Resistencia a união e padrão de condicionamento em esmalte de sistemas adesivos autocondicionantes aplicados de forma passiva ou ativa / Microtensile bond strength evaluation of self-etchiung adhesive systems on enamel

AUTOR(ES)
DATA DE PUBLICAÇÃO

2005

RESUMO

The aim of this study were evaluate the bond strength and conditioning pattern obtained from different self-etching adhesive systems applied on enamel by active and passive forms. 100 bovine incisors were sectioned in 6x6mm fragments from the buccal enamel surface. The specimens were divided into 10 groups (n= 1 O). It was used one single bottle adhesive system (Single Bond/3MESPE - SB) as Control and four self-etching adhesive systems (Tyrian SPE/BISCO - TV; Clearfil SE Bond/Kuraray - CL; One Up Bond F/Tokuyama OU and Prompt-LPop/3MESPE - PL). For each adhesive system, there were two experimental groups, The adhesive was applied by passive form (P) (during the waiting time previous the polymerization, the adhesive was left intact over the enamel surface) or the adhesive was applied by active form (A) (the adhesive was reapplied during the waiting time previous the polymerization). For the Con1rol group, the tooth were conditioned with 35% phosphoric acid/3MESPE for 30 seconds, washed with water spray for 15 seconds and lot dried with absorbent paper. Single Bond was applied following the manufacture s ins1ructions (passive con1ro! group)(Group 1). The same procedure was made for active con1rol group (Group 2), except during the waiting time previous the polymerization, the adhesive was continuously reapplied on the enamel surface, The self-etching adhesives were applied following the manufacturer s instructions, receiving both applications forms (passive and active). The specimens were restored with Filtek Z-250/3MESPE, Using a saw machine, were obtained specimens in a stick (beam) shape with 1,Omm2 1ransversal sectional area, Those sticks were individually fixed in a microtensile jig, attached in an universal testing machine. The bond strength values were analyzed by Two-way ANOVA and Tukey s test. The means, and standard deviations, expressed in MPa, were: SB/P - 10,86 (3,50)Ba; SB/A - 13,39 (1 ,24)Aa; TV/P - 9,17 (3, 19)Aab; TV/A - 8,21 (3,88)Abc; CljP 8,58 (2,46)Aab; CljA - 10,23 (3,58)Aabc; OU/P - 6,24 (1,61 )Bb; OU/A - 11,90 (2,12)Aab; PljP - 7,97 (0,91 )Aab; PL/A - 7,22 (2,05)Ac, For conditioning pattern analysis, 45 bovine incisors (n=5) were used. For groups 1 and 2, the teeth were conditioned with 35% phosphoric acid for 30 seconds, washed with water spray for 15 seconds and air dried, The self-etching adhesives were applied by passive and active forms. After that, those specimens were washed with water spray for 15 seconds, washed with acetone for 10 seconds and air dried. The specimens were prepared for SEM and observed in a JEOL 5600 LV. The images suggested that the conditioning pattern is related to bond s1rength values, that presented statistical differences for some adhesives studied

ASSUNTO(S)

dental enamel esmalte dentario

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