrospective observational study inclu
Braz. J. Cardiovasc. Surg.. Publicado em: 2021-06
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12. Determination of carrageenan in jellies with new methylene blue dye using spectrophotometry, smartphone-based colorimetry and spectrophotometric titration
Abstract Carrageenan is a seaweed polysaccharide widely used as a food gelling and thickening agent. The New Methylene Blue dye was tested as an analytical reagent for the quantification of carrageenan in commercial jelly samples. The main spectral peaks of the dye decrease with increasing carrageenan-to-dye molar ratio up to 1. Three analytical procedures w
Food Sci. Technol. Publicado em: 2021-06