Atr Ftir Spectroscopy
Mostrando 13-24 de 64 artigos, teses e dissertações.
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13. Enhanced bioactive properties of BiodentineTM modified with bioactive glass nanoparticles
Abstract Objective To prepare nanocomposite cements based on the incorporation of bioactive glass nanoparticles (nBGs) into BiodentineTM (BD, Septodent, Saint-Maur-des-Fosses Cedex, France) and to assess their bioactive properties. Material and Methods nBGs were synthesised by the sol-gel method. BD nanocomposites (nBG/BD) were prepared with 1 and 2% nBG
J. Appl. Oral Sci.. Publicado em: 2017-04
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14. Amniotic membrane as an option for treatment of acute Achilles tendon injury in rats
Abstract Purpose: To evaluate the effect of human amniotic membrane (hAM) fragment on inflammatory response, proliferation of fibroblast and organization of collagen fibers in injured tendon. Methods: Sixty rats were divided into 3 groups: C - surgical procedures without tendon lesion and with simulation of hAM application; I - surgical procedures, tendo
Acta Cir. Bras.. Publicado em: 2017-02
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15. Effects of Methylcellulose on the Properties and Morphology of Polysulfone Membranes Prepared by Phase Inversion
Polymer solutions of polysulfone (PSf) and methylcellulose (MC) in 1-methyl-2-pyrrolidone (NMP) were used to prepare ultrafiltration membranes by the phase inversion technique via immersion precipitation. The effect of MC additive on the structure and performances of the membranes was studied. The obtained membranes were characterized by scanning electron mi
Mat. Res.. Publicado em: 23/01/2017
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16. Poly(dimethylsiloxane) and Poly[vinyltrimethoxysilane-co-2-(dimethylamino)ethyl methacrylate] Based Cross-Linked Organic-Inorganic Hybrid Adsorbent for Copper(II) Removal from Aqueous Solutions
An organic-inorganic hybrid adsorbent was prepared and its application for the uptake of CuII ions from aqueous solutions was studied. The polymer network was composed of poly(dimethylsiloxane) (PDMS), vinyltrimethoxysilane (VTMS), and 2-(dimethylamino)ethyl methacrylate (DMAEMA), described as PDMS-net-P(VTMS-co-DMAEMA). The chemical groups, thermal stabilit
J. Braz. Chem. Soc.. Publicado em: 2016-12
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17. Phosphate Modification of Nano Titania and Its Effect on the Photodegradation of EDTA
The surface of nano titania was phosphate modified and characterized by X-ray diffraction (XRD), attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), energy dispersive X-ray analysis (EDX), and elemental analysis (CHN) to show the existence of phosphate in the modified nano titania. The resultant phosphated nano titania was applie
J. Braz. Chem. Soc.. Publicado em: 2016-10
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18. Tissue dissolution and modifications in dentin composition by different sodium hypochlorite concentrations
ABSTRACT Sodium hypochlorite (NaOCl) remains the most used irrigation solution during root canal preparation because of characteristics such as wide-spectrum antimicrobial activity and organic tissue dissolution capacity. However, these solutions can alter dentin composition and there is no consensus on the optimal concentration of NaOCl to be used. Objecti
J. Appl. Oral Sci.. Publicado em: 2016-06
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19. 2-(4-IODO-2,5-DIMETOXIFENIL)-N-[(2-METOXIFENIL)METIL]ETAMINA OU 25I-NBOME: CARACTERIZAÇÃO QUÍMICA DE UMA DESIGNER DRUG
Drug trafficking and the introduction of new drugs onto the illicit market are one of the main challenges of the forensic community. In this study, the chemical profile of a new designer drug, 2-(4-iodine-2,5-dimethoxyphenyl)-n-[(2-methoxyphenyl)methyl]etamine or 25I-NBOMe was explored using thin layer chromatography (TLC), ultraviolet-visible spectrophotome
Quím. Nova. Publicado em: 2016-02
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20. FTIR Spectroscopy Revealing the Effects of Laser and Ionizing Radiation on Biological Hard Tissues
This work evaluated the influence of ionizing and non-ionizing irradiations on the chemical structure of hard tissues using the mid-infrared spectroscopy. Enamel, dentin and bone slabs were submitted to gamma irradiation, as well as to Nd:YAG (λ = 1064 nm) and Er,Cr:YSGG (λ = 2078 nm) laser irradiations. The composition of slabs were evaluated by the Fouri
J. Braz. Chem. Soc.. Publicado em: 2015-12
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21. Nickel-based Catalyst Precursor Prepared Via Microwave-induced Combustion Method: Thermodynamics of Synthesis and Performance in Dry Reforming of CH4
Nickel-based catalyst precursor for dry reforming of methane was successfully prepared by a self-combustion method. Three different amino acids: urea, glycine and citric acid were tested as fuels in the redox reaction with metal nitrates. For each fuel, a thermodynamic modeling of the combustion reaction was performed. The samples were characterized by X-ray
Mat. Res.. Publicado em: 25/08/2015
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22. Surface Modification and Spectroscopic Characterization of TiO2 Nanoparticles with 2-Aminoethyl Dihydrogen Phosphate
A common strategy for the surface modification of nano TiO2 and other metal oxide nanoparticles is based on anchor groups using chelating ligands that can carry additional functionalities. This would allow the exploration of further applications of these materials. In the present work, we report the modification of TiO2 nanoparticles
J. Braz. Chem. Soc.. Publicado em: 2015-08
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23. Synthesis of Poly(Dimethylsiloxane) Networks Functionalized with Imidazole or Benzimidazole for Copper(II) Removal from Water
Functionalized elastomeric networks were obtained via a polycondensation reaction between poly(dimethylsiloxane) (PDMS) containing Si(CH3)2OH as end groups and an imidazole- or benzimidazole-modified alkoxysilane. The structure of the polymeric materials was characterized via attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR) and
J. Braz. Chem. Soc.. Publicado em: 2015-02
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24. Evaluation of sample temperature and applied power on degradation of stearic acid in inductively coupled radio frequency plasma
Plasma cleaning is a promising technology in surface treatments, despite technological interest its use is limited because its mechanisms still are not entirely understood. This work aims to evaluate how the applied power of an inductively coupled RF discharge at 13,56 MHz, with Ar and Ar+10%O2 atmospheres, affects its capabilities to etch an organic molecul
Mat. Res.. Publicado em: 21/10/2014